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Page 3 

4.2.4.3

 

VOC (POC) Analysis ......................................................................................................................... 48

 

SECTION 5

 

 INSTALLATION ....................................................................................... 49

 

5.1

 

B

ASIC 

S

YSTEM 

R

EQUIREMENTS

 ........................................................................................ 49

 

5.2

 

U

NPACKING AND 

I

NSTALLATION

 ......................................................................................... 50

 

5.2.1

 

Analyzer Dimensions and Mounting ............................................................................................ 51

 

5.2.2

 

Wiring Power and Signal Terminals ............................................................................................ 53

 

5.2.3

 

Wiring External Power Disconnection Switches .......................................................................... 55

 

5.2.4

 

System Fuse Specifications ........................................................................................................ 57

 

5.3

 

A

IR 

S

UPPLY AND 

R

EAGENT 

C

ONNECTIONS

......................................................................... 58

 

5.3.1

 

Air Supply Connection ................................................................................................................. 59

 

5.3.2

 

Reagent Connections .................................................................................................................. 60

 

5.4

 

S

AMPLE

,

 

D

RAIN AND 

E

XHAUST 

C

ONNECTIONS

 ................................................................... 62

 

5.4.1

 

Sample Inlet Tube Position ......................................................................................................... 62

 

5.4.2

 

Drain and Exhaust Connections .................................................................................................. 64

 

SECTION 6

 

 REAGENTS AND CALIBRATION STANDARDS.................................... 65

 

6.1

 

R

EAGENTS

 ....................................................................................................................... 65

 

6.2

 

C

ALIBRATION 

S

TANDARDS

 ................................................................................................ 66

 

SECTION 7

 

 ANALYZER COMMISSIONING AND STARTUP .................................... 69

 

SECTION 8

 

 MAINTENANCE MENU ........................................................................... 75

 

8.1

 

DIAGNOSTICS

 

MENU .................................................................................................... 76

 

8.1.1

 

Process Test ................................................................................................................................ 77

 

8.1.1.1

 

Pressure Test .................................................................................................................................... 77

 

8.1.1.2

 

Flow Test ........................................................................................................................................... 78

 

8.1.1.3

 

Ozone Test ........................................................................................................................................ 79

 

8.1.1.4

 

Sample Pump Test ............................................................................................................................ 81

 

8.1.1.5

 

pH Test .............................................................................................................................................. 82

 

8.1.2

 

Simulate ....................................................................................................................................... 86

 

8.1.3

 

Signal Simulate............................................................................................................................ 90

 

8.1.4

 

Data Output ................................................................................................................................. 92

 

8.1.4.1

 

Send Reaction Archive ...................................................................................................................... 93

 

8.1.4.2

 

Send Fault Archive ............................................................................................................................ 96

 

8.1.4.3

 

Send Configuration ............................................................................................................................ 96

 

8.1.4.4

 

Send All Data ..................................................................................................................................... 96

 

8.1.5

 

Input/Output Status ..................................................................................................................... 97

 

8.1.6

 

Oxygen Controller Status ............................................................................................................ 98

 

8.1.7

 

Service ......................................................................................................................................... 99

 

8.2

 

COMMISSIONING

 

MENU ............................................................................................ 100

 

8.2.1

 

Reaction Time ........................................................................................................................... 100

 

8.2.2

 

Sample Pump ............................................................................................................................ 101

 

8.2.3

 

Stream Program ........................................................................................................................ 101

 

8.2.4

 

COD/BOD Program ................................................................................................................... 103

 

8.2.5

 

New Reagents Program ............................................................................................................ 103

 

8.2.6

 

Reagents Monitor ...................................................................................................................... 104

 

8.2.7

 

Autocal Program ........................................................................................................................ 105

 

8.2.8

 

4-20mA Program ....................................................................................................................... 105

 

8.2.9

 

Alarm Program .......................................................................................................................... 107

 

8.2.10

 

Data Program ........................................................................................................................ 108

 

8.2.11

 

Information ............................................................................................................................ 108

 

8.3

 

SYSTEM

 

CONFIGURATION

 

MENU ............................................................................. 109

 

8.3.1

 

Analysis Mode ........................................................................................................................... 110

 

8.3.2

 

System Program ........................................................................................................................ 111

 

8.3.3

 

Calibration Data ......................................................................................................................... 116

 

8.3.4

 

Sequence Program ................................................................................................................... 116

 

8.3.4.1

 

Average Program ............................................................................................................................. 116

 

8.3.4.2

 

Zero Program ................................................................................................................................... 117

 

8.3.4.3

 

Span Program .................................................................................................................................. 119

 

8.3.4.4

 

Reagents Purge ............................................................................................................................... 121

 

8.3.4.5

 

Pressure/Flow Test Program ........................................................................................................... 121

 

8.3.5

 

Output Devices .......................................................................................................................... 123

 

Содержание BioTector B3500ul

Страница 1: ...652 BioTector B3500ul Online TOC Analyzer USER MANUAL October 2017 Edition 1 BS5AX 2 11a Original Instructions in English Copyright BioTector 2017 All rights reserved Printed by BioTector Printed in t...

Страница 2: ...MENU DIAGRAM 16 2 1 1 Startup State 18 2 1 2 System Status Messages 18 2 1 3 Analysis Data Screen 19 2 1 4 Analysis Graph Screen 20 2 1 5 Reagent Status Screen 20 2 1 6 Select Level Menu 21 2 1 7 Ent...

Страница 3: ...7 8 1 1 2 Flow Test 78 8 1 1 3 Ozone Test 79 8 1 1 4 Sample Pump Test 81 8 1 1 5 pH Test 82 8 1 2 Simulate 86 8 1 3 Signal Simulate 90 8 1 4 Data Output 92 8 1 4 1 Send Reaction Archive 93 8 1 4 2 Sen...

Страница 4: ...9 TROUBLESHOOTING OF SYSTEM FAULT WARNING AND NOTIFICATION EVENTS 137 9 1 BIOTECTOR FAULT EVENT EXPLANATION AND REMEDIAL ACTION 137 9 2 BIOTECTOR WARNING EVENT EXPLANATION AND REMEDIAL ACTION 141 9 3...

Страница 5: ...be impaired 1 1 Information and Safety Signs used in the Manual When any supplementary information is required and if any hazards exist the necessary information and safety signs Information Caution...

Страница 6: ...sary to work with this component it should be handled with care This symbol when noted on a product illustrates the risk of chemical harm due to its corrosive acidic caustic or solvent nature Only qua...

Страница 7: ...rop ene indicates that The instrument complies with the European product directives health safety and environmental protection legislations Conforms to ANSI UL Std 61010 1 Certified to CAN CSA Std 610...

Страница 8: ...ned herein or for incidental or consequential damages in connection with the furnishing performance or use of this material The information contained in this manual is subject to change without notice...

Страница 9: ...ary oedema may develop with delayed onset usually one or more hours after exposure Following severe acute ozone toxification recovery is slow In the few severe human cases reported 10 14 days of hospi...

Страница 10: ...s g n rales de s curit Pri re d tre toujours attentif toutes les notices de prudence d avertissement ou de danger Le non respect des instructions de s curit peut engendrer la blessure grave d individu...

Страница 11: ...en Isoler les fils lectriques de l appareil avant de commencer tout travail dans le bo tier lectronique Seul le personnel lectricien qualifi est habilit effectuer tous travaux d lectricit Se conformer...

Страница 12: ...t Pour son fonctionnement BioTector emploie de l oxyg ne O2 comme gaz porteur L oxyg ne ne doit comporter aucun gaz carbonique CO2 ni d azote N2 Le taux moyen de consommation d oxyg ne du BioTector es...

Страница 13: ...sing appropriate safety equipment 1 5 3 Pr cautions chimiques La liste de la Section 6 R actifs et Standards de Calibration Section 6 Reagents and Calibration Standards num re un certain nombre de pro...

Страница 14: ...FA Per fluoro alkoxy Vinyl Reinforced Silicon Reinforced PVC Poly vinyl chloride Fittings PFA Per fluoro alkoxy Stainless Steel SS 316 PVDF Poly vinylidene flouride Brass Pump Tubing EMPP Elastomer mo...

Страница 15: ...xy Vinyle Silicone renforc PVC renforc poly chlorure de vinyle Raccords PFA perfluoroalkoxy Acier inoxydable SS 316 PVDF polyfluorure de polyvinylid ne Laiton Tuyauterie de la pompe PPMOD polypropyl n...

Страница 16: ...ramming the BioTector The ENTER key which advances user to the next screen is also used to enter programmed settings in the BioTector The symbols used on BioTector LCD screen and their meanings are as...

Страница 17: ...Page 17 Software Menu Diagram...

Страница 18: ...yed on the top left hand side of the Analysis Data and Reagent Status screens On most other screens only the screen name is displayed in this location System status messages are displayed in the follo...

Страница 19: ...g Range 1 2 or 3 the BioTector is using to carry out its analysis The Reaction Time which is the elapsed time seconds since the analysis start The Reaction Duration which is the overall duration secon...

Страница 20: ...analyzer in C e g 26 C The CO2 instantaneous value e g 56ppm CO2i and the CO2 zero value e g 12ppm CO2z of the reaction The elapsed time e g 265s since the start of the analysis 2 1 5 Reagent Status S...

Страница 21: ...r diagnostics to download data to program the software functions and to program the system specific settings in the BioTector The sub menus in this level can be password protected using the Password m...

Страница 22: ...Standby in the system reaction archive The 4 20mA signal or other output devices are not updated When remote standby signal is deactivated the BioTector starts analyzing When remote standby signal is...

Страница 23: ...eyboard the BioTector stops as soon as its present reaction is completed An is displayed to let the operator know the function has been activated 4 Emergency Stop When this function is activated the B...

Страница 24: ...ls The comprehensive Zero Check Calibration and Span Check Calibration parameters are programmed in Zero Program and Span Program menus respectively see Section 8 3 4 2 Zero Program and 8 3 4 3 Span P...

Страница 25: ...n Check menu 3 If Span Calibration or Span Check is activated in New Reagents Program menu a Span Calibration or Span Check is carried out Once the procedure is completed the BioTector either stops or...

Страница 26: ...cate that this function has been selected If the BioTector is stopped then the Manual mode will start immediately To deactivate this function before the manual operation mode has started press the ENT...

Страница 27: ...ss the ENTER key and to return to the previous screen press the ESCAPE key 2 2 6 Fault Archive Menu In the Fault Archive menu the user can view the last 99 faults warning notification events logged in...

Страница 28: ...startup time for a scheduled task for example the startup time for a manual sample sequence in Manual Program menu 2 2 8 Contact Information Contact Information menu displays the manufacturer distribu...

Страница 29: ...em only checks the zero response at each range and displays the suggested Zero Adjust values in brackets for all ranges next to the current Zero Adjust settings When a Zero Check cycle is completed if...

Страница 30: ...8 Zero Program Zero Program function allows the user to program the number of zero reactions run at one or more ranges R1 R2 and or R3 When the number of zero calibration reactions for one or two of t...

Страница 31: ...ow are displayed in this menu 1 3 TOC Span Adjust This menu item allows the user to set the TOC span adjust factors manually by entering the STANDARD solution used and the calibrated average reaction...

Страница 32: ...Calibration and Span Check reactions are carried out If the selected range is in conflict with the programmed CALIBRATION STANDARD concentration in this menu system automatically displays a Caution R...

Страница 33: ...for TOC Calibration Standard above Section 8 3 4 3 Span Program and Section 6 2 Calibration Standards for further details 21 TC Check Std In VOC systems the sum of the TIC and TOC Check Standard solut...

Страница 34: ...s data on screen in the microcontroller memory and storage of data archive for the lifetime of the analyzer in the SD MMC card Previous 99 fault data on screen in the microcontroller memory and storag...

Страница 35: ...of 35 Maximum impedance 500 ohms Hazardous Area Certification options are available to European Standards ATEX for Zone 2 and to North American Standards Class I Division 1 and Class I Division 2 Othe...

Страница 36: ...let Temperature 2 C 60 C 36 F 140 F Sample Flow Rate Minimum 100ml per sample Sample Particle Size Up to 100 microns Ambient Temperature 5 C 45 C 41 F 113 F Cooling and heating options are available H...

Страница 37: ...1 1 Analysis Enclosure Figure 1 figure 2 and table 2 below shows the typical major analysis enclosure components of BioTector TOC Analyzer Figure 1 BioTector analysis enclosure major components typic...

Страница 38: ...Page 38 Figure 2 BioTector oxygen concentrator enclosure major components 19 20 22 21 23 24 25 26 28 27 30 29 12 16 33 34 13 31 35 32...

Страница 39: ...5 or Multi stream Valve MV6 14 Mixer Reactor 15 Ozone Destructor 16 Sample Valve MV4 17 Liquid Leak Detector 18 Exhaust Valve MV1 19 Fan 20 Oxygen O2 Tank 21 Termination Board 22 Molecular Sieve Bed 2...

Страница 40: ...Page 40 4 1 2 Motherboard Enclosure Figure 3 and table 3 below shows the BioTector motherboard enclosure components Figure 3 BioTector motherboard enclosure components 1 2 3 4...

Страница 41: ...41 Table 3 BioTector motherboard components 1 Motherboard 2 Battery Varta CR2430 Lithium 3V 285mAh ATEX IECEx Zone 1 analyzers Ex i battery 3 Processor Board 4 MMC SD Flash Memory Card Slot and Memory...

Страница 42: ...Organic Carbon POC The TOC result in a VOC system is calculated from the TC and TIC measurements as TC TIC Therefore the TOC result includes the VOC POC content of the sample In other words the TOC re...

Страница 43: ...ribed for TIC TOC systems above but unlike TIC acid first the base reagent e g Sodium Hydroxide is injected into Mixer Reactor Sample Valve and Reactor Valve activates Sample Pump rotates forward and...

Страница 44: ...Page 44 Figure 4 BioTector analysis layout typical TIC TOC system...

Страница 45: ...efinitely The theory behind the operation of the oxygen concentrator is Pressure Swing Adsorption PSA This is based on flowing air through the column the sieve bed packed with molecular sieve material...

Страница 46: ...Page 46 Figure 6 BioTector oxygen concentrator layout...

Страница 47: ...Purgeable Organic Carbon NPOC 6 At the end of the reaction the oxidized sample liquid is discharged from the reactor with increased oxygen flow 4 2 4 2 TC Analysis 1 The oxygen carrier gas flow and t...

Страница 48: ...ector to carry out scheduled TIC TICs analysis and measure TOC which includes NPOC and POC for samples which may contain volatile organic carbon and the TIC concentration of the sample remains constan...

Страница 49: ...d Reagent Requirements Instrument Air Requirements Air Quality 20 C dew point free of water oil and dust To meet or exceed the air quality specification filter pack may be required Air Supply Pressure...

Страница 50: ...e correct sequence Points to note regarding installation The BioTector should be located as close to the sample point as possible Unless it is specified the BioTector has an Ingress Protection rating...

Страница 51: ...ter FRP cabinet This enclosure facilitates easy access to all components and thus eases the service and maintenance procedures Figure 7 and table 4 below gives the dimensions of BioTector enclosure Fi...

Страница 52: ...om the top and the bottom The recommended clear space in the front of the analyzer is 1500mm for easy access to the system When BioTector is being mounted on a wall or a stand the support has to be st...

Страница 53: ...reen earthed to comply with the Electromagnetic Compatibility Directive 2004 108 EC For 4 20mA and any other signal connections only screened instrument cable which comply with the EEC directive shoul...

Страница 54: ...terminated in the phase neutral and earth terminals in the BioTector Cable glands must be used to secure the cables when necessary All electrical sample reagent drain and exhaust connections should b...

Страница 55: ...be located in easily accessible locations with a maximum distance of 2 meters from the BioTector and or the air compressor The switches must be clearly marked for their purpose The switch must comply...

Страница 56: ...BioTector electronics enclosure iii If installed close the air compressor enclosure iv Switch on the external disconnection switches The power off of the BioTector should be carried out by switching...

Страница 57: ...A F5 F 3 15A F 3 15A F6 F 2 50A F 2 50A BioTector Compressor Start Signal Cable N A L 250V Miniature 5x20mm Glass N A T 200mA T 200mA KEY A Amperes DIN German Institute for Standardization Deutsches I...

Страница 58: ...ing stainless steel fittings which were already tightened during reassembly or after service initially tighten the nut up to the point it was tightened previously then tighten slightly more using an a...

Страница 59: ...r Air Compressor The required instrument air supply pressure is 1 5 bars The minimum air supply flow rate is 8 4 m3 hour at 1 5 bar The average air consumption is less than 5 4 m3 hour and typically 3...

Страница 60: ...Please refer to the symbols and codes on the reagent containers Use of 20 or 25 liter containers is recommended for each BioTector reagents Figure 13 below shows the correct setup and connection of Bi...

Страница 61: ...he base reagent getting contaminated If any vent hole is accidentally drilled on the lid of the base container and if the fittings are not connected correctly on the base reagent contamination will oc...

Страница 62: ...pact on the Sample Pump tubing life and may require changes in system configuration settings for the correct operation of the system The point where the sample is taken from should not be pressurized...

Страница 63: ...Page 63...

Страница 64: ...be directed to a well ventilated area as oxygen and other gases may be released during the analysis The drain tubes should be at atmospheric pressure and should not be subjected to any back pressure a...

Страница 65: ...repare TOC analyzer reagents Acid and Base reagents are stable up to 1 year The reagents must be stored in a safe and secure location where the temperature does not drop below 2 C in compliance with t...

Страница 66: ...onized water Potassium Carbonate CK2O3 11 62g 99 0 purity in one liter of deionized water All hygroscopic chemicals in crystal form should be dried in an oven set at 105 C for 3 hours to remove any tr...

Страница 67: ...rity for the preparation of 1000mgC l calibration standard Table 8 Quantity of KHP required to prepare 1000 mgC l standard at various purities Purity of KHP Quantity of KHP grams to prepare 1000 mgC l...

Страница 68: ...two or more steps dilution For example to prepare a 1mgC l standard first prepare a 100mgC l standard by adding 100 grams of the 1000mgC l standard into a one liter flask and by adding enough deioniz...

Страница 69: ...the BioTector Drain the DIW from the PFA tubing into a suitable container and dispose The nuts and ferrules located on these ports will be used for the acid and base connections FMM20 reagent pumps wh...

Страница 70: ...n and Exhaust Connections connect the sample or samples to the BioTector with PFA tube These ports are labeled as SAMPLE 1 and if installed SAMPLE 2 etc _____ If a BioTector SAMPLER has been supplied...

Страница 71: ...ves should be taken throughout these tests Go to Zero Calibration menu and select RUN REAGENTS PURGE function to prime the pumps The factory Reagents Purge settings to prime reagents typically cover 3...

Страница 72: ...gram menu set the required multi stream parameters stream operation sequence number of reactions to run at each stream and operation range for each stream Automatic range change function should not be...

Страница 73: ...cycles on DIW using the Manual Program menu If manual port is not available use the input point for SAMPLE 1 If the BioTector has been in storage for a long period and if the zero readings are not sat...

Страница 74: ...nually See Section 8 1 7 Service for further details If ultra pure water is used during the Zero Calibration ensure that container with at least 5 liters of water is connected to the analyzer It is re...

Страница 75: ...Page 75 Section 8 Maintenance Menu Maintenance Menu Diagram...

Страница 76: ...Page 76 8 1 DIAGNOSTICS MENU This group of menu allows the user to access the Process Test Simulate Data Output Input Output Status and Service menus for diagnostic purposes Diagnostics Menu Diagram...

Страница 77: ...ctivated an will be shown and a small menu will display the following data Time The time for the pressure test is 60 seconds This time shows the time left to the end of the test MFC Setpoint This is t...

Страница 78: ...lockage in the lines then the setpoint should match the flow Status At the end of the test the status below is shown TESTING Test in progress PASS The Exhaust Test finished its cycle with a flow above...

Страница 79: ...ss the stop test menu item Phase 4 There is a purge period that purges any traces of ozone from the ozone tester and the result of the test is shown on the screen Phase 5 The purge of the tester is co...

Страница 80: ...M P L E T E When the o ring breaks immediately select Stop Test and press the ENTER key The ozone generator is now switched off but there will still be traces of ozone in the tester Therefore the Bio...

Страница 81: ...red with the Pump Forward Test below unless all sample lines are at the same length 2 Pump Forward Test This function starts the Sample Pump running in the forward direction When the sample has been c...

Страница 82: ...o ensure that the system is purged and leak tight Phase 3 The TIC acid and sample are added into the reactor mixed and then the program pauses to allow the pH to be tested Phase 4 The base is added to...

Страница 83: ...should have finished normally so that any liquid carried over from that reaction will not affect the pH test Therefore when the start test menu item has been activated a confirmation will be required...

Страница 84: ...moved it is recommended that a few drops of liquid is discharged manually from the reactor by tipping this tubing gently down and then measure the pH of the mixture with a pH paper 5 Continue To Next...

Страница 85: ...ch is the reactor purge phase 6 Stop Test If this is selected the program jumps to the reactor purge phase As the next phase is the reactor purge phase the user is prompted to confirm that all tubes h...

Страница 86: ...devices such as Pumps Valves MFC Mass Flow Controller etc installed and used in BioTector In BioTector when the user enters the Simulate menu as the oxygen gas flow will be required the oxygen genera...

Страница 87: ...programmed pulse time is displayed inside the brackets The pump will stop when the required number of pulses is complete or to manually stop the pump press ENTER select OFF and press ENTER again 5 Ba...

Страница 88: ...nd the valve will be activated To turn the valve off select OFF Note that only one Manual Valve can be switched on at any given time 15 Cooler The Cooler is normally automatically controlled by the sy...

Страница 89: ...state cannot be changed from this menu It only indicates the state of the Sample Sensor 23 Leak Detector if configured in the system This device is input only and therefore its state cannot be changed...

Страница 90: ...5 Output Devices for details To change the state of the device press the ENTER key set the device to ON OFF and press the ENTER key again If the device is on it will be marked with an 8 10 CO2 Alarm...

Страница 91: ...F and press the ENTER key again If the device is on it will be marked with an See Section 8 3 5 Output Devices for details 24 Fault if configured in the system Use this function to test the Fault outp...

Страница 92: ...iguration fault archive reaction archive and system diagnostics information 7 Data Program Data Program is a link to Maintenance Commissioning Data Program menu see Section 8 2 10 Data Program for det...

Страница 93: ...d first when downloading data 2 Number of Events This is the number of events to be downloaded The default is the number of events in the reaction archive which can be edited by the user 3 Start Sendi...

Страница 94: ...The calibrated TOC value in gC l TOC represents NPOC CO2p The height of the TOC CO2 peak COD BOD gc The calculated COD and or BOD value in gO l if activated in COD BOD Program menu BT_DegC BioTector...

Страница 95: ...sius C Atm Atmospheric pressure in kPa SAMPLE Sample quality from Sample Sensor signal which is used to activate SAMPLE STATUS output SMPL PUMP The five items which are number coded or a number data g...

Страница 96: ...g of data Press again to continue downloading Note If the downloading is interrupted for more than 60 seconds then the downloading is automatically resumed 3 Stop Sending Press the ENTER key to stop d...

Страница 97: ...and rows with their code logical states and function Each output name is composed of the DO prefix and two decimal index which identifies the output For instance the digital output named DO34 is digi...

Страница 98: ...ressure for the oxygen concentrator The pressure mbar and the voltage V readings as obtained from the Air Pressure Sensor are displayed in real time 6 O2 Pressure Sensor This menu item displays the ox...

Страница 99: ...lt values and automatically adjusts the zero offset values to compensate for the removal of the contamination It will therefore not be necessary to revisit the BioTector after the service or to repeat...

Страница 100: ...is not necessary The longest interval time which can be programmed is 1440 minutes or 1 day A programmed interval time would reduce the reagent usage significantly When BioTector automatically extend...

Страница 101: ...le time is determined by the system from the System Program 1 settings in System Program menu 8 2 3 Stream Program SAMPLER NO If a sampler is used with the BioTector SAMPLER is programmed YES When act...

Страница 102: ...y carry out TC TIC NPOC analysis at a variable frequency based on the programmable TC CHECK STREAM 1 3 concentration bands allows the measurement of multiple parameters of the sample without a signifi...

Страница 103: ...obtained following the procedures described in information sheet I030 TOC to COD or BOD Correlation Method which is available in the MMC SD card shipped with the BioTector Stream 1 factor is used for...

Страница 104: ...ecifically programmed for warning events LOW REAGENTS AT 20 DAYS LOW REAGENTS AT specifies the number of days 20 days by default before the system generates an 85_LOW REAGENTS warning or notification...

Страница 105: ...so sent to the 4 20mA channels programmed as STREAM 1 In STREAM MUX and FULL MUX modes specific channels are dedicated to periodically change their value in steps to indicate the stream number and res...

Страница 106: ...value For instance if the OUTPUT value is set as 100 100 of the negative result is sent as 4 20mA signal If the setting is 50 50 of the negative results is sent as 4 20mA signal When the setting is 0...

Страница 107: ...programmed level for a specific stream By default this function is disabled by 0 0ppm setting If programmed it provides an earlier warning of an unusually high TOC result from the rising slope of the...

Страница 108: ...nd of each reaction FAULT ON LINE YES FAULT ON LINE enables YES by default or disables NO the automatic printout of a fault or warning log as soon as it occurs CONTROL CHARS NO CONTROL CHARS enables Y...

Страница 109: ...NFIGURATION MENU System Configuration menus are used to configure the system in the factory The user should avoid any modifications in these menu settings unless it is absolutely necessary System Conf...

Страница 110: ...cribed in information sheet M067 BioTector Arm Configuration Upgrade Procedure which is available in the MMC SD card shipped with the BioTector When the procedures are followed the system configuratio...

Страница 111: ...requires recalibration of the system DELAY 1s 1 l h DELAY is the time 1 second by default the carrier gas is activated to inject the reagents into the Mixer Reactor with a flow of 1 l h by default SAM...

Страница 112: ...the PRESSURE CHECK FAULT level which is 6 0 l h defined in Sequence Program Pressure Flow Test Program menu for longer than 1 second during the PRESSURE CHECK phase above BioTector opens the Reactor...

Страница 113: ...me extension time until the TC level drops below 25ppm level A 91_TC OVERFLOW warning is generated if the TC level does not drop below 25ppm at the end of the maximum extension time which is 300 secon...

Страница 114: ...1 is typically 20 less of the top concentration point of TOC RANGE 1 in System Range Data menu by default SAMPLE IN 5p P V SAMPLE IN identifies the amount of sample in pulses to be injected into the r...

Страница 115: ...gC l RANGE CHANGE 3 1 defines the concentration level for the BioTector to change its range automatically from range 3 to range 1 The RANGE CHANGE 3 1 is typically 20 less of the top concentration poi...

Страница 116: ...enus are used to install the calibration data and thus to calibrate the BioTector in factory TOC CALIBRATION 1 2 and 3 shows the calibration curves for range 1 2 and 3 respectively In TC and VOC syste...

Страница 117: ...C TC readings obtained during the Zero Calibration or Zero Check reactions System initially runs the minimum number of reactions and calculates the average value at a specific programmed range If the...

Страница 118: ...of the Mixer Reactor pH ADJUST TIME 60s pH ADJUST TIME determines the mixing time 60 seconds by default the Mixer Reactor operates for the pH neutralization of the reactor SERVICE ZERO 20 5 SERVICE Z...

Страница 119: ...sed in Span Calibration reactions If TOC CALIBRATION STANDARD is programmed as 0 0 gC l system ignores the Span Calibration results and omits any related warnings defined in TOC BAND below TOC CHECK S...

Страница 120: ...reaction results for TOC In TC and VOC systems this function is named as TC BAND If the average span result is outside the tolerance limits a 30_TOC TC SPAN CAL FAIL or 33_TOC TC SPAN CHCK FAIL warnin...

Страница 121: ...FAULT flow level 6 0 l h by default the pressure test passes If the flow is greater than programmed PRESSURE TEST FAULT setting the pressure test fails and BioTector generates a 05_PRESSURE TEST FAIL...

Страница 122: ...flow test fails and BioTector generates a 22_FLOW WARNING EX or 23_FLOW WARNING SO in the fault archive and continues to run This warning is logged in the fault archive In TC TIC systems BioTector gen...

Страница 123: ...PF SAMPLER OUTPUT 1 6 OUTPUT 1 6 menus typically contain internal output settings related to system operation These relay outputs located on the Motherboard are system optional features STREAM 1 is al...

Страница 124: ...as 20 C by default CAL Calibration Valve used during span calibration check reactions ZERO CAL Calibration Valve used during zero calibration check reactions CAL SIGNAL Output set to operate on Zero S...

Страница 125: ...ith an asterisk sign in these menus as in the example for POWER BOARD OUTPUT 2 which is programmed for STOP FAULT WARNING and NOTE signals below In the example below POWER BOARD OUTPUT 2 is activated...

Страница 126: ...the type WARNING or FAULT of the 04_REACTION ERROR fault When 04_REACTION ERROR fault occurs if FAULT TYPE is programmed as WARNING by default BioTector keeps running If it is programmed as FAULT BioT...

Страница 127: ...d variation and the second parameter 0 025 defines the absolute variation in gC l If the reaction result is outside the specified bands TOC INTEGRATION LIMITS then the reaction result averaging is omi...

Страница 128: ...of 400ppm CO2 level in the environment will increase the CO2 ZERO LINE level to 250ppm within 24 days of online operation or approximately after 5000 analysis cycles CO2 ZERO ALARM 250ppm If the conce...

Страница 129: ...d value i e when there is significant quantity of air bubbles in the stream manual grab sample lines Sample Status output is set reset as soon as the Sample Sensor signal is processed Sample Status ho...

Страница 130: ...by default for longer than 5 seconds BioTector generates a 108_COOLER FAN FAULT warning When COOLER FAN ALARM voltage is set to 0 0 Volt then the Cooler Fan Fault generation is switched off SIGMATAX F...

Страница 131: ...sampled at every 2 second intervals covering 240 seconds If a fault is detected the events are stored in the CO2 ANALYZER FAULT archive and are retained even if the fault is accepted in Fault Archive...

Страница 132: ...CO2 peaks on screen exceeds the scale of the graph the CO2 analyzer keeps measuring and integrating the CO2 readings to obtain the TOC result without losing any CO2 data BAUDRATE 9600 BAUDRATE 9600bps...

Страница 133: ...the cooler temperature calibration curve which is linear When Cooler operates with PULSE WIDTH MODULATION at 50 the Cooler temperature is typically 14 C below ambient temperature which is 25 50 PWM SL...

Страница 134: ...ammed as MAN above in MANUAL PURGE CYCLE setting the first parameter 2000 by default defines the number of analysis cycles the Ozone Destructor and the BioTector Cooler operates as normal The second p...

Страница 135: ...factory configuration with the name syscnfg bin in binary format When any modification is carried out in system configuration LOAD CONFIG FROM MMC SD CARD function can be used and the user can revert...

Страница 136: ...disabled The higher level passwords can be used to access password protected lower levels For instance the DIAGNOSTICS password can be used for access the OPERATION level The SYSTEM CONFIGURATION pass...

Страница 137: ...s 92 94 96 98 HI LO AIR O2 PRESSURE Various for example air and oxygen supply problem Check oxygen pressure looking at the Oxygen Controller Status O2 CTRL STATUS menu It should be 400mbar 10mbar at 2...

Страница 138: ...em fittings Check Mixer Reactor Run Pressure Test see Section 8 1 1 1 Pressure Test for details 06_PRESSURE CHCK FAIL MFC flow did not drop below the PRESSURE CHCK FAULT level during the pressure chec...

Страница 139: ...pumps Rectify the leak 20_NO REAGENTS can also be programmed as a warning or notification condition BioTector has calculated that the reagent containers should be empty Change reagents and reset reage...

Страница 140: ...menu 8 3 4 5 Pressure Flow Test Program Various for example air and oxygen supply problem Check oxygen pressure looking at the Oxygen Controller Status O2 CTRL STATUS menu It should be 400mbar 10mbar...

Страница 141: ...through Reactor Valve MV3 has dropped below the FLOW WARNING level defined in Pressure Flow Test Program menu 8 3 4 5 Pressure Flow Test Program during the Pressure Flow Test cycle Various for example...

Страница 142: ...ctor 42_ZERO CAL FAIL Zero Calibration result is outside the specified ZERO BAND defined in Zero Program menu See Section 8 3 4 2 Zero Program for details Check the stability of the zero reactions and...

Страница 143: ...ressure sensor Replace the motherboard 82_ATM PRESSURE LOW System atmospheric pressure sensor reading is below 60kPa Therefore the sensor reading is defaulted to 101 3kPa fault operation mode Check AD...

Страница 144: ...sure to 1 5 bar when the oxygen concentrator is not running When the problem is rectified acknowledge the warning by pressing the ENTER key in the Fault Archive menu to reset the O2 Controller Board 9...

Страница 145: ...by pressing the ENTER key in the Fault Archive menu to reset the O2 Controller Board 97_HI O2 PRESSURE 1 Oxygen pressure supply has been more than 450 mbar for longer than 60 seconds Reduce oxygen pr...

Страница 146: ...1 on and 0 off in the Oxygen Controller Status menu as the valve rotates Replace the valve When the warning is cleared the green LED labeled as Stepper on the Oxygen Controller Board should be on 102_...

Страница 147: ...ach analysis cycle When system temperature drops below 48 C for longer than 2 minutes BioTector continues normal operation Check the filters in the fan and vent Check the operation of the fan Note tha...

Страница 148: ...osed to direct sun light If the problem is not related to above contact the distributor or the manufacturer 114_I O WARNING System has detected changes in the Input Output bus extender chips which hav...

Страница 149: ...actor Purge Band defined in Pressure Flow Test Program menu 8 3 4 5 Pressure Flow Test Program Various for example partially blocked reactor Faulty blocked Reactor Valve and or Sample Valve Partially...

Страница 150: ...CE TIME RESET This message is logged into the fault archives when RESET SERVICE COUNTER function is selected in Diagnostics Service menu Automatically acknowledged notification No action is required 1...

Страница 151: ...nturi Sampler is operating Option 2 Confirm that the Sample Catch Pot has sufficient sample flow which guarantees a fresh sample for each analysis cycle Option 3 Confirm that the Sample Pipe has suffi...

Страница 152: ...such as wearing eye protection and gloves throughout the service If the reagents lines do not fill with DIW during the Reagents Purge cycle raise the DIW container above the height of the BioTector g...

Страница 153: ...Replace the 100mm filter mats in fan and vent housing see item C4 in the service kit _____ Check the operation of the fan Note that at temperatures below 25 C BioTector automatically switches the fan...

Страница 154: ...th additional turns Confirm that the sealing face at the back of the reactor where the diaphragm sits is clean Install the reactor motor back onto the Mixer Reactor and tighten each bolt by engaging t...

Страница 155: ...using ultra pure water go to Maintenance System Configuration Sequence Program Zero Program and set ZERO WATER to YES See ZERO WATER in section 8 3 4 2 Zero Program for details _____ Program the conc...

Страница 156: ...tra pure water is used during the Zero Calibration ensure that container with at least 5 liters of water is connected to the analyzer It is recommended to use a sealed container with CO2 absorber and...

Страница 157: ...Page 157 Section 11 System Replacement and Spare Parts...

Страница 158: ...Mainboard with Ex i Battery for IECEx ATEX Zone 1 systems 20 B5C 013 B5C PSU Module 20 PCB 036 B5C Oxygen Controller Board 20 PCB 038 B5C Termination Board 19 MAX 008 B5C Sample Pump 20 B5C 019 B5C Ac...

Страница 159: ...inch Valve C O 20 B5C 011 B5C Oxygen Concentrator Rotary Valve 19 CO2 010 UltraLow System C CO2 Analyzer 20 B5C 025 B5C Ozone Generator Module 19 PCB 034 B5C Ozone Board 10 SMC 001 B5C Instrument Air...

Страница 160: ...he manufacturer s specified lifetimes Agreed Applications It is important that the Pre Installation Questionnaire be filled in for each new application as the manufacturer cannot guarantee the BioTect...

Страница 161: ...TFE Chloro tri fluoro ethylene DegC Degrees Celsius C DIAG Diagnostics DIN German Institute for Standardization Deutsches Institut f r Normung e V DIW Deionized Water EMPP Elastomer modified poly prop...

Страница 162: ...PVDF Poly vinylidene flouride RARCH Reaction Archive RS Remote standby reaction RW Reactor wash reaction S Span S1 S3 Stream 1 3 SC Span calibration SK Span check SM Manually input span adjust SMPL Sa...

Страница 163: ...Page 163 W Watts Z Zero ZC Zero calibration ZK Zero check ZM Manually input zero adjust ZS Zero and Span...

Страница 164: ...ach lange gr www hach lange gr Repair Service in Canada Hach Sales Service Canada Ltd 1313 Border Street Unit 34 Winnipeg Manitoba R3H 0X4 Tel 800 665 7635 Canada only Tel 204 632 5598 Fax 204 694 513...

Страница 165: ...Page 165 HACH LANGE MAROC SARLAU Villa 14 Rue 2 Casa Plaisance Quartier Racine Extension MA Casablanca 20000 T l 212 0 522 97 95 75 Fax 212 0 522 36 89 34 info maroc hach lange com www hach lange ma...

Страница 166: ...DOC012 97 80506 User Guidance for EMC Class A Equipment EMC A A A...

Страница 167: ...years The product manufacturing date can be found on the product label on the main board enclosure behind the display BioTector 25 EFUP CHINA ROHS DECLARATION TABLE ROHS Part name Toxic or Hazardous...

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