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Section 4. OPERATION

For purposes of instruction, we will reference channel 1, although channel 2 is identical.

1.

With the heater and probe cables disconnected, turn on the main power to the LC-22C.

2.

Rotate the display selector knob to illuminate “SET 1" in the red display window.

3.

Using the “SETPOINT HEATER 1" knob, select the desired temperature, which is between

ambient and 99.9°C.

4.

Turn off the main power to the LC-22C and connect the heater to “HTR-1" and the red,
yellow and black probe plugs to the same color jacks of ”PROBE-1" on the back panel.

5.

Turn on the main power to the LC-22C. The heater indicator LED will remain constantly
illuminated until the set point is reached, then it will dim or blink intermittently to

indicate maintenance at the desired temperature. You can also observe the measured

probe temperature by changing the display select switch to “SENS 1".

TEMPERATURE MEASURE-
MENT/CONTROL MODE

LC-23A or LC-23C Column Heaters
and Electrochemical Cell Preheater

1.

Ensure that the three (3) leads from the column heaters or cell preheater are plugged into

the jacks marked “PROBE 1" or ”PROBE 2"

2.

Turn on the LC-22C. Set the desired temperature (at least 5°C above ambient).

3.

The measured temperature can be read on the front panel digital display of the LC-22C by

using the display selector knob. The temperature is also available as an analog voltage
at the screw terminals marked “ 1 -” or “ 2 -”, depending upon

the channel used. Each 100 mV (0.1 volt) is equivalent to 1°C. For example:

+8.92 volts = +89.2°C
-0.36 volts = - 3.6°C

This voltage may be recorded using a strip chart recorder. Set the full scale input of
the recorder to 10 volts and observe the marked polarity on the back panel.

4.

The LED light will stay on continuously until the heater achieves the setpoint and then will
flash intermittently while maintaining this temperature. The actual temperature (within

the absolute accuracy of the probe) at any point in time will be displayed on the front

panel digital display of the LC-22C or the recording device.

Section 4. OPERATION

TEMPERATURE MEASUREMENT/CONTROL MODE

8

Содержание LC-22C

Страница 1: ...2C March 2000 MF 9010 INSTRUCTION MANUAL Temperature Controllers for Liquid Chromatography B i o a n a l y t i c a l S y s t e m s I n c 2701 Kent Avenue W e s t L a f a y e t t e I n d i a n a 4 7 9...

Страница 2: ...l Systems Inc Copyright March 2000 No portion of this manual may be reproduced without express written permission of Bioanalytical Systems Inc ALL RIGHTS RESERVED Bioanalytical Systems Inc 2701 Kent A...

Страница 3: ...rable It accepts most commercially available 15 25 or 30 cm analytical columns A solid aluminum inner compartment thermally isolated from the outer cover encloses the entire column A preheater coil is...

Страница 4: ...e securely fastened to an earth ground LC 23A and LC 23C HEAT ING COMPARTMENTS The LC 23A and LC 23C compartments are designed specifically for use with the LC 22C Controller Two cables one for heater...

Страница 5: ...1 and channel 2 are identical calibrating instructions will be given for channel 1 adjustments while channel 2 adjustments will appear in parentheses To calibrate the probe place it in an ice bath an...

Страница 6: ...also supplied Under certain circumstances dramatic band broadening may result if the preheater is not utilized Typically this becomes obvious when the temperature differential between ambient and the...

Страница 7: ...l provide satisfactory temperature control for the electrochemical cell if you keep the cover closed during operation Before installing the LC 23C give some thought to the configurations of the column...

Страница 8: ...r block through the now open utility access in the CC 5 back panel On some models the two registration posts on the CC 5 inner panel will engage the LC 23C block for support 4 Secure the LC 23C to the...

Страница 9: ...manent ferrule on the outlet end of the preheater coil A removable high pressure fitting provides an equivalent seal without irreversible attachment Use BAS part no MR 4409 Figure 7 Column Preheater C...

Страница 10: ...nd Electrochemical Cell Preheater 1 Ensure that the three 3 leads from the column heaters or cell preheater are plugged into the jacks marked PROBE 1 or PROBE 2 2 Turn on the LC 22C Set the desired te...

Страница 11: ...l 4 An analog voltage of 100 mV 0 1 volt is equivalent to 1 C For example 8 92 volts 89 2 C 0 36 volts 3 6 C This voltage may be recorded using a strip chart recorder Set the full scale input of the r...

Страница 12: ...er than ambient allow at least 1 C difference The HTR LED indicator on the LC 22C should be on continuously 4 An open circuit anywhere in the probe cable or across its input jacks will automatically s...

Страница 13: ...ed circuit If your unit fails either step 3 or 4 please contact the BAS Service Coordinator to return both the LC 22C and the probe used to make these tests for service Do not return any equipment wit...

Страница 14: ...y 0 1 C with the same temperature probe Output Temperature Calibration Output is calibrated to 100 mV per C Rear Panel Probe input jacks output temperature jack output power socket heaters line voltag...

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