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Stirring Fluid Loss Manual

100031980

Revision F

11

3

Features and Specifications

The Stirring Fluid Loss Test Assembly is equipped with a stirrer to simulate
circulation and a heating jacket to simulate the bottomhole circulating temperature
(BHCT). The pressure differential between annular and formation pressure is
simulated by pressurized nitrogen. A 325 micron mesh screen (or a porous core) and
a filtration chamber simulate the permeable zone. A control panel allows precise
setting and controlling of the temperature and pressure.

Operators use this instrument to perform standard tests outlined in the American
Petroleum Institute (API) Recommended Practice (RP) for Testing Well Cements,
API RP 10B-2.

The instrument is shown in Figure 3-1 with labels identifying its components. Refer
to Table 3-1 for the instrument specifications. The following sections describe its
features in detail.

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Содержание 210194

Страница 1: ...Fann Instrument Company Stirring Fluid Loss Manual Manual 100031980 Revision F Instrument No 210194...

Страница 2: ...red by U S Patents Fann Instrument Company reserves the right to make improvements in design construction and appearance of our products without prior notice FANN and the FANN logo are registered trad...

Страница 3: ...trument 20 5 2 Load the Sample Chamber 22 5 3 Preheat the Sample Chamber 23 5 4 Start the Stirring Fluid Loss Test 25 5 5 End the Stirring Fluid Loss Test 26 5 6 Disassemble and Clean Equipment 28 5 7...

Страница 4: ...Stirring Fluid Loss Manual 100031980 Revision F 4 9 Warranty and Returns 56 9 1 Warranty 56 9 2 Returns 56...

Страница 5: ...23 Figure 5 4 Thermocouple inserted in sample cell 24 Figure 5 5 Filtrate Unit connected to the Sample Chamber 25 Figure 5 6 Coolant Valve open for water flow 26 Figure 5 7 Coolant Valve in off positi...

Страница 6: ...trical Diagram 50 60 Hz 100052157 Rev Q 40 Table 8 3 Mainframe Assembly 50 60 Hz 100052153 Rev G 43 Table 8 4 Heating Jacket Assembly P N 100052154 Revision G 46 Table 8 5 Chamber Assembly 100020388 R...

Страница 7: ...ss during cementing operations the cement job will be more successful Adding various chemicals to a cement slurry will minimize fluid loss If fluid is lost then cement viscosity and hydration rate wil...

Страница 8: ...le consequences MANDATORY ACTION Gives directions that if not observed could result in loss of data or in damage to equipment WARNING Describes an unsafe condition or practice that if not corrected co...

Страница 9: ...id Loss Test Assembly uses nitrogen gas to pressurize and compressed air to cool Nitrogen must be supplied in an approved nitrogen gas cylinder or the nitrogen supply system must be built into the lab...

Страница 10: ...ontroller does not reliably maintain temperature then electrical repair may be required Refer to Section 7 Troubleshooting and Maintenance Always disconnect the power cable before attempting any repai...

Страница 11: ...itrogen A 325 micron mesh screen or a porous core and a filtration chamber simulate the permeable zone A control panel allows precise setting and controlling of the temperature and pressure Operators...

Страница 12: ...ing Fluid Loss Assembly Heating Jacket Pressure Gauges 2 Master Power Switch Timer Timer Switch Temperature Controller Stirrer Motor Switch Heater Switch Nitrogen Valves 2 Pressure Regulator Coolant V...

Страница 13: ...0 x 59 7 cm Weight 283 lb 128 kg Pressure Connection Nitrogen 1 8 Female NPT Air Inlet Connection 1 4 Female NPT Water Inlet Drain Connections 1 4 Female NPT Voltage and Current 50 60 Hz 230 VAC 9A 3...

Страница 14: ...chamber filtrate unit attaches to the cell cap Fluid flows through a 325 mesh screen that is on the cap and through the filtrate unit where it is cooled The screen and filtrate chamber simulate a per...

Страница 15: ...ill indicate that the slurry has an extremely low fluid loss when it may actually be high When the back pressure receiver is used the filtrate never goes to steam Instead pressure is maintained on the...

Страница 16: ...mperature rise ramp and the final set point temperature of the test slurry See Section 5 for complete operating instructions A Type J thermocouple must be used to measure the temperature Motor Switch...

Страница 17: ...pressure in the chamber Nitrogen Supply Valve N2 Supply is the main nitrogen supply valve for the complete gas pressure system The gauge registers incoming nitrogen pressure from the supply valve Nit...

Страница 18: ...Stirring Fluid Loss Manual 100031980 Revision F 18 o Air Cool for air flow arrow points to the left o Off to shut off arrow points up...

Страница 19: ...uld be given to the location of the sample preparation area and cleaning the cells following test completion The pressurizing system may also dictate installation specific requirements such as having...

Страница 20: ...ting and Maintenance for servicing if required 5 Screw paddle cap assembly in one end of the sample chamber and hand tighten Paddle cap assembly should be as nearly flush as possible with chamber end...

Страница 21: ...s well seated against spacer ring 18 Insert the filter screen with fine mesh side facing down 19 Insert a second O ring slightly greased on top of the screen 20 Screw cell cap onto the reservoir end I...

Страница 22: ...the slurry sample down the side of sample chamber to avoid getting slurry on top of paddle or down the paddle shaft Fill only to top blade not to the top of paddle This volume is approximately 320 mL...

Страница 23: ...heating jacket will be hot The fluid loss reservoir assembly constitutes a pressure vessel The safety precautions listed in Section 2 1 should be followed to assure safe operation Do not exceed 1500...

Страница 24: ...ress the Scroll until Target Set Point Use to change it if needed Press Page button many times until out of the menu Press the to bring to Auto mode and then to run the program The symbols will appear...

Страница 25: ...ring motor 4 Disconnect flexible shaft stirring cable from paddle cap assembly 5 Pull the red knob to unlock the heating jacket and rotate the jacket 180 degrees upside down 6 Push the red knob to loc...

Страница 26: ...te completely blow out in less than 30 minutes you will hear a hissing sound gas released Record the time 12 Record the time 30 minutes maximum and end the test 13 If the slurry has not dehydrated aft...

Страница 27: ...ve slowly to flow water through the heating jacket cooling coils This method allows faster cooling of the jacket and sample chamber 7 When the temperature indicates approximate room temperature rotate...

Страница 28: ...ipment 1 When pressure is completely released back off the knob on the hold down plate and remove the cylinder from the heating unit 2 Remove the paddle assembly end plate o rings screen and brass rin...

Страница 29: ...curs there 10 Repeat the pressure test and check for leaks 11 If the pressure test fails again then disassemble and replace the packing in the stirring end 12 If the pressure test passes then remove t...

Страница 30: ...presence of multiple additives in the slurry can considerably increase test result variations When one person performs the test on one instrument or when the fluid loss value is low the variation usua...

Страница 31: ...through in less than 30 minutes record the filtrate volume collected and time at which the blow through occurs Calculate the API Fluid Loss by the formula t 5 477 Qt 2 Loss Fluid API Calculated where...

Страница 32: ...auge 10 psi at 1000 psi 1 year Inspect visually before each test for plugging or tears 7 2 Packing Replacement 1 Remove the paddle from assembly 2 Hold drive tang and unscrew paddle turning it counter...

Страница 33: ...the temperature controller set point to 150o F 65 5o C Do NOT turn on the heater switch Feel the outside of the heating jacket for an increase in temperature It should remain cold 5 Turn the heater s...

Страница 34: ...nitrogen bottle and adjust the bottle regulator to 1 500 psi 5 Remove the console s rear panel Bleed off pressure before tightening fittings by turning off the bottle and opening the nitrogen vent va...

Страница 35: ...the heating jacket 5 Connect the filtrate unit to the sample chamber Hand tighten only 6 Connect the cooling lines to the filtrate unit 7 Slowly open the coolant valve by turning the handle to the rig...

Страница 36: ...llar The motor is bad Check or replace the motor The system does not heat up but the heater indicator in the temperature controller is on The heater control switch is turned off Turn the heater contro...

Страница 37: ...37 Problem or Symptom Possible Cause Corrective Action The temperature reading is about room temperature and the chamber is hot Possible short circuit in thermocouple or thermocouple cable Look for an...

Страница 38: ...part numbers Table 8 1 Stirring Fluid Loss Assembly 50 60 Hz P N 210194 Revision F Item No Part No Quantity Description 0002 100052157 1 ELECTRICAL INSTRUMENT 50 60Hz 0003 100052153 1 MAINFRAME ASSEM...

Страница 39: ...Stirring Fluid Loss Manual 100031980 Revision F 39 Figure 8 1 Stirring Fluid Loss Assembly...

Страница 40: ...E 0021 100027804 1 RESISTOR 100000 OHM 1 WATT 0022 349301 4 TERMINAL FEMALE 0023 101482068 1 TIMER ELAPSED INDICATOR 0024 208547 3 WIRE 22AWG TEFLON STRANDED BLACK 0025 208549 3 WIRE 22 AWG TEFLON STR...

Страница 41: ...SS STEEL 0160 204294 3 TIE WRAP 1 16 IN TO 2 IN DIAMETER 0170 207626 4 NUT 1 4 20 HEX REGULAR STAINLESS STEEL 0180 207753 4 WASHER SPLIT 1 4 STAINLESS STEEL 0190 208487 6 TERMINAL STRIP JUMPER 0200 20...

Страница 42: ...Stirring Fluid Loss Manual 100031980 Revision F 42 Figure 8 2 Electrical Diagram 278 00267 Rev N...

Страница 43: ...ATION 0020 100027311 2 PIN ROLL 59 022 094 0437 3 32 X 7 16 0021 100029075 1 SCREW BIND HEAD 10 32 NF X 1 STAINLESS STEEL 0022 100026443 1 NUT ELASTIC STOP 10 32 NF 0023 100025893 1 KNOB BALL DARK RED...

Страница 44: ...Stirring Fluid Loss Manual 100031980 Revision F 44 Figure 8 3 Mainframe Assembly Front View...

Страница 45: ...Stirring Fluid Loss Manual 100031980 Revision F 45 Figure 8 4 Mainframe Assembly Rear View...

Страница 46: ...28441 4 SCREW HEX CAP 5 16 18 NC X 1 1 4 0019 100028799 2 SCREW SET 8 32 NC X 1 2 CUP PORT HEX SOCKET 0020 100028439 4 SCREW HEX CAP 5 16 18 NC X 1 0021 100020379 2 SADDLE SUPPORT HEATING JACKET 0022...

Страница 47: ...Stirring Fluid Loss Manual 100031980 Revision F 47 Figure 8 5 Heating Jacket Assembly Schematic Part 1 of 2...

Страница 48: ...Stirring Fluid Loss Manual 100031980 Revision F 48 Figure 8 6 Heating Jacket Assembly Schematic Part 2 of 2...

Страница 49: ...SSEMBLY 9 102990296 1 O RING 112 VITON 0 487 ID X 0 103 W 10 102365275 3 O RING 228 VITON 2 234 ID X 0 139 W 11 100020383 1 SP CHMBR ASSY 12 100020384 1 PDDL CHMBR ASSY SPCL 13 100020385 1 CHMBR STIRR...

Страница 50: ...Stirring Fluid Loss Manual 100031980 Revision F 50 Figure 8 7 Chamber Assembly...

Страница 51: ...0 2000 PSI 0010 100032364 2 VALVE SHUT OFF BRASS 0011 100032362 1 GAUGE PRESSURE DUAL SCALE 4 INCH 0 5000 PSI 0012 100072597 1 FEMALE HALF HAND UNION TWO CUBE CEMENT 0013 100032371 1 FITTING TUBE CONN...

Страница 52: ...Stirring Fluid Loss Manual 100031980 Revision F 52 Figure 8 8 Manifold System Water Nitrogen...

Страница 53: ...e 8 7 Tool Kit Instruction Manual P N 100052158 Revision C Item No Part No Quantity Description 0001 10003198 1 INSTRUCTION MANUAL 0002 100020361 1 WRENCH ASSEMBLY 0003 100029847 1 VISE GRIP CHAIN CLA...

Страница 54: ...4 100033636 1 ELBOW FITTING TUBE SWAGELOK 90 DEG 1 8 TUBE X 1 8 MPT BRASS 0005 100001930 1 O RING 90 DURO 2 11 16 X 2 1 2 X 3 32 568 144 0006 100016378 2 ELBOW 90 DEG STREET 1 8 B2SE 0007 100072596 1...

Страница 55: ...COIL 0004 100000593 1 VALVE PLUG 1 8 MNPT BRASS 3000 PSI 250 F BUNA N SEALS 0005 100001934 1 O RING 90 DURO 1 5 8 X 1 7 16 X 3 32 568 127 0006 100072597 2 FEMALE HALF HAND UNION TWO CUBE CEMENT AUTOC...

Страница 56: ...nt enclosed with the product 9 2 Returns For your protection items being returned must be carefully packed to prevent damage in shipment and insured against possible damage or loss Fann will not be re...

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