7
Troubleshooting
How to Know When Your System Needs Maintenance
Thermo Scientific
TSQ 8000 Evo User Guide
117
How to Know When Your System Needs Maintenance
Typically, you will notice that your instrument needs maintenance when you are analyzing
your data on the computer. Some of the most common reasons and indications are as follows:
•
Contamination
—Excessive background in your mass spectra usually indicates that your
instrument is contaminated. Use the mass spectrum in the table below to understand the
origin of the contamination. Cleaning solvent peaks usually indicate that the ion source
cartridge was installed before it completely dried.
•
Fingerprints
—A series of mass peaks in your data that are 14 amu apart usually indicates
fingerprint or other hydrocarbon contamination. To avoid fingerprints, wear clean,
lint-free gloves when performing any type of maintenance on a component in the vacuum
manifold of the instrument.
•
Air Leaks
—Higher than normal vacuum pressure or poor sensitivity usually indicates an
air leak. Check the last o-ring or ferrule that you installed.
Table 2.
Diagnostics and Corrective Actions
Diagnostic
Cause of Failure
Corrective Action
Communication
Check
Unknown
Contact your Field Service Engineer.
Frequency Check
RF Dip is not correct
Run a full tune that will correct for any RF
dip problems.
Ensure source cartridge is installed.
Contact your Field Service Engineer.
SRM Efficiency
Check
Collision gas is not
supplied correctly
Check collision gas tank and pressure.
Q1 is poorly tuned
Run an EI SRM tune (not a quick tune).
Lens Continuity
Check
Ion source not inserted
properly
Remove and reinsert ion source.
Lens plate and/or
springs are damaged
Contact your Field Service Engineer.
A wire is disconnected
or shorted inside the
manifold
Contact your Field Service Engineer.
Summary of Contents for TSQ 8000
Page 1: ...TSQ 8000 Evo Mass Spectrometer User Guide 1R120586 0002 Revision C December 2015 ...
Page 22: ......
Page 148: ......