T
T
A
A
B
B
L
L
E
E
O
O
F
F
C
C
O
O
N
N
T
T
E
E
N
N
T
T
S
S
CHAPTER 1: INTRODUCTION
1
Freeze Dry Process
1
Freeze Dry Rates
2
Freeze Dry Capacity
4
Samples
Containing
Volatile
Substances
5
About This Manual
5
Typographical
Conventions
7
Your Next Step
7
CHAPTER 2: PREREQUISITES
9
Electrical Requirements
10
Location
Requirements 10
Vacuum
Pump
Requirements
10
Chamber
or
Manifold
Requirements 11
Space
Requirements
11
Your Next Step
11
CHAPTER
3:
GETTING
STARTED
13
Unpacking Your Freeze Dryer
14
Freeze
Dryer
Components
14
Setting
Up
Your
Freeze
Dryer
16
Component
Orientation 16
Vacuum
Pump
Connection 16
Electrical Connection
17
Drying Chamber or Drying Manifold Installation
17
Solvent
Safety
Precautions
17
Your Next Step
18
CHAPTER 4: USING YOUR FREEZE DRYER
19
Freeze Dryer Controls
20
Operation Checklist
22
Vacuum
Pump
Ballast
Setting
22
Purge Valve
23
Operating
the
Freeze
Dryer 24
Automatic Start-Up
24
Manual Start-Up
25