SP Scientific FTS Systems BioCool 80 Manual Download Page 25

 

Rev 002, 08/12 

 

17 

© SP Scientific 2012 

Chapter 

Fluid 

 

 

 

 

 

Selecting a fluid or fluid mixture for use in your FTS Systems BioCool™ 80 is the 

single most important decision to be made. Always select a fluid that is appropriate for 

the temperature and/or temperature range at which you will operate your system. 

Improperly selected fluid can result in damage to both your process and your 

equipment.  

 

Refer to the following table for a list of fluids that may be used with the FTS Systems 

BioCool™ 80. 

 

CAUTION: BEFORE USING ANY FLUID PRODUCT, READ THE CURRENT 

PRODUCT MATERIAL SAFETY DATA SHEET AND ANY PRECAUTIONARY 

STATEMENTS ON THE PRODUCT PACKAGE. FOLLOW ALL APPLICABLE 

PRECAUTIONS AND DIRECTIONS. 

Recommended Fluid and Selected Properties 

Fluid 

Temperature Range 

Flammability 

Toxicity 

Dielectric 

Methanol 

-80 to 20 °C 

Medium 

Low 

Low 

 

Fluid Filling 

While operating at or above ambient temperature (approximately 22 °C (72 °F)), fill 

the reservoir with your selected fluid until the fluid is about 1 inch below the gasket. 

 

If you add fluid while the system is at a sub-ambient temperature and you fail to drain 

fluid before returning the system to room temperature, the fluid may expand and 

overflow the fluid reservoir.  

Notes:

 Fluids will typically contract when cooled and expand when heated.  

The gasket at the top of the fluid reservoir does not provide a liquid tight seal.  

 

If the fluid reservoir chamber is overfilled, the liquid will flow over the rim of the fluid 

reservoir into the polyurethane insulation. Organic solvents will attack, dissolve and/or 

render ineffective the chamber insulation. When the insulation is saturated with 

solvent, the BioCool™ 80 may be unable to reach its maximum low temperature. 

 

IF THE RESERVOIR IS OVERFILLED, THE FLUID MAY OVERFLOW THE 

RESERVOIR RIM AND SEEP INTO THE POLYURETHANE INSULATION. ORGANIC 

SOLVENTS WILL ATTACK AND DAMAGE THIS INSULATION MATERIAL, 

RENDERING THE INSULATION INEFFECTIVE. WITHOUT ADEQUATE 

INSULATION, THE BIOCOOL™ 80 WILL NOT REACH MAXIMUM LOW 

TEMPERATURES.

 

 

 

 

Summary of Contents for FTS Systems BioCool 80

Page 1: ...LOW TEMPERATURE BATH OPERATOR S MANUAL FTS SYSTEMS BIOCOOL 80 Controlled Rate Freezing Bath...

Page 2: ......

Page 3: ...ion of dissemination of modifications to or the creation of derivative works from this Low Temperature Bath Operator s Manual by any means and in any form or manner is expressly prohibited except with...

Page 4: ...RECOMMENDATIONS STREAMLINE UNIT OPERATION AND PREVENT COMMON OPERATOR ERRORS WEAR SAFETY GLASSES EXPLOSIVE MATERIALS HAZARD KEEP OBJECTS AWAY FROM HEAT Safety Warnings Always transport the unit with...

Page 5: ...t or repair of parts pursuant to this warranty shall not in any way extend the original warranty period The Company shall not be responsible for any unauthorized repairs replacements or product modifi...

Page 6: ...iv Rev 002 08 12 SP Scientific 2012...

Page 7: ...tion 6 Air Flow Considerations 6 Ambient Conditions 6 Services and Utilities 6 Installing the Magnetic Stirrer and Vortex Breaker 7 Operation 9 Overview 9 Operation 9 Powering On 9 The Solo Controller...

Page 8: ...r 19 Bath System 19 Compressor Safeties 20 Refrigerant Types and Properties 20 Refrigeration System 20 Voltage 20 Accessories 21 Straw Rack Model SR 36 21 Ampule Rack Model SR 12 21 Ampule Rack Model...

Page 9: ...provide more accurate temperature control and uniformity Each configuration features an air cooled refrigeration system and stainless steel reservoir THE FLUID AND INNER WALLS OF THE RESERVOIR CAN RE...

Page 10: ...e BioCool also features the Solo microprocessor controller which provides precise temperature control within 0 1 C across the temperature control range of 80 C to 20 C 1 When powered on the BioCool 80...

Page 11: ...buzzer which is located on the back of the unit The buzzer will sound at the end of a program run notifying the operator that the run has completed Note For additional information about the buzzer inc...

Page 12: ...Introduction FTS Systems BioCool 80 4 Rev 002 08 12 SP Scientific 2012...

Page 13: ...If concealed damage or loss is discovered contact the freight carrier immediately 2 Keep all contents packing material and related paperwork intact until a written report is obtained Note SP Scientif...

Page 14: ...oper airflow and avoid damage to the refrigeration system Ambient Conditions For best low temperature operation consider that the ideal ambient temperature for your FTS Systems BioCool 80 is approxima...

Page 15: ...oses only and are intended to be removed prior to operation Place the magnetic stirrer magnet side down into the center of the reservoir 2 Pushing the edges of the stirring mechanism beyond the black...

Page 16: ...xtended to the same length this will keep the stirrer assembly centered in the bath Hold the vortex breaker by its metal handle a small tab bent 90 at the tip 4 and place it into the reservoir so that...

Page 17: ...tures within 0 1 C across the equipment s full operating temperature range Operation Powering On Note Before powering on and cooling install the magnetic stirrer and vortex breaker as described in Cha...

Page 18: ...Set Value SV Display Displays the desired fluid temperature Adjusting Bath Temperature Press the Up and or Down buttons to increase and decrease the fluid 1 temperature shown on the SV Display Press...

Page 19: ...ientific s Solo Controller operator s manual THE THREE SAMPLE PATTERNS THAT COME LOADED ON YOUR BIOCOOL 80 WERE DESIGNED FOR DEMONSTRATION PURPOSES SP SCIENTIFIC DOES NOT RECOMMEND USING THESE PATTERN...

Page 20: ...rts at 22 C and holds soaks at that temperature for 10 minutes The temperature then ramps from 22 C to 6 C in 15 minutes This results in a ramp rate of 1 9 C m A temperature of 6 C is then held soaked...

Page 21: ...amp from 7 C to 33 C over the next 52 minute period results in a ramp rate of 0 5 C m The last step is set to 3 eliminating the execution of any values programmed in the remaining steps Note The syste...

Page 22: ...in 11 minutes and then soaks at 5 for 30 minutes A ramp from 5 C to 30 C over the next 84 minute period results in a ramp rate of 0 3 C m The pattern ramps at 0 1 C m down to 35 over a period of 50 m...

Page 23: ...thermal variations SP Scientific recommends setting the Fluid Stir control dial to its maximum speed at all times for optimal operation and performance Note Do not operate the magnetic stirrer withou...

Page 24: ...Operation FTS Systems BioCool 80 16 Rev 002 08 12 SP Scientific 2012...

Page 25: ...ly 22 C 72 F fill the reservoir with your selected fluid until the fluid is about 1 inch below the gasket If you add fluid while the system is at a sub ambient temperature and you fail to drain fluid...

Page 26: ...been properly filled with fluid The magnetic stirrer must be on for the system to operate properly Refer to the magnetic stirrer operation section of the previous chapter for additional information No...

Page 27: ...ing a stiff bristled brush Blown compressed air such as the type used to dust computers may also be used to clean the fins A buildup of dust or debris on the fins of the condenser will cause a reducti...

Page 28: ...voltage or high temperatures If the voltage drops below what is required for the compressor to operate an overcurrent device turns the compressor off If the compressor temperature rises too high due t...

Page 29: ...eds Unit should run with all 3 black Delrin racks in place even if 36 straws are not being processed This will help prevent condensation of water vapor If liquid nitrogen chilled forceps are being use...

Page 30: ...The ampule rack shall accommodate 15 ampules ranging from 2 ml to 5 ml The disks of the rack can be moved up or down to accommodate different ampule sizes Loosen the nuts on either side of the rack to...

Page 31: ...he setting value It is also used to navigate between function modes The Rotate button is used to change parameters within each function mode Push the SET button and then push the Rotate button until y...

Page 32: ...S Systems BioCool 80 24 Rev 002 08 12 SP Scientific 2012 Lock the controller Press the Rotate Button to until LoC i e appears 7 in the display Press either the Down or Up arrow button until Loc2 i e a...

Page 33: ...stage compressor from starting within several minutes of a loss of power intentional or unintentional e g power switched off facility power outage loss of main power etc Magnetic stirrer does not rota...

Page 34: ...Appendix B Troubleshooting FTS Systems BioCool 80 26 Rev 002 08 12 SP Scientific 2012...

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Page 36: ...Main Street Stone Ridge NY 12484 USA 800 251 1531 845 687 0071 935 Mearns Road Warminster PA 18974 USA 800 523 2327 215 672 7800 815 State Route 208 Gardiner NY 12525 USA 800 431 8232 845 255 5000 ww...

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