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Chapter 2: Prerequisites

 

 

Product Service 1-800-522-7658 

Vacuum Pump Requirements 

The inlet fitting on the vacuum pump must be suitable for 0.50 ID hose. 
 

IMPORTANT NOTE: When selecting the vacuum pump it is very important 
to consider the flammability of the solvent that will be used.  If the solvents 
are flammable, an explosion-proof vacuum pump or one suitable for the 
solvents to be processed is recommended. See Chapter 3 Solvent Safety 
Precautions for solvents suitable for use in the CentriVap Cold Trap

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To ensure that aggressive vapors do not damage the vacuum pump, it is 
recommended that all internal wetted parts of the vacuum pump are PTFE 
or PTFE coated when using aggressive solutions. 

 

Chemical Traps 

The CentriVap Cold Trap will not provide complete vacuum pump protection 
under all circumstances. Variables that influence the Cold Traps trapping ability 
are volatility of the solvents, solvent volumes, solvent temperatures, and vacuum 
levels. Some scenarios may require a Chemical Trap for additional vacuum pump 
protection. This in-line cannister is placed after the Cold Trap and before the 
vacuum pump and holds inserts for specific sample types. Acid, solvent, moisture 
and radioisotope inserts are available. Refer to Chapter 5: Accessories for Your 
CentriVap for ordering information. 

NOTE: Several components within the CentriVap Cold Trap are made from 
stainless steel or other materials and can be degraded if exposed to acids.  
Contact Labconco before evaporating acids. 

Space Requirements 

Refer to Appendix B: Cold Trap Dimensions for dimensional drawings of the 
CentriVap Cold Traps. 
 
No person or any hazardous material should be within 12 inches of the CentriVap 
Cold Trap while it is operating. 
 
 
 

Содержание CentriVap 78110 Series

Страница 1: ...CentriVap Cold Traps Models 78110 Series 74600 Series 73850 Series...

Страница 2: ...ours of 7 30 a m and 5 30 p m Central Standard Time Part 7539802 Rev ECO L795 Warranty Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and reasona...

Страница 3: ...ctions 8 Electrical Connection 9 Ground Wire 9 Chemical Resistance of CentriVap Cold Trap Components 9 Solvent Safety Precautions 10 CHAPTER 4 MAINTAINING YOUR CENTRIVAP COLD TRAP 12 CHAPTER 5 ACCESSO...

Страница 4: ......

Страница 5: ...umes as they evaporate from the samples The stainless steel trap is used for aqueous and organic applications For corrosive applications the optional Glass Trap insert should be used The 230V 50Hz mod...

Страница 6: ...Chapter 1 Introduction Product Service 1 800 522 7658 2 It is important that you understand the warnings listed throughout this manual before you operate the CentriVap Cold Trap...

Страница 7: ...onstruction In addition a means to exhaust the vacuum pump must be provided An electrical source must be located near the installation site Carefully read this chapter to learn The electrical supply r...

Страница 8: ...d be located on a surface that is stable flat and level WARNING Solvents used in the Cold Trap can cause skin eye respiratory and digestive system disorders The CentriVap Cold Trap System should be lo...

Страница 9: ...omplete vacuum pump protection under all circumstances Variables that influence the Cold Traps trapping ability are volatility of the solvents solvent volumes solvent temperatures and vacuum levels So...

Страница 10: ...ve your CentriVap Cold Trap Set up your CentriVap Cold Trap Connect the electrical supply source to your CentriVap Cold Trap Properly exhaust your CentriVap Cold Trap Safely use solvents with your Cen...

Страница 11: ...eceive one or more of the components listed for your CentriVap Cold Trap contact Labconco Corporation immediately for further instructions 1334500 1336100 1332600 1332700 1338000 1336400 1336500 13326...

Страница 12: ...of the barb fittings on the Cold Trap Cover Assembly Secure the hoses with the clamps supplied Attach another hose to the remaining barb fitting on the Cold Trap Cover and clamp securely If the acces...

Страница 13: ...r Anodized Aluminum D D Rotor Hub Acetal Delrin C C C D D D C D C Tubing PVC D C D D D D D D D C D D D D Acid Resistant CentriVap Chamber Teflon coated Aluminum Lid Glass Bearings Stainless Steel D D...

Страница 14: ...acuum pump oil can be extended if the vacuum pump is operated for an extended period of time with the gas ballast open after the run is over This allows contaminants to be purged from the hot oil This...

Страница 15: ...MPORTANT NOTE The disposal of substances used in connection with this equipment may be governed by various Federal State or local regulations All users of this equipment are urged to become familiar w...

Страница 16: ...method will not damage equipment 1 Clean up all spills remove liquids from the chamber Clean or decontaminate all surfaces using agents suitable for the substance spilled 2 Clean lid and gasket using...

Страница 17: ...uity 10 Repair any defects to the surface where the CentriVap Cold Trap is installed Monthly 1 The rubber components on the CentriVap Cold Trap may eventually deteriorate and require replacement The e...

Страница 18: ...Trap The configuration of your CentriVap Cold Trap can be changed to accommodate your needs You may wish to add a secondary trap to trap vapors exhausted from the vacuum pump Read this chapter to lea...

Страница 19: ...Vacuum Pump Corrosion resistant 115V 50 60 Hz 3 5 amps single phase 82 liters minute 2 mBar vacuum 7393001 Diaphragm Vacuum Pump Corrosion resistant 230V 50 60 Hz 2 0 amps single phase 82 liters minut...

Страница 20: ...rt on the vacuum pump Clamp hoses securely Unscrew the clear bowl of the canister housing from the head Remove both the upper and lower caps from the filter cartridge and insert the small end of the c...

Страница 21: ...he fitting on the center tube of the Glass Trap and clamp securely Attach the hose from the vacuum pump or Secondary Trap to the other fitting on the Glass Trap and clamp securely Be certain that the...

Страница 22: ...not connected to electrical power Connect unit to proper electrical receptacle Circuit breaker blown Correct electrical problem and reset circuit breaker by pressing button Sample odor in lab Vent ho...

Страница 23: ...Insert is spent Replace with new insert New Secondary Trap has moisture in it Run vacuum pump for 24 hours to remove moisture Recovery of condensate in Cold Trap is less than normally expected Cold T...

Страница 24: ...Appendix A CentriVap Cold Trap Components The following pages list components that are available for your CentriVap Cold Trap The parts shown are the most common replacement parts If other parts are...

Страница 25: ...sor 115V 6A 1 7437701 Compressor 230V 50Hz 6B 1 7734402 Compressor 230 60Hz 7 1 7936200 Drier 8 1 7387300 Line Assembly 9 1 1360500 Valve 10 1 7464600 Wire Assembly Ground 11 1 7399700 Lid Assembly 12...

Страница 26: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 22...

Страница 27: ...2 1327208 Circuit Breaker 230V 9 2 1548603 Stem Adapter 10 2 1544501 Elbow 11 2 1548101 Stem 12 1 7398900 Insulation Lid Assembly 13 1 1334500 Power Cord 115V Not Shown 13A 1 1336100 Power Cord 230V E...

Страница 28: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 24...

Страница 29: ...2 1289308 Circuit Breaker 230V 9 2 1548603 Stem Adapter 10 2 1544501 Elbow 11 2 1548101 Stem 12 1 7398900 Insulation Lid Assembly 13 1 1336400 Power Cord 115V Not Shown 13A 1 1336500 Power Cord 230V E...

Страница 30: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 26...

Страница 31: ...Product Service 1 800 522 7658 27 Appendix B CentriVap Cold Trap Dimensions CentriVap Cold Trap 50 C Models...

Страница 32: ...Appendix B CentriVap Cold Trap Dimensions Product Service 1 800 522 7658 28 CentriVap Cold Trap 85 C Models...

Страница 33: ...Appendix B CentriVap Cold Trap Dimensions Product Service 1 800 522 7658 29 CentriVap Cold Trap 105 C Models...

Страница 34: ...ting conditions Electrical Specifications Nominal amperage for 115V 60Hz Cold Trap 50 Models 6 0A Nominal amperage for 230V 50 60Hz Cold Trap 50 Models 2 5A Nominal amperage for 115V 60Hz Cold Trap 85...

Страница 35: ...C Main supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes...

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