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Integrated Multi-parameter Sensor Operation manual

17

Figure 14 Fluoride ion sensor

Fluoride sensor Specification

principle

ion-selective electrode method

Range

0.5~1000 mg/L

resolution

0.01~1 mg/L depending on the range

Accuracy

±

10 % or

±

2 mg/L,

(the electrode is greatly affected by

temperature, field comparison is the best field calibration,

otherwise it may be out of range)

2.13 Chloride Ion Sensor

CL-ion selective electrode is a kind of solid membrane electrode. A high strength AgCl/Ag 2S compact

solids is the main material of the membrane, which then is sealed in the plastic with resin. Sliver is

adopted as the conductive electrode for the surface of solid. The appearance of chloride ion sensor is

showed by the Figure 15

Figure 15 Chloride ion sensor

Содержание BQ301

Страница 1: ...Integrated Multi parameter Sensor Operation manual BQ301 Integrated Multi parameter Sensor Operation manual...

Страница 2: ...year from the date of purchase you will be served with product maintenance for free Except the consumables 2 No matter where the product you buy from the manufacturer hereby guarantees that you will...

Страница 3: ...Integrated Multi parameter Sensor Operation manual upgraded in stages The general changes are subject to change without notice Please refer to the actual product...

Страница 4: ...mperature limit 5 1 5 Minimum depth requirement 5 Chapter 2 Introduction to Sensors 5 2 1 Temperature Sensor 6 2 2 pH Sensor 6 2 3 ORP Sensor 7 2 4 Conductivity Sensor 8 2 4 1 Conductivity Sensor 8 2...

Страница 5: ...3 4 2 2 Calibration 23 4 2 3 History data 24 4 2 4 System Settings 25 4 2 4 1 Device settings 25 4 2 4 2 Software Settings 26 4 2 5 System Information 27 Chapter 5 Setting and operation of hand manipu...

Страница 6: ...9 Ion Sensors Calibration 46 6 1 9 1 Ammonia Nitrogen Sensor Calibration 46 6 1 9 2 Nitrate ion Sensor Calibration 48 6 1 9 3 Fluorine Ion Sensor Calibration 50 6 1 9 4 Chloride Ion Sensor Calibration...

Страница 7: ...62 7 1 4 Dissolved oxygen sensor maintenance 62 7 1 5 Depth sensor maintenance 63 7 1 6 Standard optical sensor maintenance 63 7 1 7 Ion Sensor Maintenance 63 7 2 Sensor Storage 65 7 2 1 Short Storage...

Страница 8: ...a variety of electrochemical optical or physical means of detection The integrated multi parameter analyzer can be equipped with self cleaning system to obtain accurate data for a long time and with d...

Страница 9: ...of integrated multi parameter analyzer on line and can read and export the history data only can read and export history data stored by hand manipulator Also hand manipulator can complete the paramete...

Страница 10: ...ction 3 7 V Lithium Battery Protection Level IP67 Operating Temp 0 50 not frozen Storage Temp 15 60 not frozen Size 203 100 43mm Weight 0 5KG 1 2 Safety Information Please read this manual thoroughly...

Страница 11: ...he instrument otherwise it may cause personal injury or damage to the instrument If the label is marked on the instrument refer to the instrument manual for operation and or safety information If the...

Страница 12: ...lowing parameters depth temperature pH ORP conductivity turbidity dissolved oxygen chlorophyll blue green algae ammonia nitrogen nitrate fluoride and chloride The wide range of physical biological and...

Страница 13: ...responding calculation formula This formula has been built into the host software and the user can directly view the real time Celsius The appearance of the temperature sensor is shown in Figure 3 Fig...

Страница 14: ...should be no air bubbles between the bulbs of the inner electrodes of the glass electrodes and if there are bubbles the bubbles can escape easily Important Tip 2 Provided the pH is used in high sulfu...

Страница 15: ...vity sensor is a combination of two parallel plates When it is placed in the solution to be tested and a certain potential usually a sinusoidal voltage is applied across the plates the interpolate flo...

Страница 16: ...the total amount of salt dissolved in a body of water It can be automatically calculated from the conductivity and temperature detected by the multi parameter analyzer The algorithm is based on the s...

Страница 17: ...present in a body of water and is usually referred to as DO The dissolved oxygen sensor is measured by fluorescence method The top of the sensor is covered with a layer of fluorescent substance When...

Страница 18: ...er Suspended solids in water are generally clay sand colloidal matter algae plankton and microorganisms The turbidity sensor is designed based on a combined infrared absorption scatter ray method The...

Страница 19: ...ulated by subtracting the atmospheric pressure from the pressure applied by the water body The distance from the depth sensor to the liquid surface is the measurement distance Reasons that affect dept...

Страница 20: ...ng the amount of chlorophyll in the water sample The chlorophyll sensor in utilizes the characteristic that chlorophyll A has absorption peak and emission peak in the spectrum Monochromatic light emit...

Страница 21: ...lity of water bodies When the water body grows vigorously it will cause discoloration and odor The blue green algae sensor utilizes the characteristic that the cyanobacteria has an absorption peak and...

Страница 22: ...widely used include drinking water fertilizer and refrigerant To use the electrode requires the reference electrode it has good repeatability and faster response time but its accuracy is no better tha...

Страница 23: ...re 13 as below Figure 13 Nitrate ion sensor Nitrate ion sensor Specification principle ion selective electrode method Range 0 5 100mg L resolution 0 01 1 mg L depending on the range Accuracy 10 or 2 m...

Страница 24: ...by temperature field comparison is the best field calibration otherwise it may be out of range 2 13 Chloride Ion Sensor CL ion selective electrode is a kind of solid membrane electrode A high strength...

Страница 25: ...s in this manual 3 1 Instrument Unboxing Take it out of the cartons that ship the instrument and check for obvious damage If any item is lost or damaged please call customer service Tip It is normal t...

Страница 26: ...l be over pressed If there is no suitable power supply at the site you can use the 220VAC to 9 36VDC power Core definition table Wire Core No 1 2 3 4 Sensor Wire Red Black Blue White Signal 12VDC AGND...

Страница 27: ...tection device read the data stored by the probe and complete the basic setup and calibration of the instrument Connection reference diagram Figure 16 is a reference diagram Figure 16 Connection refer...

Страница 28: ...ons 1 During handling or installation please note If there is an ion electrode the counterweight should be pl aced face down do not place it sideways less than 60 degrees do not invert Or need to shak...

Страница 29: ...pplication displays as shown below The electrode is an optional ion selective electrode ammonia nitrogen nitrate ion chloride ion fluoride ion and an ORP electrode which can be arbitrarily selected an...

Страница 30: ...Data click Confirm to monitor the online data in real time If you select Automatically switch directly you do not need to re select the operating mode when changing the menu bar The starting time tota...

Страница 31: ...ction of storing historical data Before viewing historical data need set the running mode to historical data and then click confirm to view the required data in the menu of historical data If you sele...

Страница 32: ...After manually setting the current time and clicking OK the manually set time will be updated to the sensor Communication settings Baud rate 4800 9600 19200 38400 115200 When a baud rate is selected a...

Страница 33: ...s the power on switch is manually triggered Sleep cycle It is the timing acquisition operation mode It is necessary to set the timed acquisition mode to input an integer of more than 5 in the input bo...

Страница 34: ...4 2 5 System Information From the system information you can view Controller Version Power Control Version Dissolved Oxygen Turbine Version chlorophyll Version Software version chlorophyll version BGA...

Страница 35: ...ed multi parameter analyzer is starting up in the process of operation by hand manipulator Please check the details in Chapter 3 2 2 Press the key of direction downward to choose configuring and press...

Страница 36: ...e Press the keys of up and down to choose baud rate of 19200 and then choose scanning At last press the key of Enter to confirm 3 Settings of manual and automatic refresh of data Choose the key of 0 i...

Страница 37: ...be will occur So choose read first If the existing probe does not occur please revise the related options by manual operation and then choose the option of manual configuring At last press the key of...

Страница 38: ...ude and latitude in the column of history information refers to the last information saved by pressing the key of save If it is not necessary to save current information of longitude and latitude plea...

Страница 39: ...to time use and environment To ensure the accuracy of the instrument it is recommended to perform routine testing under the standard conditions for the system Note If there is only one parameter to be...

Страница 40: ...calibration methods The specific sensor calibration method will be introduced later in this chapter The calibrated menu bar is shown below Tip The calibration of each sensor follows the basic steps ab...

Страница 41: ...e pH sensor uses a 2 point calibration method The specific calibration steps are 1 First point neutral point Pour the correct amount of pH 6 864 buffer standard solution into a clean dry or pre rinsed...

Страница 42: ...ffer The specific steps are change the mode setting For on line date place the probe in a calibration container containing the correct amount of buffer standard solution at pH 9 18 place the glass bub...

Страница 43: ...lothing when preparing the solution stir to dissolve to saturation and place the sensor in the standard solution and stir at an appropriate rate Carefully immerse the probe at the end of the main unit...

Страница 44: ...or the conductivity sensor is required Before the test remove the protective soaking bottle or rubber sleeve with the soaking liquid on the sensor immerse the sensor in distilled water and then remove...

Страница 45: ...can also directly enter the value in the Correction Parameters box and click factor and deviation to calibrate the factor and deviation value 6 1 6 DO Dissolved Oxygen Calibration From the Calibratio...

Страница 46: ...n compensation measures can be taken Correcting the output result to achieve a certain range to eliminate the influence of salinity change on the output signal of the sensor is called salt compensatio...

Страница 47: ...ng immersed in any container The specific calibration steps are as follows Try to ensure that the sensor is dry before calibration When the atmospheric pressure value in the calibration interface is s...

Страница 48: ...ndard The specific calibration steps are as follows A 4 point calibration 1 Pour distilled water into a clean dry or pre rinsed calibration container Carefully immerse the probe at the end of the main...

Страница 49: ...rinsed calibration container Carefully immerse the probe at the end of the main unit in the solution Make sure that the front end of the turbidity probe is immersed in the solution for at least 2 cm W...

Страница 50: ...tion menu select the chlorophyll option to enter the chlorophyll calibration procedure as shown in the figure below and then ready to start calibration Chlorophyll calibration typically uses a two poi...

Страница 51: ...sensor and calibration container with water and dry You can also directly enter the value in the Correction Parameters box and click factor and deviation to calibrate the factor and deviation value I...

Страница 52: ...er sample of blue green algae There are usually two standards that can be used A phytoplankton water samples of known blue green algae content B Rhodamine B stain solution Remove the probe from the di...

Страница 53: ...fference of potassium ion below 5mg L is small it should be larger than 3mg L and then judge whether the standard pressure difference is in line with the 10 fold relation 6 1 9 1 Ammonia Nitrogen Sens...

Страница 54: ...L 5 mg L and 10 mg L can be selected When the concentration range of the measured water is generally between 20 and 30 then 0 02mg L 10 mg L and 50 mg L can be selected When selecting the calibration...

Страница 55: ...er with water after completion You can directly select the input value in the correction parameter box and click factor and deviation to calibrate the factor and deviation value In the mode box you ca...

Страница 56: ...n the concentration range of the measured water is generally between 5 and 10 then 0 02mg L 5 mg L and 10 mg L can be selected When the concentration range of the measured water is generally between 2...

Страница 57: ...tware interface is stable click 3 point Calibration Rinse and dry the sensor and calibration container with water after completion You can directly select the input value in the correction parameter b...

Страница 58: ...nerally between 20 and 30 then 0 02mg L 10 mg L and 50 mg L can be selected When selecting the calibration point please note that when the measured value is high select a higher value of the calibrati...

Страница 59: ...tion parameter box and click factor and deviation to calibrate the factor and deviation value 6 1 9 4 Chloride Ion Sensor Calibration See section 6 1 9 for instructions before calibration Take an opti...

Страница 60: ...00mg L can be used For instance the points of 0 02mg L 1 mg L 10mg L 200mg L and 1000mg L can be used Usually choose the points of 1 mg L and 10mg L of chloride ion and add some other points can obtai...

Страница 61: ...robe at the end of the main unit in the solution Please ensure that the front end of the Chloride Ion Sensor is immersed in the solution at least 2 cm and enter the standard value When the value in th...

Страница 62: ...the key of OK and press the key of Enter And then the pH standard solution value neutral can be input at the neutral point such as 6 86 Choose the key of OK and press the key of Enter 6 2 3 Conductiv...

Страница 63: ...ore calibration The calibration for depth sensor is mainly the calibration for the pressure of atmosphere so please make sure that the depth sensor is in the air and not immerged in any container Clic...

Страница 64: ...tion value in the square frame of the hand manipulator Then choose the key of OK and press Enter for calibration and confirm the calibration status according to the prompt of calibration status When t...

Страница 65: ...s the key of Enter to perform cleaning procedure for one time by scratching and eliminate the influence of bubbles on blue green algae calibration process Press the key of OK at the site of zero calib...

Страница 66: ...hoose first point second point third point fourth point fifth point chloride ion calibration according to actual requirement to make integrated multi parameter analyzer immerge into standard solution...

Страница 67: ...rogen calibration and press the key of calibration Press the key of Enter to calibrate the ammonia nitrogen Choose first point second point third point fourth point fifth point ammonia nitrogen calibr...

Страница 68: ...robes and rinse the sensor probe with water Do not use any object to poke the sensor otherwise the sensor film will rupture 7 1 2 pH sensor maintenance The pH sensor requires frequent maintenance to r...

Страница 69: ...e conductivity cell which can be recovered after cleaning with an alcohol cotton ball 7 1 4 Dissolved oxygen sensor maintenance It is recommended to clean the dissolved oxygen sensor at intervals usua...

Страница 70: ...trument with soap and water Soak the entire instrument in clean water for at least 5 minutes Observe the optical window of the probe clean the optical window of the probe with a tissue paper or cotton...

Страница 71: ...deionized water can be put into the electrode first and the electrode should be cleaned according to process 3 And then a little electrolyte should be added 3 Clean the electrode by shaking slightly u...

Страница 72: ...to the calibration container and tighten to prevent evaporation of the water 7 2 2 Long term storage Long term refers to the state of being unused for a long time 1 For long term storage of the pH sen...

Страница 73: ...h Any cable should be protected from wear unnecessary tension repeated bending or severe bending such as railings during use 7 4 Sensor damage check Check the appearance of the sensor for damage If th...

Страница 74: ...ate is 9600 It can communicate with the host computer PC digital instrument etc with RS485 communication function The specific MODBUS RTU table is shown in the table below MODBUS RTU Baud rate 9600 48...

Страница 75: ...ents dissolved oxygen temperature 3 represents pressure temperature 4 represents manual input temperature 422 manual temperature compensation value float read write range 10 100 2 pH value float read...

Страница 76: ...calibration 430 salinity compensation model float read write 0 no compensation 1 manual compensation 2 salinity sensor compensation 432 salinity compensation value float read write Register 430 salin...

Страница 77: ...al value of the standard liquid 1016 turbidity high point calibration float write Enter 1 into the turbidity calibration mode of register address 906 first so that the turbidity sensor enters into the...

Страница 78: ...e green algae value float read 100 300000 cells mL 1030 blue green algae AD value float read 1032 blue green algae channel value float read 1614 blue green algae factor float read write Default 1 1514...

Страница 79: ...181 represents the first point 182 represents the second point 183 represents the third point and 184 represents the fourth point 530 interval of scratching float read write unit min 532 manual scratc...

Страница 80: ...epresented by floating point number of 1 2 3 4 5 and 6 1 represents ORP 2 represents ammonia nitrogen 3 represents Nitrate ion 4 represents chloride ion And 5 represents fluoride ion 2208 calibration...

Страница 81: ...float write input the standard solution value 2244 the second point standard solution value of electrode 1 float read 2246 electric voltage of the second point standard solution calibration of electr...

Страница 82: ...th point standard solution calibration of electrode 1 float read 2264 temperature of the fourth point standard solution calibration of electrode 1 float read 2266 fifth point calibration of electrode...

Страница 83: ...presents chloride ion And 5 represents fluoride ion 2308 calibration points of electrode 2 UINT16 read write Support the command of 06 The written values of 1 2 3 4 and 5 respectively represent single...

Страница 84: ...t standard solution calibration of electrode 2 float read 2348 temperature of the second point standard solution calibration of electrode 2 float float 2350 third point calibration of electrode 2 floa...

Страница 85: ...loat write input the standard solution value 2368 the fifth point standard solution value of electrode 2 float read 2370 electric voltage of the fifth point standard solution calibration of electrode...

Страница 86: ...3 4 and 5 respectively represent single point calibration to 5 point calibration 2415 stability float read Represents the stability of the electrode voltage used during calibration the value on 0 9 r...

Страница 87: ...ond point standard solution calibration of electrode 3 float float 2450 third point calibration of electrode 3 float write input the standard solution value 2452 the third point standard solution valu...

Страница 88: ...solution value of electrode 3 float read 2470 electric voltage of the fifth point standard solution calibration of electrode 3 float read 2472 temperature of the fifth point standard solution calibrat...

Страница 89: ...ility of the electrode voltage used during calibration the value on 0 9 represents the stability 2534 first point calibration of electrode 4 float write input the standard solution value 2536 the firs...

Страница 90: ...lution value 2552 the third point standard solution value of electrode 4 float float 2554 electric voltage of the third point standard solution calibration of electrode 4 float read 2556 temperature o...

Страница 91: ...perature of the fifth point standard solution calibration of electrode 4 float read Note electrode 1 4 channels customers can choose to access according to the access channel corresponding to the corr...

Страница 92: ...ration Standard solution is not properly formulated or the electrode is damaged Slow data response Is the standard liquid contaminated According to the type of pollutants it is cleaned according to th...

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