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17.6. Density of solids and liquids 

 
In additional equipment of analytical balance there are Specific Gravity Measurement Kit.   
 

 

 
Draw. 47. Specific Gravity Measurement Kit

 

 

Components of the kit: 

 

1 Beaker 

stand 

2 Pan 

stand 

3 Float 

 

4 Beaker 

 

5 Termometer 

clamp 

6 Termometer 

 

7 String 

8 Float 

hook 

9 Top 

pan 

10 String 

11 Bottom 

pan 

 

12 Attachments 

 
 

 

Содержание CX 165

Страница 1: ...Instruction number LMI 17 02 05 09 ENG C Analytical balances CX series...

Страница 2: ...2 MAY 2009...

Страница 3: ...22 8 1 Automatic balance calibration 23 8 2 Calibration test 25 8 3 Manual calibration 25 8 4 Calibration report printout 27 9 SETTING PRINTOUTS FOR GLP PROCEDURES 28 10 SETTING TIME AND DATE 28 11 S...

Страница 4: ...RINTOUTS 60 18 1 Standard printout 60 18 2 Non standard printout 62 19 COOPERATION WITH PRINTER OR COMPUTER 67 19 1 Connections 68 20 COOPERATION WITH LABEL PRINTERS CITIZEN CLP 521 69 21 COOPERATION...

Страница 5: ...ture 10 50 C Power supply adaptor 230V 50Hz AC 11V AC Calibration internal automatic Display graphic with backlight Max ambient humidity 80 Min ambient humidity 35 when any problems with electrostatic...

Страница 6: ...the centering ring 1 close side doors of weighing chamber turn on balance supply pin of power adaptor should be connected to socket in the back of balance casing The balance with 100 mm pan open side...

Страница 7: ...Set the balance on stable table far from vibrations The balance should be replaced far from draughts and air breeze The balance should be in stable temperature and humidity room The balance should be...

Страница 8: ...hich ware in surrounding temperature work before start weighing If the analytical balances are kept in lower temperature for example in winter time before weighing the warming up time is about 8 hours...

Страница 9: ...balance to individual needs and access functions and units which are necessary at this moment It is possible to define accessible or no accessible in user menu and it is described in further part of...

Страница 10: ...ing off other subcomponents are supplied and the balance is in stand by mode Function key F fast enter into work mode Key MODE selects the work mode UNITS key changes measure units PRINT ENTER key sen...

Страница 11: ...r function 02 Ext calibr function 03 User calibr function 04 Calibr test function 05 Weight corr 0 0 06 Auto calibr 0 3 both 07 Auto cal time 0 3 3 hours 08 Print report 0 1 on P2 GLP 01 User Nowak Ja...

Страница 12: ...rinter type 0 Epson Standard 11 Cut paper 0 no P6 Printout 01 Printout no 0 standard 02 Printout 1 start 1 03 Printout 1 stop 1 04 Printout 2 start 1 05 Printout 2 stop 1 0 10 Pr edit function 11 Text...

Страница 13: ...bled 08 Temperature function 09 Balance number 114493 10 Software number MBa a 35 11 Par printout function 12 Par receive function 13 Password protection function Parameters in user menu are functiona...

Страница 14: ...ion selection 3 function name 4 currently used function 5 submenu number 6 submenu name 7 attribute of the menu 8 value of the attribute 6 1 Move in user menu User moves in the menu by the balance key...

Страница 15: ...is presented on the display move one level up to main menu Resignation parameter changing 6 1 2 Return to weighing function Introduced changes are recorded after return to weighing mode and confirm c...

Страница 16: ...d has its equvivalent on the PS keyboard for functions Description keyboard Switch on off the balance display Move to the balance menu Selects work mode Selects measure unit PRINT TARE for Direktion k...

Страница 17: ...nce manu and control the balance work The list of the commands is at the end of the manual 6 2 User menu The menu is presented in p 5 Press the Setup key in weighing level Main menu is presented on th...

Страница 18: ...ce with p 7 1 Before measurements load the pan and check if the balance show precise zero displayed in down left corner of the display only if the parameter P4 06 Autozero has the value 1 yes and chec...

Страница 19: ...er software PIPETTES user can calibrate pipettes pipettes calibration stand Function is described in further part of manual Independently on pipettes calibration for this function steam protection rin...

Страница 20: ...One user who is authorised to sets and the balance functions determined by administrator Setting password and access authorization After set the password and access parameters parameter P9 13 Passwor...

Страница 21: ...ly Kal GLP If it is set up on YES user can perform the calibration and calibration report Stars If it is settled on YES during start the balance up password is hidden under starts Administrator passwo...

Страница 22: ...re inside the balance changes more than 0 8 C Kind of calibration Internal automatic calibration started if temperature changes started if the time changes Internal manual calibration started by the b...

Страница 23: ...ntill the measurements are performed If the T O key is pressed the calibration process is stopped Set up automatic calibration Draw 12 Set up automatic balance calibration 1 main menu number 2 functio...

Страница 24: ...value of internal calibration mass function inadmissible in verified balances 06 Automatic calibration determine factor which decides about start automatic internal calibration 0 non non of the factor...

Страница 25: ...ESC cancel see drawing 6 Return to weighing p 6 1 2 Return to weighing 8 3 Manual calibration 8 3 1 Internal calibration 1 Enter submenu P1 Calibration 2 Select the function 01 Internal calibration 3...

Страница 26: ...P1 Calibration 8 Return to weighing as in the point 6 1 2 If the function DRH is active user cannot perform the external calibration process Function DRH is active in verified balances 8 3 3 Calibrat...

Страница 27: ...e external calibration process 8 4 Calibration report printout After calibration user can receive the calibration report The report can be printed on connected printer and sent to computer or recorded...

Страница 28: ...group of the parameters which declares factors on the calibration printout For fields user max 8 alphanumerical signs design max 8 alphanumerical signs introduce names by the balance keyboard or the P...

Страница 29: ...selection proper value confirm by the ENTER key 02 Time form There are two possibilities 1 time form 12 h 0 time form 24 h After selection press the ENTER to confirm 12 h form is distinguished by the...

Страница 30: ...st change digit stops flashing Repeat above activities for following values After setting new values for time press the ENTER key The balance returns to submenu P3 Date Time and displayed time changes...

Страница 31: ...ate For the value 1 YES date is displayed on top graph for the value 0 NO date is not displayed Return to weighing see Draw 6 6 1 2 Return to weighing 11 SETTING THE PARAMETERS User can adjust the bal...

Страница 32: ...indirect not stable mass indications are not presented on the display during putting on and taking off the load For low values all changes in mass during weighing are visible it enables to dosage liq...

Страница 33: ...ance sends the result from the display It is counted on base on form for the parameter x 0 1 s time yestu interval Value from 1 to 9999 can be written 08 Min mass Min mass for automatic work RS 232 Fo...

Страница 34: ...e balance show only first of them 09 Taele Hk If the measurement is done in units 11 Taele T set the attribute 0 no for two previous Enter group of the parameters P7 Units according to p 5 2 7 Draw 24...

Страница 35: ...uence on work with balance in group of the parameters P9 Others eg beep signals etc Enter submenu group P9 Others the same as in p 14 01 Setting ID it includes 6 digits 6 codes which can be used durin...

Страница 36: ...Printout of the parameters if the function is active the balance parameters in user menu are printed User gives numbers of the parameters which should be printed Draw 26 Submenu Others printing settin...

Страница 37: ...MODES 17 1 Counting pieces of the same mass It can be done after write singular piece mass Write singular piece mass Determine singular piece mass on base of standard quantity Element selection from...

Страница 38: ...h determine singular element mass from the standard batch Start the procedure of counting pieces in accordance with p 16 1 1 it does not matter which mass in the field 01 Select 07 Start and press the...

Страница 39: ...mass This way mass of singular piece can be determined on base of batch standard The are four conditions of AKD Automatic Correction of Preciseness in the balance software 1 quantity of pieces after a...

Страница 40: ...he Enter record name and Enter record value Next to name singular piece mass should be introduced It can be remembered using 02 Recall sample 17 1 3 Select piece from data base Active function of coun...

Страница 41: ...raphs and controled The function activation Draw 33 Checkweighing the function activation Display Draw 34 Checkweighing display view 1 result 2 bargraphs 3 function name 4 difference between mass of w...

Страница 42: ...etting parameters without changes Checkweighing with stage base Checkweighing in RANGE BASE which contains 500 records Name of the product for each record max 10 alphanumerical signs Value of upper ra...

Страница 43: ...Draw 37 Checkweighing stage base programming values Enter name for selected record product name Enter value of upper range Enter value of down range Confirm values with ENTER press twice Draw 38 Chec...

Страница 44: ...duct recorded in range base 8 difference between result and the ranges 9 graphic view which place weighed mass is 10 used load of the balance Selecting other product from stage base Press SETUP during...

Страница 45: ...function Draw 40 Dosage activation Display Draw 41 Dosage display 1 mass which should be added 2 graphs 3 function name 4 TR reference value mass which is declared see drawing 38 M3 01 Reference mass...

Страница 46: ...in percentages Following functions dosage weighing statistics can cooperate with deviation function Activation of the function Draw 42 Percents activation Display Draw 43 Percents display 1 percentage...

Страница 47: ...stics and change the attribute NO into attribute YES Confirm this option and press the key Enter Draw 44 Percents cooperation with other functions 1 percentage value relation of the load on the pan to...

Страница 48: ...sult can be printed Return to statistics submenu and higher levels key ESC Draw 45 Percents cooperation with other functions Statistics Reference mass In this software reference mass can be defined by...

Страница 49: ...r filter the shorter time of measurement STAGE Value in actual scale intervals is value the result must be below The result of weighing must be smaller than value of actual scale intervals in order to...

Страница 50: ...lytical balance there are Specific Gravity Measurement Kit Draw 47 Specific Gravity Measurement Kit Components of the kit 1 Beaker stand 2 Pan stand 3 Float 4 Beaker 5 Termometer clamp 6 Termometer 7...

Страница 51: ...ds is based on comparison sample mass in air weighed on top pan to the same sample mass in the liquid on bottom pan The program counts density of sample and displays it on the display The result can b...

Страница 52: ...mponents the mixture should include max 20 signs parameter 04 Recipe after set this parameter following submenu is displayed In this submenu user can write names not more than 10 signs and set standar...

Страница 53: ...e 6 quantity of weighed components in the recipe 7 name of weighed component 8 side graphs Information how much left to gain settled component is presented on these graphs Draw 50 Graphs automatic sca...

Страница 54: ...set 8 for quantity of components the program finishes preparation of the mixture after weighing 8 components The balance program creates mixture in order of recorded components in the parameter 04 Re...

Страница 55: ...o the balance memory Pour component 1 to the container in relation to information about mixture Press the UNITS key Mass of component 1 is recoded in the balance memory The information on the display...

Страница 56: ...t measure unit is displayed and after pressing ENTER User decides what statistic date are presented on the graphic display during measurements by setting their activity in the submenu of work mode val...

Страница 57: ...of variation factor 10 measure unit g 11 work mode 17 9 Calibration of pipettes Function of pipettes calibration refers to pipettes with stable and changeable capacity During the procedure precision...

Страница 58: ...ibration following data must be loaded Pipette stable changeable capacity capacity Vmax ml capacity V1 2max ml capacity Vmin ml Error of capacity Vmax Error of capacity V1 2max Error of capacity Vmin...

Страница 59: ...average capacity 5 precision error 6 amount of samples measurements Final result of the procedure is error of precision ES standard deviation sr and repeatability error CV After each check a result i...

Страница 60: ...dure 18 KINDS OF PRINTOUTS 18 1 Standard printout There are 2 types of printouts First of them is standard printout It includes result of weighing and all variables which have attribute YES in GLP sub...

Страница 61: ...les to printout submenu GLP Example of standard printout Draw 59 Example of standard printout all options settled on YES printed Draw 60 Example of standard printout Question mark before load mass mea...

Страница 62: ...Start 20 Printout 2 Stop 40 Non standard printout can be created by Edition of the printout During manual writting give all special signs as CRLF tabulator etc If function Printout Edition is used al...

Страница 63: ...time of last calibration K Kind of last calibration I Deviation of last calibration 1 Code 1 2 Code 2 3 Code 3 4 Code 4 5 Code 5 6 Code 6 Variables dependent on used work mode Variable Description Mod...

Страница 64: ...unit Value connected to work mode eg counting pieces for mode Counting pieces or deviation from standard mass in for mode Deviation Special signs used to create special printouts Singular sign c CRLF...

Страница 65: ...a c 23 Text 14 z a 1 1 2 24 Text 15 5 5 0 g Example 2 Zak ad Mechaniki Precyzyjnej RADEKW Date Time Moad mass Signature actual work mode Set following texts and write 8 signs in each of them untill it...

Страница 66: ...sign is cancelled Confirm the text On PS 2 keyboard Press F2 to enter main menu Press F3 to set parameters indications next to group P6 Printouts and press F2 to enter menu group and then select para...

Страница 67: ...18 2 3 Select non standard printouts if STANDARD printout is selected there will be only result and variables declared in the GLP see p 17 1 Standard printout drawing 60 Declaration of the variables...

Страница 68: ...w 64 Connections balance computer The balance connection DB 9 F The computer connection DB 9 F with control of sending date Balance Computer 2 RxD 3 TxD 3 TxD 2 RxD 4 DTR 6 DSR 5 GND 5 GND 6 DSR 6 DTR...

Страница 69: ...t a proper number of characters for each variable charts 2 3 and 4 After giving it an original name save the label on a computer hard drive alphanumeric characters Download the label to the CITIZEN CL...

Страница 70: ...2L c Start of the label rlabelname c Label name X c Start of variables edition 02U01NN c Variable 1 NN variable symbol 02U02NN c Variable 2 NN variable symbol 02U03NN c Variable 3 NN variable symbol 0...

Страница 71: ...rameters Now you can connect the balance with the printer a cable diagram in the users manual Check the setting of transmission parameters both in the balance and in the printer They should be the sam...

Страница 72: ...erator number F X Name of present operation work mode C 25 Date and time of last calibration K X Type of last calibration I 16 or 18 Deviation in the last calibration 1 6 Code 1 2 6 Code 2 3 6 Code 3...

Страница 73: ...g b 14 Threshold i 14 Liquid Mass density measurement p 14 Procedure c 14 Temperature a 16 Liquid mass den sity v 16 Plunger volume TABLE 4 Zmienne statystyczne wyst puj ce we wszystkich modach opr cz...

Страница 74: ...e printout according to below tables with Polish signs CP 852 A5 86 A9 88 E4 A2 98 AB BE CP 852 A4 8F A8 9D E3 E0 97 8D BD instead of polish signs write their code equvivalents To have the paper cut a...

Страница 75: ...ce There is a hook visible which can be used to suspend a sample Hang the load on the look in the hole under the balance the hook is a part of standard equipment Note 1 The suspension eye is directly...

Страница 76: ...and PC CR LF all recorded information in commands in the balance programme are sent from the balance Function SEND THE RESULT IN BASIC UNIT Command S CR LF result is sent from the balance in basic int...

Страница 77: ...on WRITE NEW OR CHANGE TIME IN THE BALANCE Command PD CR LF the balance sends settled time or this time is changed Function WRITE ACTUAL WORK MODE Command PM CR LF Function SEND SETUP Command PS CR LF...

Страница 78: ...ction SWITCH ECHO OFF FOR THE KEYBOARD Command E0 CR LF keys codes are switched off Function SWITCH ECHO ON FOR THE KEYBOARD Command E1 CR LF Function SWITCH THE BALANCE OFF Command O0 CR LF the same...

Страница 79: ...ss recorded in the balance memory higher than difference 1 Piece 1 Div 2 10 Singular mass value in counting pieces function less than actual scale interval Piece 10 Div 2 11 Mass on the pan during det...

Страница 80: ...80...

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