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Parker ChemTec II, Installation, Operating, & Maintenance Instructions

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Parker ChemTec II Installation, Operating, & Maintenance Instructions Download Page 25

 

25 

Diafiltration programming 

From the main screen: 

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Choose SETTINGS 

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Select TUBING 

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Confirm Motor RPM and head in the Tube Settings 

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Select the TUBE SIZE from the drop down, press SET 

 

 
Steps to enter a Diafiltration Recipe: 

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Return to the main screen 

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Select the RECIPES button 

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Choose an existing recipe, or click on CREATE NEW (For this Quick Start, click on CREATE NEW) 

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Click DIAFILTRATION 

 

 

 

 

Summary of Contents for ChemTec II

Page 1: ...ENGINEERING YOUR SUCCESS ChemTec II Programmable Metering Pump Installation Operating Maintenance Instructions...

Page 2: ...f any alterations This publication is for general information only and customers are requested to contact contact your local Parker Sales Representative for detailed information and advice on a produc...

Page 3: ...a Bioreactor 19 Start up Diafiltration or Maintenance of Vessel Weight 24 Start up Simple pH Maintenance of a Base reaction 28 Front Display Back Panel Interface 33 Settings 36 ChemTec II Manual Mode...

Page 4: ...FORE INSTALLING SERVICING CLEANING OR REMOVING THE FUSE FAILURE TO DO SO COULD RESULT IN BODILY HARM AND OR PROPERTY DAMAGE CAUTION OBSERVE PRECAUTIONS FOR HANDLING ELECTROSTATIC SENSITIVE DEVICES WAR...

Page 5: ...RER LE FUSIBLE NE PAS OBSERVER CES PR CAUTIONS RISQUERAIT DE CAUSER DES BLESSURES CORPORELLES OU ET D ENDOMMAGER L QUIPEMENT PRUDENCE SOYEZ PRUDENT LORSQUE VOUS MANIPULEZ DES APPAREILS SENSIBLES L LEC...

Page 6: ...d down using a soft non fluffing cloth moistened with water If required you may also use a mild detergent or Isopropanol The SciPres II disposable sensors used with the system come pre calibrated from...

Page 7: ...ng Parker customer service will be able to serve you more efficiently if you have the following information Serial number and model name of the equipment Installation procedure being used Concise list...

Page 8: ...wer supply fuse 3 15A T20 250V Battery CR1632 used to support the internal clock only not user serviceable Motor Choice of four motors 8 160 600 and 3400 RPM at 24V 3 8 Amperes Variable Pump Speed opt...

Page 9: ...allation of the USB Driver Upon connecting the ChemTec II to the PC via the provided RS232 to USB adapter cable on the Printer Port of the ChemTec II open Control Panel then Device Manager on your PC...

Page 10: ...ur PC via an RS232 to USB adapter cable PN 080 USB This will automatically create a USB Serial Port with an assigned COM Port on Windows 10 once the drivers are downloaded off the Internet Be sure you...

Page 11: ...11 SAMPLE SciDoc II Screens...

Page 12: ...12 SAMPLE SciDoc II Exports...

Page 13: ...harts as both an xls file and a txt file Files are saved at C Serial Data Loggers by type All files can be readily turned into PDFs NOTE The charts do not adjust their range automatically You must man...

Page 14: ...t will be ready to receive data from the pump 6 If the ChemTec II and scale were purchased together from Parker both will be configured to communicate with each other If purchased separately contact P...

Page 15: ...Motor RPM and head in the Tube Settings Select the TUBE SIZE from the drop down press SET Steps to enter a Volume Flow Recipe Return to the main screen Select the RECIPES button Choose an existing rec...

Page 16: ...ed to upper and lower case letters numbers and dashes Select INSERT STEP BELOW to get started Press VOLUME FLOW RATE NOTE Start and End parameters are always listed and cannot be edited or deleted Ste...

Page 17: ...he above recipe is incorrect as it does not start with a step flow rate Highlight any of the steps and edit or delete as needed Name recipe Select SAVE RECIPE place cursor in text field From the keybo...

Page 18: ...The Volume Flow Run Screen shows the ongoing process Hit PRIME to prime tubing lines and select again to stop priming Select START to begin the process Once the process starts you can select PAUSE to...

Page 19: ...ftware from https discover parker com pump support gen2 Choose ChemTec II from the menu select the appropriate COM Port and it will be ready to receive data from the pump 7 If the ChemTec II and scale...

Page 20: ...Motor RPM and head in the Tube Settings Select the TUBE SIZE from the drop down press SET Steps to enter a Mass Flow Recipe Return to the main screen Select the RECIPES button Choose an existing reci...

Page 21: ...to upper and lower case letters numbers and dashes Select INSERT STEP BELOW to get started Press MASS FLOW RATE NOTE Start and End parameters are always listed and cannot be edited or deleted Steps c...

Page 22: ...tep to the recipe Highlight any step to edit delete as needed Click SAVE AND EXIT Name recipe Select SAVE RECIPE place cursor in text field From the keyboard type the recipe name ENTER Hit ENTER again...

Page 23: ...e tubing lines and select again to stop priming Select START to begin the process Once the process starts you can select PAUSE to interrupt the process once Pause is activated it will switch to RESUME...

Page 24: ...discover parker com pump support gen2 Choose ChemTec II from the menu select the appropriate COM Port and it will be ready to receive data from the pump 7 If the ChemTec II and scale were purchased to...

Page 25: ...otor RPM and head in the Tube Settings Select the TUBE SIZE from the drop down press SET Steps to enter a Diafiltration Recipe Return to the main screen Select the RECIPES button Choose an existing re...

Page 26: ...and maintained Select DIAFILTRATION ALARMS SETTINGS to display the following screen The DIAFILTRATION ALARMS SETTINGS screen provides the following options Low Solution Alarm High Reactor Alarm Balan...

Page 27: ...ocess Once the process starts select PAUSE once Pause is activated it will switch to RESUME Select RESUME to begin the process again from where it was first paused Select STOP to end the process If AL...

Page 28: ...ems to allow for cables and tubing 3 Connect the pH ChemTec II interface cable to the output of the pH Meter and the Analog connector on the rear of the ChemTec II 4 Connect the RS232 to USB cable bet...

Page 29: ...r the parameters of the titration maintenance process and determine how close the pH Setpoint must be maintained and the max flow rate desired for reagent addition as the pH increases Several user def...

Page 30: ...TUBING Confirm Motor RPM and head Choose the TUBE SIZE from the drop down press SET Steps to enter a pH Control Recipe Return to the main screen Choose RECIPES Select an existing recipe or click on C...

Page 31: ...iod For this process to occur once and stop as in an Endpoint Titration set the Stabilization Period to a non zero value in seconds Maximum 999 seconds As long as the pH stays within the bandwidth set...

Page 32: ...s starts select PAUSE once Pause is activated it will switch to RESUME Select RESUME to begin the process again from where it was first paused Select STOP to end the process If ALARMS is selected from...

Page 33: ...alance Male DB9 labeled S1 S2 and S3 CAN In Out Male DB9 for CAN communication cables not enabled Profibus Female DB9 for Profibus communication cable not enabled SciPres II Single Use Pressure Sensor...

Page 34: ...24 3 7 19 7 15 2 3 11 23 4 6 18 8 14 1 4 10 22 Digital Connector Pin Out DIGITAL INPUTS AND OUTPUTS These are TTL inputs and outputs This means simple contact closure all that is needed on the inputs...

Page 35: ...The relays may be closed programmatically and in Manual Mode There are also connections for 24 VDC on the 7 small pins at the bottom of each connector that can be turned on and off programmatically a...

Page 36: ...Temperature Sensor option is not supported The following outlines the options for each of the settings SCALES Select SCALES and set the type of scale to be used for Scale 1 2 or 3 Most modes on the Ch...

Page 37: ...brate the flow rate TOUCH SCREEN CALIBRATION Select CALIBRATE SCREEN and follow the on screen instructions to adjust the calibration to be responsive to your touch Choose RESET SCREEN CALIBRATION to r...

Page 38: ...alues from a UV detector the Min and Max Scaled range would be based on the output of that detector i e 0 and 2 would be typical DIGITAL CONNECTION SETTINGS This is to indicate which Digital Input Con...

Page 39: ...ssures Analog Inputs and Digital Inputs Temperature Sensors are not supported so may be ignored You may also disable all alarms at once Pressure 1 Pressure 2 Pressure 3 Configure both High and Low pre...

Page 40: ...ms are logged in red text while the unit is powered Once acknowledged they will be listed in the history list below the alarm list This data is not exportable at this time System Information From the...

Page 41: ...a minimal current The Relay screen allows the Relays to be tested there are three on each connector on the rear of the unit They are 250 V 5 Amp relays The 24 VDC screen allows one to toggle the 24 VD...

Page 42: ...n the extent of pump tube wear and the time between re calibrations In contrast mass flow metering has several advantages The most important one lies in the high precision and high accuracy levels RSD...

Page 43: ...or was used for this feed application PharMed pump tubing 16 was chosen since it can generate flow rates from 4 6 ml min to 120 ml min The following Recipe was entered into the Volu Flow mode START In...

Page 44: ...T Interpolate from 0 37 gm min to 0 50 gm min over 12 hours 30 minutes Interpolate from 0 50 gm min to 0 94 gm min over 12 hours 30 minutes Interpolate from 0 94 gm min to 1 28 gm min over 12 hours 30...

Page 45: ...45 y 0 2701e0 3114x R 1 0 0 5 1 1 5 2 2 5 3 0 12 5 25 37 5 50 62 5 75 Mass Flow Rate gm min Time hours Figure 2 Mass Flow Rate vs Time Mass flow...

Page 46: ...hoe will move in opposite directions thereby exposing the inside of the upper and lower pump shoe channels 3 With the TANDEM pump head completely opened locate the mounting holes for the two 8 32 cap...

Page 47: ...e right The tube retainer spring will automatically place the correct tension on the pump tubing to prevent tube walking With the TANDEM pump head closed lightly pull the two ends of the tubing in opp...

Page 48: ...tein molecules Materials of Construction RH series pump heads have cylinder bodies and fittings made of either Kynar or Tefzel The piston and cylinder liner are ceramic except for the RH00 models whic...

Page 49: ...of the head the T in CTC refers to Tefzel and the K in CKC refers to Kynar For applications involving fluids above 90 F do not use heads with Tefzel cylinder body material Please use either Kynar or...

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Page 55: ...is available from Parker The rotating gears of a magnetic gear pump head generate significant shear thus shear sensitive solutions should not be metered dispensed with this head Use the Tandem Perista...

Page 56: ...ed your operating system conditions and the pump model being used and how long the pump has been in service If the pump self priming capability of the magnetic gear pump heads in use has diminished or...

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Page 67: ...67 Notes...

Page 68: ...California USA 93030 toll free 877 784 2234 phone 1 805 604 3400 fax 1 805 604 3401 email bioscience na parker com www parker com bioscience Parker Hannifin Manufacturing Ltd Bioscience Filtration Du...

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