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ProStar 701 Fraction Collector Control Manual

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03-914947-27:2

Table of Contents

Introduction.............................................................................................. 2

General ................................................................................................................................2

Installation and Configuration................................................................ 3

Installing the Driver Software...............................................................................................3

Configuring the Communication Server...............................................................................3

Configuring the Driver..........................................................................................................4

Configuring the Varian ProStar 701 Fraction Collector.................................................4

Configuring the Synopsis ..............................................................................................5

Building a Method ................................................................................... 7

Creating a New Method .......................................................................................................7

Control Method Section for the Varian ProStar 701 Fraction Collector.............................10

Collector Parameters Control......................................................................................12

Fraction Collector Mode Control .................................................................................14

Rack Control ...............................................................................................................17

Collection Chain Control .............................................................................................19

Starting and Viewing an Acquisition.................................................... 21

Quick Start and Sequence.................................................................................................21

Quick Start (Single Acquisition) ..................................................................................21

Sequence ....................................................................................................................23

Running Acquisition Status................................................................................................24

Viewing a Running Acquisition....................................................................................24

Status of the Varian ProStar 701 Fraction Collector...................................................24

Summary of Contents for ProStar 701

Page 1: ...Varian Inc 2700 Mitchell Drive Walnut Creek CA 94598 1675 USA Varian Inc 2005 03 914947 27 Rev 2 ProStar 701 Fraction Collector Control Galaxie Driver Manual...

Page 2: ...r 4 Configuring the Synopsis 5 Building a Method 7 Creating a New Method 7 Control Method Section for the Varian ProStar 701 Fraction Collector 10 Collector Parameters Control 12 Fraction Collector Mo...

Page 3: ...oduction General This document describes the configuration of the Varian ProStar 701 Fraction Collector driver It also explains how to build a control method for this driver how to start and view a ru...

Page 4: ...erver To communicate with the ProStar 701 module an RS232_Interface or an RS232_PC communication bus must be configured on the acquisition server The parameters of the bus to must be the following Sto...

Page 5: ...ng the Varian ProStar 701 Fraction Collector Click on the button corresponding to the Varian ProStar 701 Fraction Collector driver and the configuration screen appears Communication Window Select from...

Page 6: ...system name in the bottom part of the Galaxie Configuration Manager screen A pop up menu appears click on Stop Then right click on the system name again and click on Start 3 Go back to the System Con...

Page 7: ...the installed devices For example the following pictures represent the synopsis of the Varian ProStar 701 Fraction Collector Galaxie Configuration Manager Screen Galaxie Chromatography Data System Sc...

Page 8: ...ting of final results To initially set up a method it is not necessary to define all of the sub method sections however you must fill in the instrument control section prior to starting an acquisition...

Page 9: ...method is created for a particular system When starting an acquisition the name of the system that performs the acquisition must be correct since method access is limited only to those methods associa...

Page 10: ...matography Data System The next step is the definition of each of the method sections The instrument control section must be defined in order to start an acquisition In the following part of this guid...

Page 11: ...d Once the new method is created select the control section in the lower part of the browser The following screen appears Press the button to display the System Control Method Advanced Tools window to...

Page 12: ...s and Collection Chain Click on the required sub section to define the corresponding parameters that will be used during the chromatographic run The toolbar allows you to easily scroll through the con...

Page 13: ...t the way the fraction size is defined None no collection Time fraction size based on time Drop fraction collection by drop Note that some parameters of the other sub sections will be activated or may...

Page 14: ...Collection Mode sub section The values run from 0 to 3559 sec Define in the Collection Option list where the peaks and non peaks are sent Peaks Rack1 2 Non peaks Valve Peaks Rack1 2 Non peaks Drain Pe...

Page 15: ...e determined Time peaks are determined by time The Fraction Windows table is activated The user has to determine the time size of each fraction Slope peaks are sensed by their rate of change of signal...

Page 16: ...or OR Time If AND Time is selected the peak will only be collected when both a time window is active and the slope or level detection conditions are met If OR Time is selected the peak will be collect...

Page 17: ...dows this table has to be filled if the Time mode of collection is activated User has to define the fraction time sizes Up to 25 lines can be defined Use the following buttons to edit the table to add...

Page 18: ...k field is automatically filled in The value displayed by default in the Tubes Rack field is the maximum tubes available in the rack this value can be reduced by the user In the Fraction Size field en...

Page 19: ...available for Rack 2 Bottles 9 Beaker 1 Custom 256 Use of a rectangular rack with max 16 rows and 16 tubes per row User has to define the first and last tube position ProStar 701 Fraction Collector w...

Page 20: ...nd collect fractions in same tubes all the fractions 1 of the X samples are sent in the same tube all the fractions 2 of the X samples are sent in the same tube where X is the Overlay Number In the Ov...

Page 21: ...e last fraction of the first injection and the first fraction of the second injection are dropped in consecutive tubes Next Row the collector return to a new row between two consecutive injections Ski...

Page 22: ...ol method has been correctly programmed an analysis can be started The next section briefly describes how to start an acquisition Quick Start Single Acquisition 1 Press the button In the Quick Start w...

Page 23: ...Data System the Injection Volume the Vial position and the Rack number if required must be entered Other parameters associated with each acquisition channel can be entered in the Channel X tab 3 Clic...

Page 24: ...ber of samples and the sequence name 2 The sequence is displayed Complete the sequence information columns refer to the Galaxie Chromatography Data System User s Guide The Method Name the Run Name the...

Page 25: ...the status window where the driver modules are listed Varian ProStar 701 Fraction Collector Status Click on the button corresponding to the ProStar 701 Fraction Collector driver and the fraction coll...

Page 26: ...e user defines the rack and the tube positions where the collector has to move to If selecting the button the collector moves to its initial position moves to the following tube moves to the next rack...

Page 27: ...send the solution in the Drain waste or to collect it in tubes this allows the user to work in local or to take the control of the ProStar 701 Fraction Collector via Galaxie Remote If an acquisition i...

Page 28: ...this button stops the fraction collection User can stop and start again the collection during an acquisition the log will be created according these stop start actions Note that when performing colle...

Page 29: ...914947 27 2 The buttons available in the right part of the Overview part have the same functions as in the Status window Not Ready no information is listed Events contains the communication state bet...

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