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LC-23A COLUMN HEATING
COMPARTMENT

1.

Place the LC-23A heating Compartment in the desired location. Six holes with captive
6-32 threads are provided for secure mounting on your liquid chromatograph, if
desired. The holes are positioned to fit early model (pre 1986) BAS liquid

chromatography support stands.

2.

Connect the LC-23A heater power cable to the power socket on the back panel of the

LC-22C Controller.

3.

Connect the red, black and yellow plugs on the probe cable to the jacks marked “PROBE
1" or ”PROBE 2" on the LC-22C back panel.

4.

Remove the cover on the LC-23A Column Heater by unscrewing the two cap screws.
Place the column in the recessed cavity and route the inlet and outlet tubing out of the
top and bottom slots. A special preheater block (EW-8146) is also supplied. Under

certain circumstances, dramatic band broadening may result if the preheater is not
utilized. Typically this becomes obvious when the temperature differential between

ambient and the desired set point exceeds 20-25°C.

If you plan to use several different styles of column endfittings, it is best to use

removable plastic fittings. BAS recommends a 2-piece PEEK finger-tight seal as
provided in BAS part no. MR-4409 (this includes a nut and ferrule). One piece plastic
fittings tend to loosen at higher temperatures.

Figure 3.

Position of Mounting Points on LC-23A Heater.

Figure 4.

LC-23A Column Heater with LC-23PH Preheater Installation.

 2.01

 5.00

 6.00

 3.37

 0.50

 0.75

 0.50

 8.89cm

 4.92cm

 4.12cm

 10.79cm

 9.36cm

 39.37cm

 2.03cm

 2.54cm

 1.93cm

PREHEATER

1.91 x 2.54cm

INLET DEPTH

1.89cm

CHANNEL WIDTH

0.685cm

COLUMN

HEATER

BLOCK

SENSOR

LOCATION

ADAPTER FOR

25-30cm COLUMNS

OUTLET DEPTH

1.85cm

Section 3. INSTALLATION

LC-23A COLUMN HEATING COMPARTMENT

4

Содержание LC-22C

Страница 1: ...2C March 2000 MF 9010 INSTRUCTION MANUAL Temperature Controllers for Liquid Chromatography B i o a n a l y t i c a l S y s t e m s I n c 2701 Kent Avenue W e s t L a f a y e t t e I n d i a n a 4 7 9...

Страница 2: ...l Systems Inc Copyright March 2000 No portion of this manual may be reproduced without express written permission of Bioanalytical Systems Inc ALL RIGHTS RESERVED Bioanalytical Systems Inc 2701 Kent A...

Страница 3: ...rable It accepts most commercially available 15 25 or 30 cm analytical columns A solid aluminum inner compartment thermally isolated from the outer cover encloses the entire column A preheater coil is...

Страница 4: ...e securely fastened to an earth ground LC 23A and LC 23C HEAT ING COMPARTMENTS The LC 23A and LC 23C compartments are designed specifically for use with the LC 22C Controller Two cables one for heater...

Страница 5: ...1 and channel 2 are identical calibrating instructions will be given for channel 1 adjustments while channel 2 adjustments will appear in parentheses To calibrate the probe place it in an ice bath an...

Страница 6: ...also supplied Under certain circumstances dramatic band broadening may result if the preheater is not utilized Typically this becomes obvious when the temperature differential between ambient and the...

Страница 7: ...l provide satisfactory temperature control for the electrochemical cell if you keep the cover closed during operation Before installing the LC 23C give some thought to the configurations of the column...

Страница 8: ...r block through the now open utility access in the CC 5 back panel On some models the two registration posts on the CC 5 inner panel will engage the LC 23C block for support 4 Secure the LC 23C to the...

Страница 9: ...manent ferrule on the outlet end of the preheater coil A removable high pressure fitting provides an equivalent seal without irreversible attachment Use BAS part no MR 4409 Figure 7 Column Preheater C...

Страница 10: ...nd Electrochemical Cell Preheater 1 Ensure that the three 3 leads from the column heaters or cell preheater are plugged into the jacks marked PROBE 1 or PROBE 2 2 Turn on the LC 22C Set the desired te...

Страница 11: ...l 4 An analog voltage of 100 mV 0 1 volt is equivalent to 1 C For example 8 92 volts 89 2 C 0 36 volts 3 6 C This voltage may be recorded using a strip chart recorder Set the full scale input of the r...

Страница 12: ...er than ambient allow at least 1 C difference The HTR LED indicator on the LC 22C should be on continuously 4 An open circuit anywhere in the probe cable or across its input jacks will automatically s...

Страница 13: ...ed circuit If your unit fails either step 3 or 4 please contact the BAS Service Coordinator to return both the LC 22C and the probe used to make these tests for service Do not return any equipment wit...

Страница 14: ...y 0 1 C with the same temperature probe Output Temperature Calibration Output is calibrated to 100 mV per C Rear Panel Probe input jacks output temperature jack output power socket heaters line voltag...

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