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Introduction

ARL  EQUINOX  X-Ray  diffractometers  are  designed  for  measuring  of  crystalline  samples  (powder,
bulk,  metals,  thin  layers,  etc...),  phase  identification,  nanoscale  structural  analysis,  non-destructive
quality control, as well as for many other applications.

Thermo  Fisher  Scientific  develops  and  sells  many  sample  holders  that  can  be  plugged  in  Thermo
Fisher  Scientific  diffractometers  in  order  to  analyze  the  samples.  The  sample  holders  sometimes
consist of moving parts and electronics which are needed for more complex devices to control sam-
ple's movement.

All ARL EQUINOX instruments are shipped with a basic non-spinning sample holder suited for pow-
der measurement in reflection mode. This sample holder is necessary for adjustment and alignment
and can be used for measurement of samples as well.

This instrument is intended for professionals. The user is advised to read the following instructions
and any other additional information supplied by Thermo Fisher Scientific before operating the instru-
ment.

Thermo Fisher Scientific declines all responsibilities for improper use by unauthorized personnel or
non-authorized operation of the instrument.

For any additional information, contact Thermo Fisher Scientific.

Supplied Items

Before the shipment, the sample holders are tested and packed carefully. However damage can oc-
cur during the transport.

If  the  sample  holder  or  any  additional  supplied  item  has  been  damaged  during  transport,  or  if  you
notice  any  signs  of  a  possible  damage,  please  contact  both  the  transport  company  representative
and the Thermo Fisher Scientific representative as soon as possible.

Furthermore,  if  you  notice  that  any  part  is  missing  or  you  have  any  questions  about  the  delivered
items, contact the Thermo Fisher Scientific representative.

Storage

The storage where the instrument is stored has to meet following ambient specifications:

Temperature: 0 – 50°C, relative humidity: < 95% (without condensation).

Assistance

The  Thermo  Fisher  Scientific  worldwide  technical  support  network  consists  of  highly  trained  field
service engineers, technical support specialists and service coordinators who are ready to quickly as-
sist  the  customers  with  answers  and  solutions  to  service  needs  and  application  questions.  If  you
need any help, please contact the local Thermo Fisher Scientific representative.

Manufacturer

THERMO FISHER SCIENTIFIC INEL SAS
71 rue d’Orléans
45410 ARTENAY, FRANCE
Tel : +33(0)2-38-80-45-45

Confidential, limited rights

PN AA83871 | Revision A

SSCA Sample Holder: Instruction Notice

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Introduction

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Summary of Contents for ARL EQUINOX Series

Page 1: ...Thermo Scientific ARL EQUINOX Series SSCA Sample Holder Instruction Notice AA83871 A February 2022...

Page 2: ...to the Power Supply 4 3 Setting of the Incidence Angle 5 Sample Preparation Procedure 5 1 Preparing the Sample Outside a Glove Box 5 2 Preparing the Sample Inside a Glove Box 5 3 Preparing Sample Ins...

Page 3: ...his document is the original manual The information in this document is subject to change without notice We assume no responsibility for any errors that may appear in this document Confidential limite...

Page 4: ...nal information contact Thermo Fisher Scientific Supplied Items Before the shipment the sample holders are tested and packed carefully However damage can oc cur during the transport If the sample hold...

Page 5: ...not specified by Thermo Fisher Scientific the protection provided by the sample holder may be impaired Only accessories that comply with Thermo Fisher Scientific specifications are allowed to be used...

Page 6: ...strapping of a Kapton window on a Viton O ring and by a stainless steel belt This makes the easy replacement of the window Two rapid connectors allow to connect to the gas system like vacuum pump of...

Page 7: ...er has to be inser ted in the reference hole For more detailed information refer to the ARL EQUINOX instruction notice Connections to the Power Supply The SSCA sample holder is supplied by 12VDC The p...

Page 8: ...in the picture below The longest line represents the incidence angle equal to 0 2 Each short line represents 2 of incidence angle 4 The medium long lines represent 10 of inci dence angle 3 Then the i...

Page 9: ...he surface of the powder mount in order to avoid line displacement error due to height error Use a glass slide to make the surface flat and homogeneous Set the Kapton disk in the housing to make ease...

Page 10: ...ractometer as described above If sample does not require any further preparation then proceed as described in Preparing the Sam ple Outside a Glove Box on page 9 If the sample requires a preparation s...

Page 11: ...ing for low energy X ray it is better to replace the argon gas by heli um nitrogen or other inert acceptable gas Introduction of components inside the glove box The following figure shows the parts wh...

Page 12: ...le holder exit from the glove box Insertion of the SSCA in the ARL EQUINOX Insert the sample holder in the sample holder mounting hole of the instrument Do not use any un necessary force The sample ho...

Page 13: ...ing the sealing between the cover and the sample holder should be replaced if damaged No glue Window Ref 100421014 can be replaced if necessary Remove the 24 M3 screws Remove the Kapton foil Remove an...

Page 14: ...in ON position If the problem persists contact Thermo Fisher Scientific You observe peak shift Check your sample preparation make sure that you have right amount of powder in the cup Check the alignm...

Page 15: ...irectives EN 61010 1 2010 Safety requirements for electrical equipment for measurement control and laboratory use Part 1 General requirements 2011 65 EC restriction of the use of certain hazardous sub...

Page 16: ...ng Sample Inside a Glove Box and Gas Replacement 10 Preparing the Sample Inside a Glove Box 10 Preparing the Sample Outside a Glove Box 9 R Revision Table 3 S SSCA Sample Holder Description 5 Safety 5...

Page 17: ...ic and its subsidiaries unless otherwise specified Learn more at thermofisher com elemental or email us at info spectrometry thermofisher com Thermo Fisher Scientific Brno s r o Vlastimila Pecha 1282...

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