KAM Simple Precision LKF Скачать руководство пользователя страница 20

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KFMANUAL 0317

KAM CONTROLS, INC.

Remove any exterior contamination from Cathode Solution Cell with tissue paper and 

acetone being careful not to damage the platinum wires and screen on the outside of the 

cell.

Fill the Cathode Cell with acetone and stopper the inlet joint. Shake the unit until any dirt 

is removed. This should be repeated several times. Pour out and discard acetone.

Wash the outer surface with acetone.

Pour approximately 5 ml of acid into the Cathode Solution Cell. 

Place the cell in a 50 ml beaker and fill the beaker with acid to the same level as is in the 

cell. Secure the Cathode Solution Cell so that it will not fall over. Allow the cell to remain 

in the solution overnight.

After the cell has stood overnight, discard the nitric acid in the cell, and rinse the inside 

and outside of the cell with running tap water until the yellow color disappears.

Place distilled water in the cell and place it in a 400 ml beaker filed with distilled water.

Place the beaker on a hot plate and bring the water to a slow boil for at least one hour.

Repeat this operation until there is no coloration of the water.

Remove the Cathode Solution Cell from the water and fill it with acetone to overflowing, 

flooding the outside of the cell as well. Shake the cell, dump out the acetone, then refill 

and repeat.

Dry the cell with a forced air dryer. 

NOTE: Do not use compressed air as the increased pressure could damage the compo-

nents.

Place the entire assembly in a laboratory oven and continue to dry it for several hours at 

120º F. 

MAINTENANCE continued

NOTE: The Detector Electrodes can be cleaned in a similar manner if required. 

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Содержание Simple Precision LKF

Страница 1: ...PKF Karl Fischer Moisture Analyzer TEL 1 713 784 0000 FAX 1 713 784 0001 Email Sales KAM com KAM CONTROLS INC 3939 Ann Arbor Drive Houston Texas 77063 USA User Manual KFMANUAL 0317 An ISO 9001 certif...

Страница 2: ...dding reagent 7 Base assembly 8 Setting date and time 9 Reset reagent life 9 Sample size and titration mode 10 Initial titration 10 Running samples 11 moisture content determination Sample dilution 12...

Страница 3: ...e maintenance program By analyzing lube oil on compressors turbines etc the Moisture Analyzer can detect cooling water leaks before they become severe enough to damage equipment Karl Fischer titrimetr...

Страница 4: ...exceeds API MPMS 10 9 ASTM D4928 ISO 12937 and EI 386 Generator electrode config With diaphragm Titration speed 1000 g H2 O min max at high H2 O concentrations Power requirements Operates on either A...

Страница 5: ...ion Cell Assembly Titration Cell Sleeve Power Cord Storage Silica Gel Storage Detector Electrode Wire Cathode Solution Cell Wire Swivel Clamp 3 COMPONENTS FRONT PANEL portable model shown REAR PANEL p...

Страница 6: ...screen Battery Life Indicator blinks when charging USB Indicator BlueTooth Power Cord Charging portable units LCD Display main menu shown Screen Navigation Arrows ENTER Key Karl Fischer Moisture Anal...

Страница 7: ...o not apply pressure to the Electrode Rather let it seat under its own weight Rotate it half a turn backward and forward to ensure the grease is spread evenly and a seal has been created Drop the cera...

Страница 8: ...n Cell Jack black Detector Electrode Jack red Turn the swivel clamp toward back of KF unit and place the entire Generator Solution Cell assembly into the Titration Cell Sleeve Turn Swivel Clamp over t...

Страница 9: ...set time navigate to time indicator and use the UP DOWN arrows to change the hour 24 hour clock and use the RIGHT LEFT arrows to move between fields Press ENTER to save values and return to Main Menu...

Страница 10: ...5 After long periods without use the unit has been turned off and or each time the reagents have been replaced you must run an initial titration to remove any ambient moisture from the reagents and c...

Страница 11: ...m the inside of the syringe The tip of the plunger should exactly align with the sample volume marking Press NEW SAMPLE key on Keypad The display will read Inject Sample and a thirty second countdown...

Страница 12: ...h sample log Data for any individual sample can be retrieved by using the UP DOWN arrows to navigate to the desired sample number and pressing ENTER The display will show the date time water percentag...

Страница 13: ...ill appear Type in the desired name for the output file in the format Filename xls and hit save Example August titrations xls A window will open with all the sample files listed Select all the KFF fil...

Страница 14: ...G WITHTHE OPTIONAL BLUETOOTH PRINTER 1 2 3 4 5 MENU Reagent Life Date Time Saved Samples Language Calibration Version Info English 78 Aug15 98 BT Mode 09 21 BT Mode Modem Printer Scanning for Printer...

Страница 15: ...ueTooth icon will appear at the top of the screen This indicates the devices have been paired successfully To print from the MAIN MENU use the navigation arrows to scroll down to Saved Samples and pre...

Страница 16: ...nother record to the printer while a record is still printing NOTE if at any time the KF unit is turned off you must turn off the printer then follow the steps on page 14 of this manual to reconnect t...

Страница 17: ...on the side of the printer two times in quick succession The printer will shut down Wait until the blue light on the printer stops blinking and turns off Then press the power button once more The pri...

Страница 18: ...om the cell Dispose of fluids according to SDS sheet s Empty contents of Generator Solution Cell by pouring into a suitable container or aspiration Dispose of fluids according to the SDS sheet Thoroug...

Страница 19: ...KF Karl Fischer Moisture Analyzer due to the potential for the other types of grease to absorb moisture and interfere with titration if it is silicon based KAM CONTROLS is not responsible for problems...

Страница 20: ...night discard the nitric acid in the cell and rinse the inside and outside of the cell with running tap water until the yellow color disappears Place distilled water in the cell and place it in a 400...

Страница 21: ...Calibration Verification Check Solution 1 1 ml and 10 l Gastight Syringes 14 and 19 gauge Needles package of rubber Septums 100 Funnels 2 Special Grease 1 and Silica Gel 1 REAGENTS and CONSUMABLES GL...

Страница 22: ...SAMPLE INJECTION PORT P 09044 STIR BAR P 09050 DRYING TUBE P 09029 RUBBER SEPTUM pack of 100 P 09015 SPECIAL GREASE 25 g tube P 370420 REPLACEMENT RECHARGEABLE BATTERY for model 09031 P 370400 POWER...

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