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62

5

Optimizing Performance

Optimization for Lowest Carry-over

Optimization for Lowest Carry-over

Several parts of an injection system can contribute to carry-over:

•

needle outside

•

needle inside

•

needle seat

•

sample loop

•

seat capillary

•

injection valve

The autosampler continuous flow-through design ensures that sample loop, 
needle inside, seat capillary, and the mainpass of the injection valve is always 
in the flow line. These parts are continuously flushed during an isocratic and 
also during a gradient analysis. The residual amount of sample remaining on 
the outside of the needle after injection may contribute to carry-over in some 
instances. When using small injection volumes or when injecting samples of 
low concentration immediately after samples of high concentration, carry-over 
may become noticeable. Using the automated needle wash enables the 
carry-over to be minimized and prevents also contamination of the needle 
seat.

Содержание G1329A

Страница 1: ...Agilent 1260 Infinity Preparative Autosampler User Manual...

Страница 2: ...ch license Restricted Rights Legend If software is for use in the performance of a U S Government prime contract or subcon tract Software is delivered and licensed as Commercial computer software as d...

Страница 3: ...tions 27 Performance Specifications 28 3 Installing the Autosampler 33 Unpacking the Autosampler 34 Optimizing the Stack Configuration 37 Installing the Autosampler 41 Installing the Thermostatted Aut...

Страница 4: ...als for Maintenance 105 Main Assemblies 106 Analytical Head Assembly 108 Vial Trays 111 Standard Autosampler Accessory Kit G1329 68725 112 Preparative Autosampler Accessory Kit G2260 68705 113 Mainten...

Страница 5: ...5 Contents 10 Appendix 137 General Safety Information 138 Lithium Batteries Information 142 Radio Interference 143 Sound Emission 144 Agilent Technologies on Internet 145...

Страница 6: ...6 Contents...

Страница 7: ...to the Autosampler 8 Sampling Sequence 10 Injection Sequence 11 Sampling Unit 13 Needle Drive 14 Analytical head preparative head 14 Injection Valve 15 Transport Assembly 16 Early Maintenance Feedback...

Страница 8: ...rs simultaneously A specially designed sample rack holding 100 1 8 ml vials is available for use with thermostatted autosamplers The half size racks trays are not designed for an optimal heat transfer...

Страница 9: ...the next sampling sequence begins Different valves are available for the standard and preparative autosamplers Control of the vial temperature in the thermostatted autosampler is achieved using an ad...

Страница 10: ...e mainpass position at the end of the sampling sequence The sampling sequence occurs in the following order 1 The injection valve switches to the bypass position 2 The plunger of the metering device m...

Страница 11: ...obile phase flows through the autosamplers metering device sample loop and needle ensuring all parts in contact with sample are flushed during the run thus minimizing carry over Figure 2 Mainpass Posi...

Страница 12: ...ple loop Figure 4 on page 12 Figure 4 Drawing the Sample When the metering unit has drawn the required volume of sample into the sample loop the needle is raised and the vial is replaced in the sample...

Страница 13: ...blies needle drive metering device and injection valve The sampling units for the standard and the preparative autosamplers are different Figure 6 Autosampler Sampling Unit NOTE The replacement sampli...

Страница 14: ...ndle to linear motion The drive nut pushes the sapphire plunger against the tension of the spring into the analytical head The base of the plunger sits on the large bearing of the drive nut which ensu...

Страница 15: ...ction valve Two microswitches monitor switching of the valve bypass and mainpass end positions No valve adjustments are required after replacing internal components Table 2 Injection Valve Technical D...

Страница 16: ...of the gripper assembly for sample vial transport The rotational movement of the motors is converted to linear motion X and Z axes by toothed belts connected to the drive spindles The rotation theta a...

Страница 17: ...position errors automatically e g if the gripper is accidentally moved out of position when loading vials into the vial tray The initialization positions of the moving components are sensed by reflec...

Страница 18: ...re monitors the usage of specific components in the instrument and provides feedback when the user setable limits have been exceeded The visual feedback in the user interface provides an indication th...

Страница 19: ...ilent Technologies if you want to use features such as start stop common shut down prepare and so on With the appropriate software the RS 232C connector may be used to control the module from a comput...

Страница 20: ...tion to the Autosampler Electrical Connections Figure 8 Autosampler plus Thermostat Electrical Connections E 7 GH 8 86C Wjh GZbdiZ K Va cjbWZg djieji GZaVn XdciVXih 8dccZXi dc 6AH I ZgbdhiVi 7 I Zgbdh...

Страница 21: ...tector RI Detector Thermostatted Column Compartment Vacuum Degasser CAN Yes Yes Yes Yes Yes No GPIB Yes Yes Yes Yes Yes No RS 232C Yes Yes Yes Yes Yes No APG Remote Yes Yes Yes Yes Yes Yes Analog Yes...

Страница 22: ...22 1 Introduction to the Autosampler Agilent 1200 Infinity Interfaces...

Страница 23: ...gilent Technologies 2 Site Requirements and Specifications Site Requirements 24 Power Consideration 24 Power Cords 25 Bench Space 26 Environment 26 Physical Specifications 27 Performance Specification...

Страница 24: ...and the thermostat G1330B Both modules have a separate power supply and a power plug for the line connections The two modules are connected by a control cable and both are turned on by the autosampler...

Страница 25: ...can be easily reached and unplugged Provide sufficient space behind the power socket of the instrument to unplug the cable WARNING The absence of ground connection and the use of an unspecified power...

Страница 26: ...d in a level position If a complete Agilent 1200 Infinity Series system is to be installed on the bench make sure that the bench is designed to carry the weight of all the modules For a complete syste...

Страница 27: ...0 55 C 32 131 F See warning on page 27 Ambient non operating temperature 40 70 C 4 158 F Humidity 95 at 25 40 C 77 104 F Non condensing Operating Altitude Up to 2000 m 6500 ft Non operating altitude...

Страница 28: ...fety features Leak detection and safe leak handling low voltages in maintenance areas error detection and display Injection range 0 1 100 l in 0 1 l increments Up to 1500 l with multiple draw hardware...

Страница 29: ...voltages in maintenance areas error detection and display Injection range 0 1 900 l in 0 1 l increments recommended 1 l increments Up to 1800 l with multiple draw hardware modification required Repli...

Страница 30: ...voltages in maintenance areas error detection and display Injection range 0 1 100 l in 0 1 l increments recommended 1 l increments Up to 15 00 l with multiple draw hardware modification required Repli...

Страница 31: ...es in maintenance areas error detection and display Injection range 0 1 900 l in 0 1 l increments recommended 1 l increments Up to 1800 l with multiple draw hardware modification required Up to 5000 l...

Страница 32: ...32 2 Site Requirements and Specifications Performance Specifications...

Страница 33: ...ing the Autosampler 34 Damaged Packaging 34 Delivery Checklist 34 Optimizing the Stack Configuration 37 Installing the Autosampler 41 Installing the Thermostatted Autosampler 44 Flow Connections 48 In...

Страница 34: ...inspection Delivery Checklist Ensure all parts and materials have been delivered with the autosampler The instrument box contains the instrument and an Accessory kit A separate box contains the refer...

Страница 35: ...ction sheet no PN Wrenches 1 4 5 16 inch 8710 0510 Rheotool socket wrench 1 4 inch 8710 2391 Hex key 4 mm 15 cm long T handle 8710 2392 Hex key 9 64 inch 15 cm long T handle 8710 2394 Hex key 2 5 mm 1...

Страница 36: ...Wrenches 1 4 5 16 inch 8710 0510 Rheotool socket wrench 1 4 inch 8710 2391 Hex key 4 mm 15 cm long T handle 8710 2392 Hex key 9 64 inch 15 cm long T handle 8710 2394 Hex key 2 5 mm 15 cm long straight...

Страница 37: ...shown in Figure 9 on page 37 and Figure 10 on page 38 Figure 11 on page 39 and Figure 12 on page 40 show the configuration recommended for a thermostatted autosampler These configurations optimize the...

Страница 38: ...ampler Optimizing the Stack Configuration Figure 10 Recommended Stack Configuration for an Autosampler Rear View GZbdiZ XVWaZ 86C 7jh XVWaZ 68 edlZg 86C 7jh XVWaZ id chiVci E adi 6cVad h cVa id gZXdgY...

Страница 39: ...ptimizing the Stack Configuration Figure 11 Recommended Stack Configuration for a thermostatted ALS Front View 9Z VhhZg 6AH I ZgbdhiVi 9ZiZXidg chiVci E adi Ejbe HiVcYVgY dg EgZeVgVi kZ 6jidhVbeaZg Hd...

Страница 40: ...timizing the Stack Configuration Figure 12 Recommended Stack Configuration for a thermostatted ALS Rear View 86C Wjh XVWaZ 6cVad h cVa id gZXdgYZg A6C id A8 8 ZbHiVi dc 6cVad h cVa id gZXdgYZg 6jidhVb...

Страница 41: ...ies e g shock hazard when the module cover is opened and the instrument is connected to power Never perform any adjustment maintenance or repair of the module with the top cover removed and with the p...

Страница 42: ...t the power cable to the power connector at the rear of the sampler 7 Connect the CAN cable to the other Agilent 1200 Infinity modules 8 If an Agilent Chemstation is the controller connect either The...

Страница 43: ...f the sampler Figure 14 Cable Connections E 7 GH 8 86C Wjh GZbdiZ K Va cjbWZg djieji GZaVn XdciVXih 86C XVWaZ id egZk djh bdYjaZ NOTE If the front cover is not installed the autosampler is in a not re...

Страница 44: ...t the module can lead to personal injuries e g shock hazard when the module cover is opened and the instrument is connected to power Never perform any adjustment maintenance or repair of the module wi...

Страница 45: ...correctly engaged in the Thermostat locks WARNING Personal injury To avoid personal injury keep fingers away from the needle area during Autosampler operation Do not attempt to insert or remove a vial...

Страница 46: ...r and the Thermostat see Figure 17 on page 47 10 Connect the power cables to the power connectors 11 Connect the CAN cable to the other Agilent 1200 Infinity modules 12 If an Agilent ChemStation is th...

Страница 47: ...47 Installing the Autosampler 3 Installing the Thermostatted Autosampler Figure 17 Cable Connections E 7 GH 8 GZbdiZ K Va cjbWZg djieji GZaVn XdciVXih I ZgbdhiVi 6jidhVbeaZg XVWaZ 86C Wjh...

Страница 48: ...kit Preparations Sampler is installed in the LC system WARNING Toxic and hazardous solvents The handling of solvents and reagents can hold health risks When opening capillary or tube fittings solvents...

Страница 49: ...49 Installing the Autosampler 3 Flow Connections Figure 18 Hydraulic Connections 8dajbc XdbeVgibZci caZi XVe aaVgn LVhiZ ijWZ c AZV X VccZa HdakZci lVhiZ dg Xdggj ViZY lVhiZ ijWZ Ejbe djiaZi XVe aaVgn...

Страница 50: ...ide the sample tray into the autosampler so that the rear of the sample tray is seated firmly against the rear of the sample tray area 4 Press the front of the sample tray down to secure the tray in t...

Страница 51: ...r location via carrier ensure The transport assembly is parked The vial tray is secured If the autosampler is to be shipped to another location the transport assembly must be moved to the park positio...

Страница 52: ...52 3 Installing the Autosampler Transporting the Autosampler...

Страница 53: ...53 Agilent Technologies 4 Using the Autosampler Solvent Information 54 Sample Trays 56 Choice of Vials and Caps 58...

Страница 54: ...vents e g Acetonitrile or Methanol 5 Solvents Brown glass ware can avoid growth of algae Always filter solvents small particles can permanently block the capillaries Avoid the use of the following ste...

Страница 55: ...iltered through dry aluminium oxide which adsorbs the peroxides Solutions of organic acids acetic acid formic acid and so on in organic solvents For example a 1 solution of acetic acid in methanol wil...

Страница 56: ...als to be used simultaneously Table 11 Supported trays for the Autosampler G1329A G2260A Description Part Number Tray for 100 x 2 ml vials G1313 44510 Halftray for 15 x 6 ml vials G1313 44513 Halftray...

Страница 57: ...ys the numbering convention is slightly different The vial positions of the right hand half tray begin at position 101 as follows Left hand 40 position tray 1 40 Left hand 15 position tray 1 15 Right...

Страница 58: ...cessfully tested using a minimum of 15 000 injections with the Agilent 1200 Infinity autosampler Table 12 Crimp Top Vials Description Volume ml 100 Pack 1000 Pack 100 Pack silanized Clear glass 2 5181...

Страница 59: ...scription Septa 100 Pack Silver aluminum Clear PTFE red rubber 5181 1210 Silver aluminum Clear PTFE red rubber 5183 4498 1000 Pack Blue aluminum Clear PTFE red rubber 5181 1215 Green aluminum Clear PT...

Страница 60: ...Blue polypropylene Clear PTFE red rubber 5182 0717 Green polypropylene Clear PTFE red rubber 5182 0718 Red polypropylene Clear PTFE red rubber 5182 0719 Blue polypropylene Clear PTFE silicone 5182 072...

Страница 61: ...ted Needle Wash 63 Using an Injector Program 64 General Recommendation to Lowest Carry over 65 Fast Injection Cycle and Low Delay Volume 66 Overlapped Injection Mode 66 General Recommendations for Fas...

Страница 62: ...ss of the injection valve is always in the flow line These parts are continuously flushed during an isocratic and also during a gradient analysis The residual amount of sample remaining on the outside...

Страница 63: ...best results the wash vial should contain solvent in which the sample components are soluble and the vial should not be capped If the wash vial is capped small amounts of sample remain on the surface...

Страница 64: ...the bypass grove is filled with the start concentration of the mobile phase Otherwise the separation could be influenced especially if microbore columns are used For example Outside wash of needle in...

Страница 65: ...In case the needle seat has got contaminated and carry over is significantly higher than expected the following procedure can be used to clean the needle seat Go to MORE INJECTOR and set needle to hom...

Страница 66: ...waits with switching to mainpass until the actual run is finished You gain the sample preparation time when using this process Switching the valve into the bypass position reduces the system delay vol...

Страница 67: ...erlapped injection is used To reduce the injection time the detector balance has to be set to OFF NOTE For the last injection of the sequence with overlapped injections it has to be considered that fo...

Страница 68: ...the mobile phase is adequately degassed Also using the automated needle wash see Optimization for Lowest Carry over on page 62 between injections reduces carry over to a minimum further improving the...

Страница 69: ...igher value speeds up the injection cycle by shortening the time the metering unit requires to eject solvent at the beginning of the injection cycle when the plunger returns to the home position An EJ...

Страница 70: ...etime of the Vespel seal is drastically reduced a seal made of Tefzel is available Tefzel is more resistant than Vespel to extremes of pH however is a slightly softer material Under normal conditions...

Страница 71: ...71 Agilent Technologies 6 Troubleshooting and Diagnostics Agilent Lab Monitor Diagnostic Software 72 Overview of the Sampler s Indicators and Test Functions 73...

Страница 72: ...Infinity HPLC modules This includes tests and calibrations procedures as well as the different injector steps to perform all the maintenance routines Agilent Lab Advisor also allows users to monitor t...

Страница 73: ...event of an electronic mechanical or hydraulic failure the instrument generates an error message in the user interface For details on error messages and error handling please refer to the Agilent Lab...

Страница 74: ...74 6 Troubleshooting and Diagnostics Overview of the Sampler s Indicators and Test Functions...

Страница 75: ...ating the Firmware 77 Warnings and Cautions 78 Using the ESD Strap 78 Cleaning the module 79 Overview of Main Repair Procedures 80 Early Maintenance Feedback EMF 82 EMF Counters 82 Using the EMF Count...

Страница 76: ...removing the autosampler from the stack removing the covers and disassembling the autosampler Safety Flap Flex Board It is strongly recommended that the exchange of the safety flap and flex board is d...

Страница 77: ...Firmware The Agilent 1200 Infinity LC modules are fitted with FLASH EPROMS These EPROMS enable you to update the instrument firmware from the ChemStation PCMCIA card or through the RS232 interface The...

Страница 78: ...to recommendations given by the supplier WARNING Module is partially energized when switched off as long as the power cord is plugged in Repair work at the module can lead to personal injuries e g sh...

Страница 79: ...ith water or a solution of water and mild detergent Do not use an excessively damp cloth as liquid may drip into the module WARNING Liquid dripping into the electronic compartment of your module Liqui...

Страница 80: ...80 7 Maintenance Overview of Main Repair Procedures Overview of Main Repair Procedures Figure 21 Main Assemblies...

Страница 81: ...epair Procedures 1 Power supply 2 ASM board 3 Transport assembly 4 Metering seal Metering Seal and Plunger on page 98 5 Needle Needle Assembly on page 86 6 Rotor seal Rotor Seal on page 94 7 Needle se...

Страница 82: ...been exceeded The visual feedback in the user interface provides an indication that maintenance procedures should be scheduled EMF Counters The autosampler provides two EMF counters Each counter incre...

Страница 83: ...ions of the instrument Setting the EMF Limits The setting of the EMF limits must be optimized over one or two maintenance cycles Initially no EMF limit should be set When instrument performance indica...

Страница 84: ...ions Certain maintenance procedures require the needle arm metering device and gripper assembly to be moved to specific positions to enable easy access to components The maintenance functions move the...

Страница 85: ...nutes See Needle Assembly on page 86 Exchanging the seat assembly When the seat shows indication of damage or blockage 10 minutes See Needle Seat Assembly on page 89 Exchanging the rotor seal After ap...

Страница 86: ...87103 needle seat 1 G1313 87202 Needle assembly 900 l loop cap for G1313 87101 needle seat 1 G2260 87201 Needle assembly 900 l loop cap for G2260 87101 needle seat Preparations Select Start in the ma...

Страница 87: ...til the needle screw is aligned with the hole in the safety cover 2 Remove the sample loop fitting from the needle fitting 3 Loosen the fixing screw and lift out the needle 4 Insert the new needle Ali...

Страница 88: ...the needle fitting 6 Use Needle Up to lift the needle to a position approximately 2mm above the seat 7 Ensure the needle is aligned with the seat Next Steps 8 On completion of this procedure Install...

Страница 89: ...y 0 17 mm i d 2 3 l for G1329A B 1 G1313 87103 Needle seat assy 0 12 mm i d 1 2 l for G1329A B 1 G2260 87101 Needle seat assy 0 50 mm i d 20 l for G2260A Preparations Select Start in the maintenance f...

Страница 90: ...o port 5 of the injection valve 5 Use Down to position the needle approximately 2 mm above the seat 6 Ensure the needle is aligned with the seat If required bend the needle slightly until the needle i...

Страница 91: ...329B functionality part of stator head 1 0101 1268 Stator face for G2260A Preparations Remove the front cover Remove the leak tubings if necessary CAUTION Removing the stator head The stator face is h...

Страница 92: ...e in place on the stator head Ensure the pins on the stator engage in the holes in the stator head 5 Install stator head and stator face Tighten the bolts alternately two turns at a time until the sta...

Страница 93: ...93 Maintenance 7 Simple Repairs 7 Slide the waste tube into the waste holder in the leak tray 8 On completion of this procedure Install the front cover...

Страница 94: ...al Vespel for G1329A 1 0100 1849 Rotor seal Tefzel for G1329A 1 0101 1416 Rotor seal PEEK for G1329B 1 0101 1268 Rotor seal PEEK for G2260A Preparations Remove front cover Remove the leak tubing if ne...

Страница 95: ...Remove all capillary fittings from the injection valve ports 2 Loosen each fixing bolt two turns at a time Remove the bolts from the head 3 Remove the stator head stator face and stator ring 4 Remove...

Страница 96: ...ards the valve body 6 Install the stator ring with the short of the two pins facing towards you at the 12 O Clock position Ensure the ring sits flat on the valve body 7 Place the stator face in place...

Страница 97: ...7 Simple Repairs 9 Reconnect the pump capillaries to the valve ports see Figure 18 on page 49 10 Slide the waste tube into the waste holder in the leak tray 11 On completion of this procedure Install...

Страница 98: ...pack of 2 for 100 l analytical head 1 Metering seal pack of 1 for 900 l analytical head 1 5063 6586 Metering plunger for 100 l analytical head 1 5062 8587 Metering plunger for 900 l analytical head on...

Страница 99: ...base of the metering head assembly 4 Disassemble the metering head assembly 5 Use a small screwdriver to carefully remove the seal Clean the chamber with lint free cloth Ensure all particular matter...

Страница 100: ...ully insert the plunger into the base The closed side of the metering head must be on the same side as the lower one of the two capillary drillings 9 Install the fixing bolts Tighten the bolts securel...

Страница 101: ...101 Maintenance 7 Simple Repairs 11 Reinstall the capillaries Next Steps 12 On completion of this procedure Install the front cover 13 Select End in the maintenance function Change piston...

Страница 102: ...13 60010 Gripper assembly Preparations Select Start in the maintenance function ChangeGripper Turn off the power to the autosampler Remove the front cover 1 Identify the slit below the gripper motor a...

Страница 103: ...ill be blocked 4 Hold the paper clip in place press the gripper release button and rotate the gripper arm to the right 5 The gripper arm will come off 6 Replace the gripper arm by holding the paper cl...

Страница 104: ...ce Board When At installation or when defective Tools required Flat head screwdriver Parts required Description 1 Interface board CAUTION Electronic boards are static sensitive and should be handled w...

Страница 105: ...al Trays 111 Standard Autosampler Accessory Kit G1329 68725 112 Preparative Autosampler Accessory Kit G2260 68705 113 Maintenance Kit G1313 68730 for G1329A 114 Maintenance Kit G1313 68719 for G1329B...

Страница 106: ...106 8 Parts and Materials for Maintenance Main Assemblies Main Assemblies Figure 23 Autosampler Main Assemblies...

Страница 107: ...ion valve assembly for G2260A 0101 0921 0101 1422 0101 1267 5 Vial tray thermostatted see Vial Trays on page 111 G1329 60011 6 Gripper assembly G1313 60010 7 Illumination assembly G1367 60040 8 Autosa...

Страница 108: ...em Description Part Number Analytical head assembly includes items 1 6 01078 60003 1 Plunger assembly 5063 6586 2 Screw M4 40 mm lg for mounting of assembly 0515 0850 3 Adapter 01078 23202 4 Support s...

Страница 109: ...109 Parts and Materials for Maintenance 8 Analytical Head Assembly Figure 24 Analytical Head Assembly cdi h dlc...

Страница 110: ...y 900 l G1313 27700 7 Screw M5 60 mm lg for mounting of assembly not shown here 0515 2118 Table 22 Preparative Head Assembly 900 l for G2260A Item Description Part Number Preparative head assembly 900...

Страница 111: ...ler Vial Trays and Tray Base Item Description Part Number 1 Adapter air channel G1329 43200 2 Tray for 100 2 ml vials thermostattable G1329 60011 3 Spring G1313 09101 4 Tray base for G1329A G1329B G22...

Страница 112: ...e screw caps 100 pk 5182 0717 Label halftray no PN Vial instruction sheet no PN Wrenches 1 4 5 16 inch 8710 0510 Rheotool socket wrench 1 4 inch 8710 2391 Hex key 4 mm 15 cm long T handle 8710 2392 He...

Страница 113: ...182 0717 Label halftray no PN Wrenches 1 4 5 16 inch 8710 0510 Rheotool socket wrench 1 4 inch 8710 2391 Hex key 4 mm 15 cm long T handle 8710 2392 Hex key 9 64 mm 15 cm long T handle 8710 2394 Hex ke...

Страница 114: ...nce Kit G1313 68730 for G1329A Maintenance Kit G1313 68730 for G1329A Table 26 Maintenance Kit for G1329A Item Description Part Number 1 Rotor seal Vespel 0100 1853 2 Needle assembly 100 l G1313 87201...

Страница 115: ...Maintenance Kit G1313 68719 for G1329B Table 27 Maintenance Kit for G1329A Item Description Part Number 1 Rotor seal PEEK 0101 1416 2 Needle assembly 100 l G1313 87201 3 Needle seat assembly 0 17 mm G...

Страница 116: ...G1313 6871 Multi Draw Kit G1313 6871 Table 28 Multi Draw Kit for G1329A and G1329B Item Description Part Number 1 Seat capillary 500 l 0 5 mm id G1313 87307 2 Seat capillary 1500 l 0 9 mm id G1313 87...

Страница 117: ...63A for G1329A 900 l Injection Upgrade Kit G1363A for G1329A Table 29 900 l Injection Upgrade Kit for G1329A only Item Description Part Number 1 Analytical Head 900 l G1313 60007 2 Loop Extension 900...

Страница 118: ...18 8 Parts and Materials for Maintenance External Tray G1313 60004 External Tray G1313 60004 Table 30 External Tray Item Description Part Number 1 External tray G1313 60004 2 Disposal tube G1313 27302...

Страница 119: ...119 Agilent Technologies 9 Identifying Cables Cable Overview 120 Analog Cables 122 Remote Cables 125 BCD Cables 130 External Contact Cable 132 CAN LAN Cables 133 Auxiliary Cable 134 RS 232 Cables 135...

Страница 120: ...390 integrator 01046 60203 3392 3 integrators 01046 60206 3394 integrator 01046 60210 3396A Series I integrator 03394 60600 3396 Series II 3395A integrator see details in section Remote Cables on page...

Страница 121: ...1100 1200 module to ChemStation 1 m Agilent 1100 1200 module to ChemStation 2 m 10833A 10833B RS 232 cable Agilent 1100 1200 module to a computer This kit contains a 9 pin female to 9 pin female Null...

Страница 122: ...0 1200 Infinity modules The other end depends on the instrument to which connection is being made Agilent Modules to 3390 2 3 Integrators Connector 01040 60101 Pin 3390 2 3 Pin Agilent module Signal N...

Страница 123: ...94 6 Integrators Agilent Modules to BNC Connector Connector35900 60750 Pin 3394 6 Pin Agilent module Signal Name 1 Not connected 2 Shield Analog 3 Center Analog Connector8120 1840 Pin BNC Pin Agilent...

Страница 124: ...124 9 Identifying Cables Analog Cables Agilent Modules to General Purpose Connector01046 60105 Pin 3394 6 Pin Agilent module Signal Name 1 Not connected 2 Black Analog 3 Red Analog...

Страница 125: ...inity modules The other end depends on the instrument to be connected to Agilent Modules to 3390 Integrators Connector 01046 60203 Pin 3390 Pin Agilent module Signal Name Active TTL 2 1 White Digital...

Страница 126: ...t Low NC 4 Blue Shut down Low NC 5 Pink Not connected NC 6 Yellow Power on High 9 7 Red Ready High 1 8 Green Stop Low NC 9 Black Start request Low Connector01046 60210 Pin 3394 Pin Agilent module Sign...

Страница 127: ...integrator prints START not ready NOTE START and STOP are connected via diodes to pin 3 of the 3394 connector Connector03394 60600 Pin 3394 Pin Agilent module Signal Name Active TTL 9 1 White Digital...

Страница 128: ...t Low NC 4 Blue Shut down Low NC 5 Pink Not connected NC 6 Yellow Power on High 14 7 Red Ready High 4 8 Green Stop Low NC 9 Black Start request Low 13 15 Not connected Connector5061 3378 Pin HP 1050 P...

Страница 129: ...wn Prepare run Low 4 3 Gray Start Low 7 4 Blue Shut down Low 8 5 Pink Not connected NC 6 Yellow Power on High 3 7 Red Ready High 6 8 Green Stop Low NC 9 Black Start request Low Connector01046 60201 Pi...

Страница 130: ...to Agilent Modules to General Purpose Connector G1351 81600 Wire Color Pin Agilent module Signal Name BCD Digit Green 1 BCD 5 20 Violet 2 BCD 7 80 Blue 3 BCD 6 40 Yellow 4 BCD 4 10 Black 5 BCD 0 1 Or...

Страница 131: ...ilent Modules to 3396 Integrators Connector03396 60560 Pin 3392 3 Pin Agilent module Signal Name BCD Digit 1 1 BCD 5 20 2 2 BCD 7 80 3 3 BCD 6 40 4 4 BCD 4 10 5 5 BCD0 1 6 6 BCD 3 8 7 7 BCD 2 4 8 8 BC...

Страница 132: ...gilent Modules Interface Board to general purposes Connector G1103 61611 Color Pin Agilent module Signal Name White 1 EXT 1 Brown 2 EXT 1 Green 3 EXT 2 Yellow 4 EXT 2 Grey 5 EXT 3 Pink 6 EXT 3 Blue 7...

Страница 133: ...LAN connectors CAN Cables LAN Cables Agilent 1200 module to module 0 5 m 5181 1516 Agilent 1200 module to module 1 m 5181 1519 Agilent 1200 module to control module G1323 81600 Description Part number...

Страница 134: ...ug to be connected to the Agilent 1100 Series vacuum degasser The other end is for general purpose Agilent 1200 Infinity Series Degasser to general purposes Connector G1322 81600 Color Pin Agilent mod...

Страница 135: ...kit 9 to 9 pin female and one adapter 9 pin male 25 pin female Suited for instrument to PC 34398A Cable Printer Serial Parallel is a SUB D 9 pin female vs Centronics connector on the other end NOT FO...

Страница 136: ...136 9 Identifying Cables RS 232 Cables...

Страница 137: ...137 Agilent Technologies 10 Appendix General Safety Information 138 Lithium Batteries Information 142 Radio Interference 143 Sound Emission 144 Agilent Technologies on Internet 145...

Страница 138: ...of design manufacture and intended use of the instrument Agilent Technologies assumes no liability for the customer s failure to comply with these requirements General This is a Safety Class I instrum...

Страница 139: ...ts described in the manual are made with power supplied to the instrument and protective covers removed Energy available at many points may if contacted result in personal injury Any adjustment mainte...

Страница 140: ...rking with solvents please observe appropriate safety procedures e g goggles safety gloves and protective clothing as described in the material handling and safety data sheet by the solvent vendor esp...

Страница 141: ...ult from directly viewing the light produced by the deuterium lamp used in this product The apparatus is marked with this symbol when hot surfaces are available and the user should not touch it when h...

Страница 142: ...to national waste disposal regulations for batteries Replace only with the same or equivalent type recommended by the equipment manufacturer WARNING Lithiumbatteri Eksplosionsfare ved fejlagtig h ndte...

Страница 143: ...n against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscreened cables or used for measureme...

Страница 144: ...s provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position 70 dB Sound Pressure Lp 70 dB A...

Страница 145: ...ogies on Internet For the latest information on products and services visit our worldwide web site on the Internet at http www agilent com Select Products Chemical Analysis It will provide also the la...

Страница 146: ...121 133 remote 120 125 RS 232 121 135 cables overview 120 CAN cable 133 capillaries 48 choice of vials and caps 68 cleaning 79 condensation 26 D damaged packaging 34 34 delay volume 51 58 58 delay 51...

Страница 147: ...ve seal 68 low volume capillary kit 68 maintenance 68 optimizing performance bypassing the autosampler 58 low volume capillary kit 58 minimizing delay volume 51 58 58 P park transport assembly 34 park...

Страница 148: ...fications 28 34 stack configuration 38 40 rear view 38 40 standard autosampler accessory kit contents 35 stator 15 status indicator 73 step functions 73 stepper motor 14 T temperature 28 theta axis 16...

Страница 149: ...149 Index...

Страница 150: ...al contains user information about the Agilent 1260 Infinity Preparative Autosampler The manual describes the following introduction to the autosampler site requirements and specifications installing...

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