Contents
1 Getting
Started
3
1.1 Layout of the liquid handling system
3
1.2 Layout of the
in situ
sample
stick
4
1.3 Layout of the pump
4
2 General
procedures
6
2.1
Sample
loading
6
2.1.1
Loading
Vessel
1
6
2.1.2
Loading
Vessel
2
6
2.2
Evacuation
of
the
system
6
2.2.1 Removing air from Vessel 1
7
2.2.2 Removing air from Vessel 2
7
2.2.3 Removing air from Vessel 3
7
2.2.4 Evacuation of the sample cell
7
2.3
Freeze-Pump-Thaw
cycle
8
2.3.1
Sample
in
Vessel
1
8
2.3.2
Sample
in
Vessel
2
8
2.3.3
Sample
in
Vessel
3
9
2.4
Liquid
transfers
9
2.4.1 Vessel 1 to sample cell
9
2.4.2 Vessel 3 to sample cell
10
2.4.3 Recovery of liquid in manifold to Vessel 2
10
2.4.4 Recovery of liquid in sample cell to Vessel 1
11
2.4.5 Recovery of liquid in sample cell to Vessel 2
11
2.4.6 Recovery of liquid in sample cell to Vessel 3
11
3 Example
Experiment
13
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2
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