Kyoto DA-640 Operation Manual Download Page 32

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4. Calibration and Check

Hint

The criteria of determining OK or NG by Check can be
configured on “Menu”

”Check & Calibrate”.

For details, refer to the separate Function Description.

Hint

The check record is stored on “Menu”

”Data

control”

”Check data”.

For details, refer to the separate Function Description.

Summary of Contents for DA-640

Page 1: ...Density Specific Gravity Meter DA 650 DA 645 DA 640 Operation Manual Read this operation manual thoroughly before use Ver 00 A N 59 00051 01 48 ...

Page 2: ......

Page 3: ...nd 5 7 inch TFT LCD touchscreen z Easy connection to your PC through LAN z Easy transfer of measurement data to your PC with USB flash drive z Keyboard can also be connected for easy entry of sample name or numbers USB LAN ports z Free repair within one year after the date of purchase Some exceptions may apply After the sale service z The latest model of KEM s highly esteemed benchtop density spec...

Page 4: ...randy wine distilled spirit etc alcohol degree or concentration of extract is used in quality control The alcohol degree is used in taxation 5 Food Brix concentration is used in QC of food material like honeydew extracts saline solution syrup or isomerized sugar Brix is also used for QC of soy sauce cooking sauce or gravy 6 Fat and oil Density SG is used for quality control of plant oil or animal ...

Page 5: ...stallation Avoid a place under any of the following conditions to avoid malfunction Caution Under vibration Under direct sunlight Corrosive gas atmosphere Ambient humidity exceeding 85 RH Heavily loaded and fluctuated or near power source or magnetic field Excessive range of temperature other than specified Power supply Caution Do not share power as shown below Power source for this unit AC 100 24...

Page 6: ...may lower repeatability or result in measurement error as the nature of such samples can be changed by oscillation Storage Caution Use our shipping box to store the equipment Thoroughly clean and dry the measuring cell if you do not plan to use the equipment for a certain period of time Do not store where temp is extremely high or low where humidity is high or where is dusty Other cautions Caution...

Page 7: ... manual to raise your attention 1 Warning Warning This symbol means danger of possible death or severe injury 2 Note Note This symbol means the important information about the product 3 Hint Hint This symbol means technical tips for the best performance of your equipment z It is prohibited to copy a part or whole of the manual without prior consent z If you should find any ambiguous or missing des...

Page 8: ... Installation 11 2 Parts Configuration 14 3 Preparation for Measurement 19 3 1 Warming up 19 3 2 Necessary tools 20 3 3 Set up measurement conditions 21 cell temperature stability limit time 21 4 Calibration and Check 23 4 1 Calibration 23 4 2 Check Calibration 27 5 Measurement 31 5 1 Normal measurement 31 5 2 Measurement with syringe 35 6 Convenient Useful Functions 39 7 Maintenance 50 7 1 Check ...

Page 9: ...sage 56 8 2 Technical tips 59 9 Additional Information 61 9 1 Parts and consumables 61 9 2 Glossary and reference 65 9 3 Convenient and useful optional devices 76 9 4 Specifications 77 9 5 International standards 79 9 6 Index 80 9 7 Warranty and after the sale service 82 ...

Page 10: ...Measurement Procedures 8 Measurement Procedures How to measure Start measurement P 31 Before measurement Change measure condition temperature precision P 21 Check the unit P 27 Calibrate the unit P 23 ...

Page 11: ...s See 1 2 STEP 4 Prepare materials for measurement Ethanol for cleaning and drying pure water for calibration etc See 3 2 STEP 6 Calibration Follow navigation guide on display for calibration See 4 STEP 7 Measurement Now ready to measure your sample See 5 STEP 3 Warming up unit Warm up the unit for required length of time See 3 1 STEP 5 Set up measure condition Temperature stability sense limit ti...

Page 12: ...00051 00 48 1 Desiccant Container 12 01148 02 48 1 Connecting Tube 12 01997 01 48 1 For drain solenoid valve side Connecting Tube 12 01998 00 48 1 For drying Connecting Tube 12 01999 00 48 1 For drain cell outlet Connecting Tube 12 02000 00 48 1 For sampling Connecting Tube 12 02699 00 48 1 For purge gas Lure Adapter 20 05764 00 48 1 Adapter for syringe Darin Tube 20 05789 01 48 1 For pump side Op...

Page 13: ...o insert the adapter until you hear a click 3 Connect power cord z Connect the power cord to the power outlet for 3P outlet The 3P outlet contains the earth terminal wired to the ground There is no need to ground the earth for 2P outlet The 2P outlet needs grounding by adding an AC 3P adapter Ground the earth by connecting the green wire to the earth terminal on the outlet 4 Install the desiccant ...

Page 14: ...f printer is shown below Item What to do Range Default Printer Select whether use the printer or not 0 None 1 IDP 2 DP 3 Other 2 DP Interface Select where to connect printer 0 COM1 1 COM2 2 COM3 3 COM4 1 COM2 Baud rate Select digital configuration 0 2400 1 4800 2 9600 3 19200 4 38400 1 4800 Parity Select digital configuration 0 None 1 Odd 2 Even 0 None Stop bit Select digital configuration 0 0 1 1...

Page 15: ...nt is harmful the vent tube must be connected The vent tube drains out waste liquid a little so that the other end of vent tube must be placed in the waste container just like drain tube 8 Connecting drain tube z Fix the drain tube from pump unit in waste container a bottle or tank Warning Place the waste container sufficiently away from the operator in case toxic gas is generated and remains harm...

Page 16: ...ing speed can be controlled by turning the dial To drain or rinse turn it to Drain and execute at max speed When turned downward it sets in purge mode and sends dry air 5 Sampling Speed Controller Sampling speed can be controlled here It works when switching lever is in Sample position and pumping is going on When sample is highly viscous use higher intake power When viscosity is low turn it down ...

Page 17: ...ed or purple it is time to replace the silica gel 10 RS 232C Connector This port is used to connect Sample Changer or PC for data acquisition by the optional software SOFT CAP 11 USB Connector This port is for USB flash drive 12 LAN Connector This port is for PC data manipulation 13 Power Switch Power is turned On or Off by this switch 14 Power Connector AC Adapter The supplied AC adapter plug is ...

Page 18: ...ns to standby mode MENU key Setup window appears to select method sample etc See separate Function manual Note To operate the touch screen use the stylus or your finger Do not use a sharp pointed pen or pencil Otherwise the screen may be damaged or broken Hint If any part of screen other than button or two buttons are pressed at a time it beeps but is no use Touch the button securely one by one wh...

Page 19: ...nit When pressed it shows window to select the unit See 3 3 Set up measure condition Option The connected optional unit is shown here When pressed it shows peripherals to select Temperature Shows both current and setup temperature here When pressed it shows window to select measure temperature See 3 3 Set up measure condition Status Shows current condition of the event like measurement underway or...

Page 20: ... Enter characters in alphabetical letters and numbers To confirm the entry press Enter Capital or small letters can be selected Up to 16 letters numbers can be entered sample ID can accept up to 32 characters Excess characters are shown with mark Alphabetical Capital Alphabetical Small Number ...

Page 21: ...emperature and becomes stable once you turn on the equipment or when you change the cell temperature with a difference of 30 C or smaller from the previous one Required warm up time is as follows Model Warm up time DA 650 Approx 60 mins DA 645 Approx 30 mins DA 640 Approx 10 mins Ambient temperature 20 C 1 Power ON z Turn on the power The display on the right appears 2 Wait for stable cell tempera...

Page 22: ...y volatile solution that easily dissolves the rinse solution 1 When satisfactory rinse solutions 1 and 2 are not available add rinse solution 3 which can dissolve both rinse 1 and 2 used in between two steps A highly volatile solvent can be used not only as rinse solution 1 but also 2 as well Typical rinse solutions are as shown below Select as necessary for sample character Beverage Soft drink Wi...

Page 23: ...he measurement temp and press Enter 2 Select stability meas mode z Press Stability key Select stability from 0 3 normal 1 3 Select limit time z Select a limit time of measurement When it exceeds the limit time measurement is aborted with results on display Range 0 9999 sec 0 means infinite which does not abort measurement Hint For other details of setup press Menu Method For details refer to the s...

Page 24: ...ime is very short but deviation is sharp Level 2 Fast Oscillation frequency is predicted where temperature of sample and cell differs from each other to some extent Measuring time is short but deviation is substantial Level 1 Normal Oscillation frequency is predicted where temperature of sample and cell is close to each other This mode is typical and standard since accurate results can be expected...

Page 25: ...and water is necessary whenever a change occurs on the equipment such as installation place cell temperature etc Calibration is simple and easy Just follow Calibration Navigator 1 Select Calibration z Press Calibration z Press Next You will see a message Dry meas cell When Check Calibration Press Check Press Calibration Navigator 2 Clean measuring cell Rinse 2 z Make sure the sample drain lever is...

Page 26: ...ment beeps A message of Start water calib will appear 5 Sampling of pure water z Adjust sample drain lever to Sample z Adjust sampling speed controller to slowest scale 0 z Press PUMP to start sampling of pure water z Slowly turn the controller until you reach optimal speed for sampling Do not stop turning the controller abruptly Doing so may generate air bubbles in the sample z Check through cell...

Page 27: ...ration Once completed equipment beeps 7 Print out calibration results Once calibration is completed equipment beeps and main screen as shown on the right appears Then calibration results and factors will be printed out Printout example of calibration results Failed is shown when calibration fails ...

Page 28: ...n the cell with rinse 2 for about 10 sec z Once completed press PUMP to stop pump operation Hint For quick cell cleaning when rinsing the cell suck air and water alternately by detaching sampling tube from water at intervals 9 Dry the cell z Wipe off sampling tube with waste cloth and put it in drying tube z Press PURGE twice A message of Auto drying will appear and equipment starts to dry the cel...

Page 29: ... Press Next A message of Dry the cell will appear When no Check button MENU Æ Check Calibration Æ Check Calibration Setup Æ Calibration Setup Then turn ON Check Before Calib 2 Clean the cell rinse 2 z Make sure sample drain lever is on Drain z Wipe off tip of sampling tube with waste cloth z Put the tube in rinse 2 ethanol or acetone z Press PUMP to clean the cell with rinse 2 for about 10 sec z O...

Page 30: ...rain lever to Sample z Adjust sampling speed controller to slowest scale 0 z Press PUMP to start sampling of pure water z Slowly turn the controller until you reach optimal speed for sampling Do not stop turning the controller abruptly Doing so may generate air bubbles in the sample z Check through cell window to make sure there is no air bubble in the cell z Press PUMP again to stop sampling 5 Ch...

Page 31: ...s on Drain z Wipe off tip of sampling tube with waste cloth z Put the tube in rinse 2 ethanol or acetone z Press PUMP to clean the cell with rinse 2 for about 10 sec z Once completed press PUMP to stop pump operation 8 Dry the cell z Wipe off sampling tube with waste cloth and put it in drying tube z Press PURGE twice A message of Auto drying will appear and equipment starts to dry the cell Once c...

Page 32: ...f determining OK or NG by Check can be configured on Menu Check Calibrate For details refer to the separate Function Description Hint The check record is stored on Menu Data control Check data For details refer to the separate Function Description ...

Page 33: ...ling tube with waste cloth z Put the tube in rinse 2 ethanol or acetone z Press PUMP to clean the cell with rinse 2 for about 10 sec z Once completed press PUMP to stop pump operation Hint For quick cell cleaning when rinsing the cell suck air and water alternately by detaching sampling tube from water at intervals 2 Dry the cell z Wipe off sampling tube with waste cloth and put it in drying tube ...

Page 34: ...g Hint Be careful when sampling speed is increased abruptly e g scale 0 Æ 5 air bubbles may be formed Hint For a series of measurements of the same sample continue sampling at the same speed For a different type of sample start sampling by adjusting speed first 4 Start measurement z Press START A message of Measuring will appear 5 Measurement ends z Once oscillation frequency becomes stable measur...

Page 35: ...in sample z Adjust sample drain lever to Drain z Remove sampling tube from sample z Press PUMP to drain sample 7 Clean the cell rinse 1 z Make sure sample drain lever is on Drain z Wipe off tip of sampling tube with waste cloth z Put the tube in rinse 1 pure water or toluene z Press PUMP to clean the cell with rinse 1 for about 10 sec z Once completed press PUMP to stop pump operation ...

Page 36: ...tube z Press PURGE twice A message of Auto drying will appear and equipment starts to dry the cell Once completed equipment beeps and pump stops running Hint For continued measurements For self cleaning repeat step 3 to 6 For cleaning each time repeat step 3 to 9 Hint For those samples liable to form air bubble slow down the sampling speed and suck in excessive sample liquid for successful measure...

Page 37: ...s on Drain z Wipe off tip of sampling tube with waste cloth z Put the tube in rinse 2 ethanol or acetone z Press PUMP to clean the cell with rinse 2 for about 10 sec z Once completed press PUMP to stop pump operation 2 Dry the cell z Wipe off sampling tube with waste cloth and put it in drying tube z Press PURGE twice A message of Auto drying will appear and equipment starts to dry the cell Once c...

Page 38: ...er put tip of drain tube in tube holder beforehand z Check through cell window to make sure there is no air bubble in the cell 4 Start measurement z Press START Measuring message appears 5 Measurement ends z Once oscillation frequency becomes stable measurement comes to an end and result density of sample will be shown Result will be printed out when printer is connected Note To cancel hold of dis...

Page 39: ...as the following example 6 Drain sample z Remove syringe from sample inlet z Wipe off taint around sample inlet with tissue Hint For better cleaning the cell first suck in sample liquid in cell with syringe 7 Drain sample z Put drain tube in sampling pump z Put sampling pump in sample inlet z Adjust sample drain lever to Drain z Press PUMP to drain sample ...

Page 40: ... tip of sampling tube with waste cloth z Put the tube in rinse 2 ethanol or acetone z Press PUMP to clean the cell with rinse 2 for about 10 sec z Once completed press PUMP to stop pump operation 1 0 Dry the cell z Wipe off sampling tube with waste cloth and put it in drying tube z Press PURGE twice A message of Auto drying will appear and equipment starts to dry the cell Once completed equipment ...

Page 41: ...rinse sequence etc By creating Method for each sample the sample is measured effectively You can select method files and register copy or delete them Also you can edit conditions of stored method files For most frequently measured samples like oil and Brix the appropriate methods are provided and stored as standard To use standard methods see 6 5 4 Industry Segments 6 1 1 Selection of method entry...

Page 42: ...istered sample file You can select register copy or delete sample file 6 2 4 Auto mode Auto mode is effective when selected for sample mode Useful with barcode reader See 6 9 4 Barcode reader Barcode reader can call for method name and file user name etc 6 2 5 Concentration scan This mode creates working curve for concentration from density or SG Concentration table relation of concentration to de...

Page 43: ...ocessed on PC 6 3 2 Calibration Record You can view 10 years record of calibration changes of oscillation frequency in graph and check past 20 data files print or save in USB flash drive which can be manipulated on PC 6 3 3 Check Record You can view 10 years record of check changes of oscillation frequency in graph and check past 20 data files print or save in USB flash drive which can be manipula...

Page 44: ...an value SD or RSD when sample number high order or method is changed These values can be easily batch processed by the auto computation and printed out 6 4 3 Recalculation You can select conditions and sort out recalculate concentration conversion formula or print out data both at present and in the past 6 4 4 Statistics You can batch calculate data to obtain mean value SD and RSD This is useful ...

Page 45: ...these functions A unique feature is the white LED of high intensity for those sample liquids which may be affected under normal lighting To customize sound refer to 6 8 7 6 5 3 International Selection of language from English Japanese or additional language Notation of date and temperature unit Celsius or Fahrenheit and air pressure for calibration are user s choice 6 5 4 Industry Segments Those m...

Page 46: ...of logon function allows user to use the equipment with password for logon off or key lock on off Logon function is option Once logon is significant a password is required each time a different user works on the unit 6 6 3 Logoff Logoff can be made by a user who has a password To change the operator the function of logon and logoff is required 6 6 4 Auto Logoff The unit turns off automatically whe...

Page 47: ...n is unable Here you select calibration 6 7 2 Alarm Setup This function alarms the operator about calibration check You can select on or off of alarm and due time for calibration check 6 7 3 Calibration Setup Calibration usually uses air and water but density standard liquid of which density is known can also be used Here you select sample normally air and water and measure condition for calibrati...

Page 48: ...xt time onward Those items are Method Sample Concentration conversion Sequence User Report Sound and Language 6 8 1 Method The purpose of method is to simplify measurement setup by grouping measuring conditions including measure temperature stability rinse sequence etc Method file is registered selected copied or deleted here Measuring conditions in file can also be edited The most frequently used...

Page 49: ...or recorded in memory The user of unit is registered selected copied or deleted and appears on display and printout User with password can lock or unlock unit and customize background and font colours of display for easy identification 6 8 6 Report Report function selects print format among from Off Short GLP and Custom When customize form is chosen it can be stored with an individual name Thus re...

Page 50: ...r identifies vials on changer rack 6 9 2 Cell When the external cell is connected you can measure a sample at different temperature at a time You have to wait for temperature equilibrium without it External cell is made to order 6 9 3 Printer Other than standard supplied printer various types of printer are available All of them are conformed to GLP GMP 6 9 4 Barcode When the optional barcode read...

Page 51: ...d purge can be selected and executed 6 10 1 DCU When the optional auto sampling unit DCU 600 is connected to density meter DCU can be operated on display screen of density meter Change nozzle position sampling rinse and purge can be activated 6 10 Control 6 10 2 Rinse Purge When the optional auto sampling unit DCU 551 DCU 600 or multiple sample changer CHD 502 is connected the event of rinse and p...

Page 52: ...surement Check item Daily Periodic Criteria Auto scanning Yes Yes When the power is turned on the opening message appears without error When an error should be found refer to 8 1 Troubleshooting Check Calibration Yes Yes Oscillation by check calibration does not change for a time the same direction It may change with corrosive liquid strong alkali or hydrofluoric acid in contact See 4 Calibration ...

Page 53: ...een measured and labeled must be within specified range Viscosity correction Yes When density standard e g JS100 JS500 is measured with viscosity correction the difference of results from label must be within specified range Daily Periodic check list after measurement Check item Daily Periodic Criteria Cell cleaning Yes Yes The cell must be clean after rinsed and dried See 3 2 Preparation Waste li...

Page 54: ...tion laboratory in the field of density The number 0115 is the JCSS accreditation number assigned to our density standard liquid laboratory JCSS accredited calibration laboratories are assessed on JIS Q 17025 2000 ISO IEC 17025 1999 JCSS accredited density standard liquids can be used to guarantee the quality of calibration on oscillating type density meters The Density Standard Liquid Laboratory ...

Page 55: ...er and pull out the filter 1 Replace the filter z Push and open the cover z Clean or change the filter Replacement of silica gel When blue grains of silica gel turn to pink purple or red replace the silica gel with new one Or you can dry the old one so as to reuse it 1 Discard the old silica gel z Take out the old one from container 2 Fill out new one z Put your finger on top of vent hole not to a...

Page 56: ...d one end of tube joint and pull it toward you As the arrow indicates the way how it is removed Rotor Pump tube cassette Pump tube Tube joint 3 Apply grease z Apply the supplied grease around the new tube and axle of cassette Apply grease Pump tube Axle of rotor 4 Fit pump tube z Fit the new pump tube onto the rotor To fit draw the rotor toward you as shown in figure The tube joint must be pushed ...

Page 57: ...e the fitting z Remove tube nozzle Connect the tube nozzle Connect the nozzle as shown below 1 Connect the nozzle z Insert tube nozzle z Tighten screw A z Tighten screw B and C 2 Connect lock nut and adapter z Fix the adapter with lock nut tentatively z Put on seal washer z Put on wave washer z Tighten the adapter joint with lock nut z Tighten lock nut Note Do not tighten the adapter nut and lock ...

Page 58: ...have been defective Turn off and turn on the equipment Still the same error occurs contact your local distributor 3 Sensor error detected Contact your local agent Code E 2xxx Hardware may have been defective Turn off and turn on the equipment Still the same error occurs contact your local distributor 4 Calibration required Calibration may have not been conducted Conduct a calibration 5 Calibrate w...

Page 59: ...art temp scan Check temp scan table The error appears if wrong concentration scanning has been set in Review the temperature scan table as below More than 2 points for linear more than 3 for quadratic more than 4 for cubic equation Communication with sample changer when connected may have failed Check if communication cable is properly connected Also check setting of communication port CHD 502 is ...

Page 60: ...tion is finished 13 X days left until periodic check The message appears when the due date is approaching Check or calibrate now and you can cancel the alarm The message will disappear When day interval is changed it will be effective only after check or calibration is finished 14 Periodic Check Today The alarm appears when it is the day of periodic check or calibration Check or calibrate now and ...

Page 61: ...y be solidified Raise cell temperature to the same level as sample Concentration distribution may not be even in viscous sample e g sucrose Carefully stir sample liquid to equalize concentration Repeatability of separated liquid is not stable The result is unstable When the solvent does not dissolve in sample liquid measurement result may not be stable with contaminated measuring cell Change the s...

Page 62: ...perature and humidity are high e g 35 C 85 RH and the cell temperature is low e g 15 C the cell window may mist Blow dry air through the air intake vent for about 10 minutes Hint If the problem with density measurement persists even after the above countermeasure taken contact your local distributor Dry air intake vent ...

Page 63: ...r sampling Connecting Tube 12 02699 00 48 1 For purge gas Rubber Cover 20 05748 00 48 1 For sample opening Lure Adapter 20 05764 00 48 1 Adapter for syringe Drain Tube 20 05789 01 48 1 For pump side Protective Rubber 20 05915 00 48 1 Round for sample opening Operation Manual CD ROM 12 02845 00 48 1 Incl Operation Manual Function Description Quick Manual Quick Manual 59 00053 01 48 1 12 02833 01 48...

Page 64: ...atrix Printer AC 100V 12 02028 00 48 1 Incl connecting cables 9P 25P MiniDIN8P DSUB9P Dot Matrix Printer AC 120V 12 02028 01 48 1 Incl connecting cables 9P 25P MiniDIN8P DSUB9P Dot Matrix Printer AC 230V 12 02028 02 48 1 Incl connecting cables 9P 25P MiniDIN8P DSUB9P Connecting Cable 9P 9P 12 02012 00 48 1 Connecting Cable 9P 25P 12 02013 00 48 1 Connecting Cable MiniDIN8P DSUB9P 64 00625 00 48 1 ...

Page 65: ...e bottle each Viscosity liquid 100 61 00028 00 48 0 855 Pure water viscosity liquid 100mPa s one bottle each Viscosity liquid 200 61 00029 00 48 0 861 Pure water viscosity liquid 200mPa s one bottle each Viscosity liquid 500 61 00030 00 48 0 871 Pure water viscosity liquid 500mPa s one bottle each Viscosity liquid 2000 61 00031 00 48 0 879 Pure water viscosity liquid 2000mPa s one bottle each Each...

Page 66: ...9 Additional Information 64 Hint Ethanols of 45 to 100 are also available Contact your local distributor for details ...

Page 67: ...y measuring the frequency of weight in cubic if the cubic volume is constant When the measuring is vibrated in a chamber filled with liquid or gas its oscillation frequency differs from density of sample Suppose T is oscillation frequency T can be expressed as follows K Mc dVc T π 2 Where d Density of sample in cell Vc Volume of sample that is cell volume Mc Mass of measurement cell K Constant Vc ...

Page 68: ...ration liquid reference measurement of highly viscous sample would turn out to be higher than true value The effect of viscosity when measured is as follow Low viscosity liquid water Japanese sake whisky less than 5mPa s The effect 0 0001g cm3 or less Viscous liquid olive oil tomato juice engine oil 5 1000mPa s The effect 0 0001 0 0008g cm3 High viscosity liquid honey mayonnaise hair conditioner o...

Page 69: ...on 67 DA 650 645 640 Flow chart of oscillation type density meter DA 6xx series DA 6xx series features shortened drying time and free selection of waste container by providing drying pump A P and sampling pump P P separately ...

Page 70: ...ed as Bx The unit is or degree Brix is used to express sucrose concentration sugar content in those industries like foods winery sugar and fruit farm Usually they use the scale for density of sucrose at 20 C converted to weight percent concentration w w Sucrose solution of weight percent 30 100g solution contains 30g sucrose and 70g water is expressed as Brix 30 Generally Brix is known as the meas...

Page 71: ...by French scientist A Baume expressed as Be Heavy Baume s degree is for SG larger than 1 Heavy Baume s degree 1 SG 15 4 C 1 144 3 Light Baume s degree SG unit measured by Baume s hydrometer by French scientist A Baume expressed as Be Light Baume s degree is for SG smaller than 1 Light Baume s degree 1 SG 15 4 C 1 144 3 10 Japanese sake degree It is the unit for SG of sake used as the measure to te...

Page 72: ...d from the following equation API degree 141 5 G 131 5 Where G is mass of crude oil at 60 F 15 56 C and shows ratio of mass of the same volume of water at 60 F Crude oil varies in quality from place to place where produced Some oil contains mostly gasoline some mostly heavy oil or those easily solidified or none solidified Dwaddell degree Unit for SG of dye Water at 4 C is the reference 0 Dwaddell...

Page 73: ...ccurate instrument less uncertainty If this process of searching calibration continues finally it reaches the national standard When the accuracy of a measuring instrument can be traced back to the national or international standard it is called traceable When the reference substance used in the analytical instrument is traceable the instrument can be defined as traceable to national standard Dens...

Page 74: ...8 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 0 00118 0 00118 0 00118 0 00117 0 00117 0 00116 0 00116 0 00116 0 00115 0 00115 0 00115 0 00114 0 00114 0 00113 0 00113 0 00113 0 00112 0 00112 0 00112 0 00111 0 00111 0 00111 0 00110 0 00110 0 00110 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 0 00109 0 00109 0 00109 0 00108 0 00108 0 00108 0 00107 0 00...

Page 75: ...25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 0 0012 0 0012 0 0012 0 0012 0 0012 0 0012 0 0012 0 0012 0 0012 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 0011 0 001...

Page 76: ...403 0 99368 0 99333 0 99297 0 99259 0 99222 0 99183 0 99144 0 99104 0 99063 0 99021 0 98979 0 98936 0 98893 0 98848 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 0 98804 0 98758 0 98712 0 98665 0 98617 0 98569 0 98521 0 98471 0 98421 0 98371 0 98320 0 98268 0 98216 0 98163 0 98109 0 98055 0 98000 0 97945 0 97890 0 97833 0 97776 0 97719 0 97661 0 97603 0 97544 75 76 77 ...

Page 77: ...0 9947 0 9944 0 9940 0 9937 0 9933 0 9930 0 9926 0 9922 0 9918 0 9914 0 9910 0 9906 0 9902 0 9898 0 9894 0 9889 0 9885 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 0 9880 0 9876 0 9871 0 9866 0 9862 0 9857 0 9852 0 9847 0 9842 0 9837 0 98312 0 9827 0 9822 0 9816 0 9811 0 9806 0 9800 0 9795 0 9789 0 9783 0 9778 0 9772 0 9766 0 9760 0 9754 75 76 77 78 79 80 81 82 83 84 ...

Page 78: ...out results Thermal Printer DP 600 Dot Matrix Printer IDP 100 Multiple Sample Changer CHD 502N 30 samples Auto measurement cleaning Auto Clean and Sampling Unit DCU 551N DCU 600 DA 650 DA 645 DA 640 Operation from your PC Measurement data transfer to your PC ƒf ƒ Žû W ƒ ƒtƒg ƒE ƒF ƒA Title SOFT CAP KYOTO ELECTRON ICS Data Capture Software SOFT CAP Contact your local distributor for details ...

Page 79: ...y including measurement parameters density auto correction concentration conversion etc Stability Four modes of stability according to measurement accuracy and time Density Auto Correction 1 Saves conversion table or formula at your desired temperatures according to your samples 2 Temperature conversion table preprogrammed according to ASTM standard for petroleum petroleum products and lubricating...

Page 80: ... 6 W 14 3 D 10 7 H inches Weight 18 kg 39 7 lbs Export Packing in Double Carton Box G W 21 kg 540 W 480 D 460 H mm May vary in some cases G W 46 3 lbs 21 3 W 18 9 D 18 1 H inches 1 2 According to KEM standard measurement conditions 3 Enquire for applicable models ...

Page 81: ...nsation Table for Petroleum Products U S A JIS K 2249 Japan ASTM D 4052 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter U S A ASTM D 5002 Standard Test Method for Density and Relative Density of Crude Oils by Digital Density Analyzer U S A ISO 12185 Crude petroleum and petroleum products Determination of density Oscillating U tube method International ISO ...

Page 82: ...bles 61 Control 49 D Daily check 50 Data management 41 Density 68 Density of dry air 72 Density of pure water 74 Dimensions 78 Dot Matrix Printer 12 dustproof filter 53 Dwaddell degree 70 E Entry 46 Error message 56 Ethanol degree 69 Exceptions 82 Extract 70 F Flow chart 67 Function 42 G Glossary 65 H Hint 5 I International standards 79 ISO 9001 52 J Japanese sake degree 69 JCSS 52 L limit time 21...

Page 83: ...ion 3 20 RSD 71 S Sample 40 Security 44 Setup 43 SG 68 silica gel 53 Specifications 77 stability 21 22 Standard Deviation 71 Standard Liquid 52 63 Supplied parts 10 syringe 35 T Technical tips 59 Thermal Printer 12 tools 20 Touchscreen 17 Traceability 71 U Uncertainty 71 Unpack the carton 10 V viscosity correction 66 Viscosity Liquid 63 W Warm up 19 Warning 3 5 Warranty 82 Warranty period 82 ...

Page 84: ...an authorized service personnel 2 Used under the condition or in a range other than specified 3 Operated in a way other than instructed in manual or help 4 Caused by user s misuse or careless operation 5 Due to user s inadequate environmental condition 6 Attributed to fire earth quake lightning God s act 7 Maker will not be liable for any damage or loss whether physically or monetary caused by the...

Page 85: ...102 0074 Japan Ph 81 3 3239 7333 Fax 81 3 3237 0537 URL http www kyoto kem com Factories 56 2 Ninodan cho Shinden Kisshoin Minami ku Kyoto 601 8317 Japan Ph 81 75 691 4122 Fax 81 75 691 9961 74 Ninodan cho Shinden Kisshoin Minami ku Kyoto 601 8317 Japan Ph 81 75 691 4121 Fax 81 75 691 4127 ...

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