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DOC1049R (22 February 2024 12:07) 

www.keit.co.uk 

Back to Table of Contents 

This document should be read in conjunction with  DOC1048R IRmadilloNA User Manual 

– 

Safety. 

1.1.  Purging the IRmadilloNA 

The  IRmadilloNA  spectrometer  is  designed  to  be  continuously  purged.  This  eliminates  any 
interference in operation caused by changing levels of water vapour and carbon dioxide (CO

2

within the instrument, both of which interact strongly with infrared (IR) light. 

The IRmadilloNA is fitted with purge inlets on the probe and spectrometer body. The Inlets are 
shipped with blanking plugs that need to be removed before use. There are breathers on both 
the probe and spectrometer body.  

 

Figure 1: Purge inlet and outlet locations on ASM0627-09 

The ideal purge gas is dry nitrogen. Alternatively, dry air from a purge gas generator can be 
used. The output from this purge gas generator should have a minimum quality according to 
ISO8573-1:2010  of  Class  1:2:1  (dust:water:oil)  or  better.  Keit  can  recommend  suitable 
generators  that  achieve  this  outlet  air  quality;  contact  [email protected].  Purge  gas 
generators may include an internal compressor or use factory-supplied compressed air with a 
minimum quality of Class 4:4:4 (dust:water:oil). 

 

NOTE 

REMARQUE 

All FTIR spectrometers are very sensitive to water vapour and 
carbon  dioxide.  Even  in  well-controlled  environments,  e.g., 
laboratories,  environmental  changes  can  be  large  enough  to 
cause  significant  changes  in  the  spectrum.  We  STRONGLY 
recommend purging the instrument at all times. 

Tous les spectromètres FTIR sont très sensibles à la vapeur d’eau 
et au dioxyde de carbone. Même dans des environnements contrôlés 
(des 

laboratoires, 

par 

exemple), 

les 

changements 

dans 

l’environnement peuvent être suffisants pour causer des variations 
de spectre significatives. Il est VIVEMENT recommandé de toujours 
purger l’instrument. 

 

 

 

Содержание IRmadillo DOC1049R

Страница 1: ...DOC1049R 22 February 2024 12 07 DOC1049R IRmadilloNA User Manual Hardware Model Number ASM0627 09 N Cx O Gx D3x www keit co uk support keit co uk...

Страница 2: ...nd 7 2 Maintenance 8 2 1 Spectrum health 8 2 1 1 Use at high temperature 8 2 1 2 Emitter ageing 9 2 2 Remote health check 9 2 3 Cleaning the fibre optic data cable connectors 9 2 3 1 Cleaning the Sour...

Страница 3: ...e used The output from this purge gas generator should have a minimum quality according to ISO8573 1 2010 of Class 1 2 1 dust water oil or better Keit can recommend suitable generators that achieve th...

Страница 4: ...If the purge tubing is disconnected the blanking plugs must be fitted to the inlet connections on the probe and body to maintain the IP rating and exclude dust The IRmadilloNA requires a stabilisation...

Страница 5: ...reduced diameter section of the pipe The minimum flow velocity should be 1 5 m s 5 ft s 4 Install the IRmadilloNA so that the probe tip is fully in the flow We recommend putting the probe tip as close...

Страница 6: ...d The following are suitable Water Acetone Alcohols Surfactant solutions Alkanes hexane cyclohexane etc Ethers Once exposed to a suitable solvent wipe the ATR with a clean cloth The metal tube of the...

Страница 7: ...of interest within the spectrum is between 800 and 1800 cm 1 This section of the absorbance plot should maintain a relatively flat line with no consistently repeating peaks Cleaning Mode can be used t...

Страница 8: ...other background must be taken before any spectra can be measured Figure 6 Negative peaks indicating the background was taken when the probe was unclean or not fully purged 1 4 Taking a background FTI...

Страница 9: ...ment 2 1 1 Use at high temperature Figure 7 Probe is heated causing the spectrum to tilt In Figure 7 the spectrum is tilted with positive absorbance at lower wavenumbers and negative absorbance at hig...

Страница 10: ...perform an annual examination of your system s health data remotely to determine if any servicing needs to be carried out This includes review of internal diagnostics for warnings and errors component...

Страница 11: ...rease the probability of fracture Prot gez la fibre des contraintes et des courbures serr es rayon de courbure 30 mm interdit Les courbures serr es provoquent une contrainte la surface du verre et aug...

Страница 12: ...en The pen fits over each of the two male fibre ferrules and is aligned by the transparent cover Push and click once on each ferrule Figure 12 Using the fibre cleaning pen to the Souriau plug Once bot...

Страница 13: ...Page 12 DOC1049R 22 February 2024 12 07 www keit co uk Back to Table of Contents Figure 13 Reconnecting the Souriau connectors Locknut Align keyways...

Страница 14: ...ions can cause damage to the instrument If in doubt please consult with Keit Le stockage du spectrom tre IRmadilloNA non aliment et non purg dans des conditions inad quates peut endommager l instrumen...

Страница 15: ...t force we recommend to tighten the thumbscrew until resistance is felt 1 turn For volatile substances it is recommended to keep the stopper cap in place during use Figure 14 Sample cell fitted to IRm...

Страница 16: ...s is an alternative to installing the IRmadilloNA into a main pipeline It is fixed in place using a tri clamp that locates over the rear of the flow cell and two semi circular collars that fit around...

Страница 17: ...ency Annual 4 2 2 Low flow cell ASM1222 The low flow cell that can be secured to the end of the probe for continuous analysis of your process The flow cell is equipped with two 1 16 NPT fittings to at...

Страница 18: ...ll have not perished They should show no signs of swelling tearing or degradation Also inspects the clamp and C pieces for any signs of degradation cracks or damage If the clamp and or the C pieces sh...

Страница 19: ...r as a bench top instrument for offline sampling Angled at 35 the probe can be positioned into beakers or other vessels for ease of use It can also be configured for two heights to give added flexibil...

Страница 20: ...meter over such that the mounting holes are pointed upward the instrument should be disconnected from power coms and purge to avoid damage to the cables or twisting Position the inclined stand over th...

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