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Chapter 6: Troubleshooting 

 

Product Service 1-800-522-7658 

19 

PROBLEM 

CAUSE 

CORRECTIVE ACTION 

No vacuum/poor vacuum 
(cont.)

 

Pump is not functioning 
properly 

Check pump by locating vacuum gauge 
closer to pump and close off rest of system.  
Check pump oil for cloudiness or particles 
and change. 

 

 

 

 

 

If pump is faulty, seek authorized service or 
replace pump. 

 

 

 

 

Cold Trap lid not seated 

Hold lid down until vacuum is initiated. 

 

 

 

 

Ice formed on Cold 
Trap lid sealing 
surface 

Defrost and wipe dry. 

 

 

 

 

Secondary Trap 
Cannister not fitted 
properly 

Tighten all connections to and from the 
Secondary Trap Cannister. 

 

 

 

 

Secondary Trap Insert 
is spent 

Replace with new insert. 

 

 

 

 

New Secondary Trap 
has moisture in it 

Run vacuum pump for 24 hours to 
remove moisture. 

 

 

 

Recovery of condensate 
in Cold Trap is less than 
normally expected 

Cold Trap is not ON 

Check to make sure switch is ON and 
condensing unit fan is moving air out of 
the rear of the cabinet. 

 

 

 

 

Cold Trap does not 
cool down 

Turn vacuum pump OFF and allow 
Cold Trap to cool for at least 30 min. to 
reach temperature. 

 

 

 

 

 

-50°C temperature can be checked with 
a solvent thermometer or digital 
thermometer. 

 

 

 

Frequent oil change 
needed in pump 

Secondary Trap insert 
is spent 

Change insert often. 

 

 

 

 

Cold Trap is not 
emptied after each run 
and dried 

Empty the traps (glass or stainless steel) 
after each run and replace. 

 

 

 

 

Vacuum too strong for 
chemical  

Use a Secondary Trap insert and 
diaphragm pump. 

 

 

 

 

Содержание CentriVap 78110 Series

Страница 1: ...CentriVap Cold Traps Models 78110 Series 74600 Series 73850 Series...

Страница 2: ...ours of 7 30 a m and 5 30 p m Central Standard Time Part 7539802 Rev ECO L795 Warranty Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and reasona...

Страница 3: ...ctions 8 Electrical Connection 9 Ground Wire 9 Chemical Resistance of CentriVap Cold Trap Components 9 Solvent Safety Precautions 10 CHAPTER 4 MAINTAINING YOUR CENTRIVAP COLD TRAP 12 CHAPTER 5 ACCESSO...

Страница 4: ......

Страница 5: ...umes as they evaporate from the samples The stainless steel trap is used for aqueous and organic applications For corrosive applications the optional Glass Trap insert should be used The 230V 50Hz mod...

Страница 6: ...Chapter 1 Introduction Product Service 1 800 522 7658 2 It is important that you understand the warnings listed throughout this manual before you operate the CentriVap Cold Trap...

Страница 7: ...onstruction In addition a means to exhaust the vacuum pump must be provided An electrical source must be located near the installation site Carefully read this chapter to learn The electrical supply r...

Страница 8: ...d be located on a surface that is stable flat and level WARNING Solvents used in the Cold Trap can cause skin eye respiratory and digestive system disorders The CentriVap Cold Trap System should be lo...

Страница 9: ...omplete vacuum pump protection under all circumstances Variables that influence the Cold Traps trapping ability are volatility of the solvents solvent volumes solvent temperatures and vacuum levels So...

Страница 10: ...ve your CentriVap Cold Trap Set up your CentriVap Cold Trap Connect the electrical supply source to your CentriVap Cold Trap Properly exhaust your CentriVap Cold Trap Safely use solvents with your Cen...

Страница 11: ...eceive one or more of the components listed for your CentriVap Cold Trap contact Labconco Corporation immediately for further instructions 1334500 1336100 1332600 1332700 1338000 1336400 1336500 13326...

Страница 12: ...of the barb fittings on the Cold Trap Cover Assembly Secure the hoses with the clamps supplied Attach another hose to the remaining barb fitting on the Cold Trap Cover and clamp securely If the acces...

Страница 13: ...r Anodized Aluminum D D Rotor Hub Acetal Delrin C C C D D D C D C Tubing PVC D C D D D D D D D C D D D D Acid Resistant CentriVap Chamber Teflon coated Aluminum Lid Glass Bearings Stainless Steel D D...

Страница 14: ...acuum pump oil can be extended if the vacuum pump is operated for an extended period of time with the gas ballast open after the run is over This allows contaminants to be purged from the hot oil This...

Страница 15: ...MPORTANT NOTE The disposal of substances used in connection with this equipment may be governed by various Federal State or local regulations All users of this equipment are urged to become familiar w...

Страница 16: ...method will not damage equipment 1 Clean up all spills remove liquids from the chamber Clean or decontaminate all surfaces using agents suitable for the substance spilled 2 Clean lid and gasket using...

Страница 17: ...uity 10 Repair any defects to the surface where the CentriVap Cold Trap is installed Monthly 1 The rubber components on the CentriVap Cold Trap may eventually deteriorate and require replacement The e...

Страница 18: ...Trap The configuration of your CentriVap Cold Trap can be changed to accommodate your needs You may wish to add a secondary trap to trap vapors exhausted from the vacuum pump Read this chapter to lea...

Страница 19: ...Vacuum Pump Corrosion resistant 115V 50 60 Hz 3 5 amps single phase 82 liters minute 2 mBar vacuum 7393001 Diaphragm Vacuum Pump Corrosion resistant 230V 50 60 Hz 2 0 amps single phase 82 liters minut...

Страница 20: ...rt on the vacuum pump Clamp hoses securely Unscrew the clear bowl of the canister housing from the head Remove both the upper and lower caps from the filter cartridge and insert the small end of the c...

Страница 21: ...he fitting on the center tube of the Glass Trap and clamp securely Attach the hose from the vacuum pump or Secondary Trap to the other fitting on the Glass Trap and clamp securely Be certain that the...

Страница 22: ...not connected to electrical power Connect unit to proper electrical receptacle Circuit breaker blown Correct electrical problem and reset circuit breaker by pressing button Sample odor in lab Vent ho...

Страница 23: ...Insert is spent Replace with new insert New Secondary Trap has moisture in it Run vacuum pump for 24 hours to remove moisture Recovery of condensate in Cold Trap is less than normally expected Cold T...

Страница 24: ...Appendix A CentriVap Cold Trap Components The following pages list components that are available for your CentriVap Cold Trap The parts shown are the most common replacement parts If other parts are...

Страница 25: ...sor 115V 6A 1 7437701 Compressor 230V 50Hz 6B 1 7734402 Compressor 230 60Hz 7 1 7936200 Drier 8 1 7387300 Line Assembly 9 1 1360500 Valve 10 1 7464600 Wire Assembly Ground 11 1 7399700 Lid Assembly 12...

Страница 26: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 22...

Страница 27: ...2 1327208 Circuit Breaker 230V 9 2 1548603 Stem Adapter 10 2 1544501 Elbow 11 2 1548101 Stem 12 1 7398900 Insulation Lid Assembly 13 1 1334500 Power Cord 115V Not Shown 13A 1 1336100 Power Cord 230V E...

Страница 28: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 24...

Страница 29: ...2 1289308 Circuit Breaker 230V 9 2 1548603 Stem Adapter 10 2 1544501 Elbow 11 2 1548101 Stem 12 1 7398900 Insulation Lid Assembly 13 1 1336400 Power Cord 115V Not Shown 13A 1 1336500 Power Cord 230V E...

Страница 30: ...Appendix A CentriVap Cold Trap Components Product Service 1 800 522 7658 26...

Страница 31: ...Product Service 1 800 522 7658 27 Appendix B CentriVap Cold Trap Dimensions CentriVap Cold Trap 50 C Models...

Страница 32: ...Appendix B CentriVap Cold Trap Dimensions Product Service 1 800 522 7658 28 CentriVap Cold Trap 85 C Models...

Страница 33: ...Appendix B CentriVap Cold Trap Dimensions Product Service 1 800 522 7658 29 CentriVap Cold Trap 105 C Models...

Страница 34: ...ting conditions Electrical Specifications Nominal amperage for 115V 60Hz Cold Trap 50 Models 6 0A Nominal amperage for 230V 50 60Hz Cold Trap 50 Models 2 5A Nominal amperage for 115V 60Hz Cold Trap 85...

Страница 35: ...C Main supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes...

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