jenway 7310 Operating Manual Download Page 80

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Spectrum

Single less than icon - decrease the wavelength by 1 times scan interval

Spectrum

Double greater than icon - increase the wavelength by 10 times scan

interval

Spectrum

Single greater than icon - increase the wavelength by 1 times scan

interval

Spectrum

Wavelength icon - manually enter the wavelength

Spectrum

Add points to the spectral points analysis table

Spectrum

View spectral points analysis table

Spectrum

Data point interval – used in print setup

Quantitation

Measure sample

Quantitation

Quantitation table – Opens quantitation table

Quantitation

Number of standards

Quantitation

View standard curve

Quantitation

Curve fit – enables the curve fit to be adjusted

Quantitation

Sigma icon – Displays curve statistics

Quantitation

Create new standard curve

Quantitation

Tick icon - Read Standard

Quantitation

Back icon – Re-measure previous standard

Quantitation

Cross icon – Cancel creation of new standard curve

Quantitation

Curve statistics – used in print setup

Kinetics

Settings menu

Kinetics

Hand icon – Manual y-axis scaling

Kinetics

Hand icon with cross through it - Auto y-axis scaling

Kinetics

0000s

Start time pause – Opens lag time/start on level menu

Kinetics

000

000 - Resets lag time, standard or factor values to zero

Kinetics

Clock icon - Set the lag time

Kinetics

ABS/%T icon - Set the start on level

Kinetics

Greater than - Start above

Kinetics

Less than - Start below

Kinetics

No start on level set

Summary of Contents for 7310

Page 1: ...Spectrophotometers Models 7310 7315 Operating Manual 731 005 REV D 06 10 ...

Page 2: ......

Page 3: ... those items defined in the maintenance procedures herein there are no user serviceable items in this instrument Removal of covers and attempted adjustment or service by unqualified personnel will invalidate the warranty and may incur additional charges for repair 4 References should always be made to the Health and Safety data supplied with any chemicals used Generally accepted laboratory procedu...

Page 4: ...setup 19 4 2 Time and date 20 4 3 Instrument settings menu 20 4 4 Security and setting passwords 21 4 4 1 Setting security codes 21 4 4 2 Settings lock 21 4 4 3 Method lock 21 4 5 Mode selection 22 4 6 Diagnostics 22 4 7 GLP settings 22 4 8 Screen contrast 23 4 9 Lamp save 23 SECTION 5 Photometrics 25 5 1 Mode specific parameters 25 5 2 Method set up 25 5 2 1 Selecting a wavelength 26 5 3 Calibrat...

Page 5: ...oints analysis 36 SECTION 8 Quantitation 38 8 1 Mode specific parameters 38 8 2 Method setup 39 8 2 1 Selecting a wavelength 39 8 2 2 Quantitation table 39 8 2 2 1 Selecting number of standards 39 8 2 2 2 Selecting concentration units 39 8 2 2 3 Changing the resolution 40 8 2 2 4 Selecting absorbance or transmittance 40 8 2 2 5 Adding standards 40 8 2 3 Standard curve 40 8 2 3 1 Creating a new sta...

Page 6: ...g results 57 10 8 Autologging 58 10 8 1 Setting the number of sample repetitions 58 10 8 2 Selecting result s destination 59 10 9 Connecting to a PC 59 SECTION 11 Accessories and spare parts 60 11 1 Optional accessories 60 11 2 Connecting the accessories 60 11 2 1 Internal printer 60 11 2 2 Passive accessories 61 11 2 3 Active accessories 61 11 2 3 1 Automatic 8 cell turret 62 11 2 3 2 Peltier 62 ...

Page 7: ...odule replacement 71 12 3 Service 72 SECTION 13 Troubleshooting 73 13 1 Error codes 73 13 2 Troubleshooting guide 75 13 3 Technical support 75 SECTION 14 Declaration of conformity 76 SECTION 15 Glossary of icons 78 Index 85 ...

Page 8: ...y 1 T 0 01Abs at 1 000 Absorbance Resolution 0 1 T 0 001A Stray light 0 5 at 340nm 0 5 at 340nm and 220nm Stability 0 002Abs hr after 30 minute warm up 0 001Abs hr without warm up Concentration Range 300 to 9999 Resolution Selectable 1 0 1 0 01 0 001 Calibration Blank with a single standard or factor Units no units ppm EBC SRM mEq l mEq M mM µM nM U U l U ml g l mg l µg l ng l g dl mg dl µg dl mg ...

Page 9: ... Light source Tungsten halogen lamp Xenon lamp Lamp save Yes Not applicable GLP Current time and date user ID settings lock and method lock Number of users 999 Methods memory 48 in each measurement mode Results memory Limited by attached mass storage device Removable media USB supplied Outputs USB Analogue RS232 Internal printer Power 24V Size w x d x h 275 x 400 x 220mm Weight 6kg ...

Page 10: ...NMANCD 8 Optional accessories as ordered 2 2 INSTALLATION Models 7310 and 7315 are supplied ready to use The unit should be placed on a clean flat surface which is free from drafts and vibrations The units are designed for operation on 90V to 264V AC input at 47 to 63Hz Select the correct plug attachment and attach to the power supply unit as shown below Fig 2 2 1 Power supply unit with various pl...

Page 11: ...ck port and the instrument 2 3 DISPLAY These spectrophotometers have a dot matrix display which enables icons and graphs to be displayed clearly Following successful completion of the power on tests the main menu screen will be displayed Fig 2 3 1 Display 1 Spectrum measurement mode 2 Photometrics measurement mode 3 Back key 4 Time and date menu 5 Quantitation measurement mode 6 Instrument setting...

Page 12: ... above or adjacent to the key The only exception to this is the back key which is always active The main menu screen and surrounding keypad is displayed below Fig 2 4 1 Display 1 Spectrum measurement mode 2 Photometrics measurement mode 3 Back key 4 Time and date menu 5 Quantitation measurement mode 6 Instrument settings menu 7 Concentration measurement mode 8 Kinetics measurement mode 7310 09 02 ...

Page 13: ...itch for the unit 3 Power in socket Connection socket for power supply unit 4 RS232 serial port Connection to a PC or external serial printer 5 Output sockets Analogue output 2 6 FRONT PANEL The image below shows the front panel of the instrument Fig 2 6 1 Front Panel 1 Integral printer optional accessory 2 Keypad 3 USB memory stick slot 4 Instrument lid 5 Display 15 2 1 2 3 3 4 5 1 5 4 ...

Page 14: ...tration mol l 1 l is the path length cm This law shows that absorbance is linear to concentration but this is only true for low concentrations For absorbance levels above 3 the concentration starts to move away from the linear relationship Transmittance is the proportion of the light which passes through the sample Therefore T It Io Absorbance is inversely related to transmittance A log 1 T 3 2 SP...

Page 15: ...t temperature and light levels should remain as constant as possible 2 If required adherence to Standard Operating Procedures SOP and Good Laboratory Practice GLP should be monitored with regular calibration checks and a suitable Quality Control QC programme 3 The sample chamber lid must be fully closed during measurement and before any readings are recorded or printed 4 The correct selection of s...

Page 16: ...e measurement unless a suitable temperature controlled sample holder is in use Temperature change during measurement may cause air bubbles to form on the walls of the sample holder This is a common cause of drift during measurement 7 In the preparation of samples and standards high grade borosilicate glass and AR grade chemicals and reagents must be used Good quality deionised water or other suita...

Page 17: ...rast and lamp save menus All of the measurement modes open initially into a minimal operating menu This menu allows calibration and simple readings to be taken without changing any measurement parameters Pressing the key adjacent to the JW icon opens the expanded operating menu This menu enables changes to measurement parameters and settings to be made Depending on the mode the measurement paramet...

Page 18: ...rease or decrease the number The clock function uses a 24 hour format In the time and date menu to set the date press the key adjacent to the calendar icon Select the digit to be changed using the keys at the bottom of the screen Use the keys adjacent to the arrow icons to increase or decrease the number The date format can be displayed as either European dd mm yy or American mm dd yy To change be...

Page 19: ...unction is accessed through the instrument settings menu by pressing the key adjacent to the open padlock icon One press will lock the settings instantly To unlock the settings press the key again This will open the security code menu as detailed in section 4 4 1 The previously set security code must be entered to unlock the settings When the settings lock is active methods can still be opened del...

Page 20: ...ement mode icons which are displayed on the main menu are identified with a mode shown icon The mode icons which are not displayed on the main menu are identified with a mode not shown icon To change a mode from displayed to restricted or vice versa press the key adjacent to the measurement mode icon Once the required modes have been selected press the key adjacent to the tick icon to save the cha...

Page 21: ...trument settings menu 4 9 LAMP SAVE This function is only available on the 7310 visible spectrophotometer which uses a tungsten halogen lamp The lamp save function enables the time in minutes to be set after which the lamp will be turned off following a period of no lamp activity i e no readings have been performed This function is accessed through the instrument settings menu by pressing the key ...

Page 22: ...on and the lamp will begin to warm up The lamp cold icon is displayed adjacent to the calibrate to zero icon in the measurement mode The time needed for the lamp to warm up is five minutes To view the remaining warm up time press the key below the lamp cold icon Calibration and measurements can be performed whilst the lamp is warming up but these results may not be accurate Once the warm up time o...

Page 23: ...ing menu enables measurement parameters to be changed The utility toolbar on the left hand side of the screen enables access to printing print setup options results methods and autologging options For more details on the different functions of the utility toolbar refer to section 10 Fig 5 1 1 Expanded Operating Menu 5 2 METHOD SET UP This measurement mode is very simple and the only parameters whi...

Page 24: ...100 transmittance Once the calibration is complete the measure sample icon appears and the sample can be measured If the wavelength is adjusted before a sample is measured the measure sample icon will disappear and the instrument must be calibrated again at the new wavelength 5 4 SAMPLE MEASURMENT Itisnotpossibletomeasureasamplebeforetheinstrument has been calibrated at the selected wavelength Onc...

Page 25: ...ility toolbar on the left hand side of the screen enables access to printing print setup options results methods and autologging options For more details on the different functions of the utility toolbar refer to section 10 The settings icon enables the wavelength units resolution standard or factor to be set Fig 6 1 1 Expanded Operating Menu 6 2 METHOD SETUP 6 2 1 Selecting a Wavelength The wavel...

Page 26: ...ecting this option will calculate the factor If the factor is known it is not necessary to measure a known standard s concentration When the standard or factor is not selected the value should be set to 1 00 6 2 2 1 Selecting Concentration Units The units of concentration can be selected from a number of options no units ppm EBC SRM mEq l mEq M mM µM nM U U l U ml g l mg l µg l ng l g dl mg dl µg ...

Page 27: ...f the screen to select the digit to be changed The key below the digit must be pressed twice to select the adjacent digit For example 00 the first press of the key alters 10 the second press alters 01 Use the keys adjacent to the arrow icons to increase or decrease the selected number Factor values of 0 001 to 10 000 can be entered The factor value can be reset to zero by pressing the key adjacent...

Page 28: ...n calibrated at the selected wavelength In this operating mode the type of sample measurement performed depends on the calibration which has been carried out 6 4 1 Measuring a Sample After Calibrating to a Standard Remove the cuvette containing the standard sample and place a cuvette containing the sample to be measured in the sample chamber Close the instrument lid and press the key below the mea...

Page 29: ...rinting print setup options results methods and autologging options For more details on the different functions of the utility toolbar refer to section 10 The scan settings icon enables the graph y axis absorbance or transmittance operating mode start and end wavelengths and scan interval to be set The peaks and valleys threshold icon enables the peaks and valleys threshold to be set The peaks and...

Page 30: ...nge from 198 to 1000nm To set the start wavelength in the scan settings menu press the key adjacent to the wavelength on the far left of the x axis This opens the number entry screen Use the keys at the bottom of the screen to select the digit to be changed and use the keys adjacent to the arrow icons to increase or decrease the number Once the required start wavelength has been entered press the ...

Page 31: ...ected for a wavelength range of 400 to 503nm 7 2 1 4 Y Axis Scaling This function enables the scale of the y axis of the spectrum graph to be adjusted either manually or automatically The automatic scaling is represented by the hand icon with a cross through it and the manual scaling by the hand icon without the cross To select manual or automatic scaling press the key adjacent to the hand icon Re...

Page 32: ...ll be needed to stop the baseline scan Press the key adjacent to the tick icon to confirm stopping the baseline scan and return to the expanded operating menu Press the key adjacent to the cross icon to continue the baseline scan Once the baseline scan has been completed the scan sample icon is displayed and a sample can be measured If the wavelength range or the scan interval is changed before a ...

Page 33: ...eshold value The spectral points analysis function enables points to be selected from the scan to analyse absorbance or transmittance at selected wavelengths 7 5 1 Peaks and Valleys Threshold This function enables the peaks and valleys threshold to be set at 1 5 10 or turned off To select the threshold value press the key adjacent to the peaks and valleys threshold icon Repeat presses of the key w...

Page 34: ...yse the absorbance or transmittance at a selected wavelength To access this function press the key adjacent to the spectral points analysis icon and this opens the selection screen A solid vertical line will appear on the far right of the screen Use the keys below the greater than or less than icons to move the line along the spectrum by decreasing or increasing the wavelength by one scan interval...

Page 35: ...ints analysis table If a wavelength entered is outside the scan range the check number warning icon will be displayed before the wavelength is automatically adjusted to within the range To view the points in the spectral points analysis table press the key adjacent to the spectral points analysis table icon Only three points can be displayed on the screen at one time to view the other points in th...

Page 36: ...the expanded operating menu The quantitation expanded operating menu enables measurement parameters to be changed The utility toolbar on the left hand side of the screen enables access to printing print setup options results methods and autologging options For more details on the different functions of the utility toolbar refer to section 10 The standard curve icon enables the current standard cur...

Page 37: ...o be accessed from this screen by pressing the key adjacent to the standard curve icon The standard curve can also be viewed from this screen by pressing the key adjacent to the standard curve icon 8 2 2 1 Selecting Number of Standards The number of standards used to create a standard curve can be changed from 2 to 6 standards To change the number of standards press the key below the number of sta...

Page 38: ...con to save the changes The photometric values of the standards can also be entered if known To enter the photometric value press the key adjacent to the photometric value in the table that corresponds to the relevant concentration this opens the number entry screen Use the keys at the bottom of the screen to select the digit to be changed and use the keys adjacent to the arrow icons to increase o...

Page 39: ... correlation coefficient r2 To exit this screen press the key adjacent to the tick icon The quantitation table can also be viewed from this screen by pressing the key adjacent to the quantitation table icon 8 2 3 1 Creating a New Standard Curve Before creating a new curve it is necessary to enter the concentrations of the standard solutions in the quantitation table Also the number of standards sh...

Page 40: ...erating menu where unknown samples can be measured When this operating mode is exited the current standard curve will be saved until it is replaced by a new curve The automatic 8 cell turret can be used to assist creating a new curve Refer to section 11 3 1 1 for more details 8 3 CALIBRATION The zero calibration must be performed at the same wavelength as the standards were measured at and the unk...

Page 41: ...tistics function is accessed by pressing the key below the S icon in the quantitation curve menu The algorithm of the curve fit can be changed by pressing the key below the curve fit icon For more information regarding curve fit and statistics refer to section 8 2 3 0 600 ABS 0 300 0 000 0 00 y mx c 0 60 0 30 ppm Y mX C m 1 000 c 0 000 r2 1 149 ...

Page 42: ...ty toolbar on the left hand side of the screen enables access to printing print setup options results methods and autologging options For more details on the different functions of the utility toolbar refer to section 10 The settings icon enables the wavelength units resolution graph y axis absorbance or transmittance operating mode standard factor measurement time lag time and start on level to b...

Page 43: ...th a cross through it and the manual scaling by the hand icon without the cross To select manual or automatic scaling press the key adjacent to the hand icon Repeat pressing of the key cycles between manual and automatic scaling In automatic y axis scaling the absorbance or transmittance values are cleared from the settings screen When the kinetics measurement is complete the y axis is automatical...

Page 44: ... far left side of the x axis This opens the lag time start on level menu To set the lag time press the key adjacent to the clock icon Use the keys at the bottom of the screen to select the digit to be changed and the keys adjacent to the arrow icons to increase or decrease the number The lag time can be reset to zero by pressing the key adjacent to the 000 icon Once the required lag time has been ...

Page 45: ...can be reset to zero by pressing the key adjacent to the 000 icon Once the standard value has been entered press the key adjacent to the tick icon to save and return to the settings menu screen The entered value is now displayed in the settings menu adjacent to the standard icon A standard value should only be entered if the factor is not known If the factor is known the standard value should be s...

Page 46: ...tion must be performed at the same wavelength at which the sample will be measured Insert a cuvette containing the blank solution into the sample chamber and close the instrument lid Press the key below the calibrate to zero absorbance icon The instrument will calibrate to 0 00 absorbance Once the calibration is complete the start kinetics measurement icon will be displayed and a sample can be mea...

Page 47: ...ent press the key adjacent to the S icon which opens the statistics menu over the top of the expanded operating menu The information displayed includes concentration absorbance per minute rate of change correlation coefficient r2 start time absorbance and end time absorbance If the operating mode selected was transmittance then the statistics displayed will be transmittance instead of absorbance I...

Page 48: ... intervals The double greater than or double less than icons move the line in 5 second time intervals Once the required initial and final times have been selected press the key adjacent to the S icon to display the statics menu for that portion of the experiment The information displayed includes concentration absorbance per minute rate of change correlation coefficient r2 start time absorbance an...

Page 49: ... the name of the method press the key below the eraser icon One press of the key will delete one letter holding the key for 2 seconds will delete the name completely To select letters use the keys adjacent to the arrow icons to move around the menu Once the required letter is highlighted press the key below the pencil icon to select the letter Up to eight characters can be selected To change the l...

Page 50: ...ess the key adjacent to the cross icon to cancel and return to the option of saving one or all of the methods to USB memory stick 10 2 OPENING METHODS Methods can be opened from the internal memory of the instrument or from a USB memory stick Before a method can be opened from a USB memory stick it must be saved to the internal memory of the instrument first 10 2 1 OPENING METHODS FROM INTERNAL ME...

Page 51: ...n to the option of opening one or all methods from the USB memory stick If a single method is selected to be opened this method will be stored in the same location that is was saved in when it was saved to the USB memory stick 10 3 DELETING METHODS In the expanded operating menu press the key adjacent to the method icon to open the method selection menu and use the keys adjacent to the arrow icons...

Page 52: ...saved results are listed alphabetically with the date and time that the result was generated If there is already a result saved under the same name confirmation will be needed to replace the existing result with the new one Press the key adjacent to the tick icon to confirm replacement Press the key adjacent to the cross icon to cancel and return to the results naming menu In photometrics concentr...

Page 53: ...ey adjacent to the result Press the key below the delete icon Confirmation will be needed to delete the selected result press the key adjacent to the tick icon to confirm deletion Press the key adjacent to the cross icon to cancel and return to the results selection menu 10 7 PRINTING The utility toolbar in the expanded operating menu enables results to be printed and print setup options to be set...

Page 54: ...ected press the key adjacent to the tick icon to save and return to the expanded operating menu 10 7 1 1 Print Setup PHOTOMETRICS AND CONCENTRATION In the photometrics and concentration measurement modes the print setup menu does not contain any additional post analysis statistics 10 7 1 2 Print Setup SPECTRUM In the spectrum measurement mode print setup menu it is possible to print off the spectr...

Page 55: ...ween a tick and a cross icon for selected or deselected To select the data interval press the key adjacent to the data interval icon Repeat presses will cycle between 0 1 5 10 30 or 60 seconds Once the required options have been selected press the key adjacent to the tick icon to save and exit print set up 10 7 2 Printing Results Results displayed in the expanded operating menu can be printed by p...

Page 56: ...name press the key adjacent to the tick icon To change the name press the key below the eraser icon One press of the key will delete one letter holding the key for 2 seconds will delete the name completely To select letters use the keys adjacent to the arrow icons to move around the menu Once the required letter is highlighted press the key below the pencil icon to select the letter Up to eight ch...

Page 57: ...o be recorded Press the key adjacent to the tick icon to confirm selection Press the key adjacent to the cross icon to cancel and return to the expanded operating menu 10 8 2 Selecting Result s Destination The autolog menu enables the result s destination to be set To select the internal printer press the key adjacent to the printer icon This option is only available if an internal printer is conn...

Page 58: ...ING THE ACCESSORIES There are two types of accessories which can be fitted in the sample chamber passive or active accessories The range of passive accessories includes 10 x 10mm single cuvette holders single water heated cuvette holders adjustable path length 10 to 100 mm cuvette holders test tube holders boiling tube holders film holders and micro cuvette holders The range of active accessories ...

Page 59: ... fed correctly 11 2 2 PASSIVE ACCESSORIES Unscrew the thumb screw to undo the passive accessory Lift out the passive accessory To fit a different passive accessory simply place the accessory in the correct orientation align the thumb screw and tighten to fix in place To replace the passive accessory with an active accessory refer to section 11 2 3 11 2 3 ACTIVE ACCESSORIES Unscrew the thumb screw ...

Page 60: ... the correct position If the fitting is too tight use a small screw driver to loosen the ball bearings before pushing the carousel down onto the shaft 11 2 3 2 Peltier For this accessory as well as removing the passive accessory base plate the front panel of the instrument must also be removed Loosen screws 5 and 6 until the front panel can be lifted out in the forwards direction Take the peltier ...

Page 61: ...ing must be kept as short as possible and the tubing must not be allowed to obstruct the ligth path For sipping 1 Connect the sipper pump tubing to the outlet port on the flow through cuvette 2 Secure the tubing using the clip on the righthand side of the pump head 3 Ease the tubing round the rollers by carefully rotating them clockwise by hand Clamp the tubing into the clip on the left hand side ...

Page 62: ...he motor 3 Fit the other end onto the inlet port on the flow through cuvette 4 Fit the second 300mm length of tubing to the outlet port of the flow through cuvette Once secured ensure the tubing is routed into the two retaining clips located on the base plate at the side of the pump head 5 Fit the other end of the tubing onto the outlet port located on the inside of the front bulkhead 6 Connect a ...

Page 63: ...n measured To adjust the wavelength press the key below the 8 cell turret icon and use the arrow icons to adjust the wavelength 11 3 1 1 Automatic 8 cell turret supporting creation of a standard curve in quantitation The 8 cell turret can be used to support creation of a new standard curve in the quantitation measurement mode Refer to section 8 2 3 1 for more details When the standard measurement ...

Page 64: ...he expanded operating menu The peltier will begin to heat or cool depending on the current temperature 11 3 3 Sipper pump When the sipper is in use the sipper pump icon is displayed in the bottom right hand corner of the screen The pump direction is displayed by an arrow icon below the sipper pump icon The sipper pump can operate in manual or timed mode depending on the option selected in sipper p...

Page 65: ...ey below the calibrate timed sipper icon Select the required pump direction by pressing the key below the forwards or backwards arrow icon Press the key adjacent to the tick icon to continue to the next stage of the calibration sequence Insert the inlet tubing into the sample container and press the key adjacent to the single greater than icon The sipper pump will start and the sample will be pump...

Page 66: ...ir uptake is recorded To fine tune the amount of air uptake press the keys below the plus or minus icons to increase or decrease the amount of air taken in The recorded time will be adjusted accordingly Once the fine tuning is complete or if none is required press the key adjacent to the tick icon to move to the next stage of the calibration sequence Once the sample uptake and air gap have been pr...

Page 67: ...ap take up time If an air gap of zero was previously selected this screen will not appear and the calibration sequence will continue to sample disposal Once this stage of the calibration sequence is complete press the key below the sipper pump icon to dispose of the sample Confirmation will be needed to start the sipper pump Press the key adjacent to the cross icon to cancel and return to the expa...

Page 68: ...tier settings enabling the temperature to be set Refer to section 11 3 2 for more details The sipper pump can operate in a manual or timed mode Refer to section 11 3 for more details 11 4 SPARES Part Code Description of Spare Part 012 075 Tungsten halogen lamp 730 545 Xenon lamp module 735 801 10x10mm path length cuvette holder 060 084 Pack of 100 disposable plastic visible wavelength 10x10 cuvett...

Page 69: ...s panel located on the rear of the instrument refer to section 2 5 1 Remove the screws holding the lamp access panel in place 2 Withdraw the lamp access panel and unscrew the lamp bracket fixing screw 3 Grasp and rotate the lamp bracket to gain access to the lamp 4 Remove the old lamp from the holder The lamp is a plug in fit and should be removed by gently easing it from the holder 5 Carefully re...

Page 70: ... Department for a reference number which you should include with your faulty equipment Please also ensure you include a clear description of the fault and a completed copy of our Decontamination Certificate This is available as a downloadable pdf file at www jenway com or contact us and we will be happy to fax you a copy Please clearly mark the package for the attention of the Service Department a...

Page 71: ...g the top left button during the power on tests performed when the instrument is turned on 2 the parameters have been corrupted so the instrument has reset itself Solution Press the key adjacent to the tick icon to action Err 3 Dark Calibration Error This error indicates that the dark level is too high during calibration In normal operation the lamp is switched off during an operator initiated War...

Page 72: ... adjacent to the tick icon to carry on using the instrument Restart the unit if the problem persists contact a service technician Err 8 Unable to find Vane on Turret This error indicates that the vane position zero on the turret cannot be found Warning The most likely causes for this error are 1 The turret carousel has been removed and not replaced Redo Solution Check if the turret is in the sampl...

Page 73: ... USB memory stick Ensure the USB memory stick has free capacity Ensure there is a result displayed on the screen Unable to continue kinetics Due to the nature of the kinetics measurements stopping the measurement after measurement before completion will result in some measurement cancelling abort action time being lost Therefore the experiment cannot be continued It must be restarted The peaks and...

Page 74: ...SECTION 14 Declaration of Conformity 76 ...

Page 75: ...SECTION 14 Declaration of Conformity 77 ...

Page 76: ...n English English icon Language selection Common USB memory stick Common Save to USB memory stick Common Load from USB memory stick Common Result already saved to USB memory stick Common 1 Single method save icon Common 1 48 1 48 method save icon Common 1 Single method open icon Common 1 48 1 48 method open icon Common Axis icon View the result graphically Common ABC icon View the results as a tex...

Page 77: ...n screen Common Resolution Common 400nm Wavelength Common ABS T Abs T icon Operating mode either absorbance or transmittance Common Lamp cold Common Lamp save Common Caution icon accompanied by error code Common Check number Common Stop icon accompanied by error code Main Menu Opens concentration measurement mode Main Menu Opens kinetics measurement mode Main Menu Opens photometrics measurement mo...

Page 78: ...nterval between each sample measurement repetition Autolog Batch ABC icon Set batch name for repeated measurements Autolog Batch append add existing results Autolog Batch delete overwrite existing results Instrument Closed padlock icon Settings locked Settings Instrument Open padlock icon Settings unlocked Settings Instrument Methods unlocked method selection menu enabled Settings Instrument Metho...

Page 79: ...ts standard or factor value to zero Concentration Check standard Spectrum Scan settings menu Spectrum Hand icon Manual y axis scaling Spectrum Hand icon with cross through it Auto y axis scaling Spectrum Scan interval Spectrum Baseline scan Spectrum Baseline scan in progress Spectrum Scan sample Spectrum Sample scan in progress Spectrum Peaks and valleys threshold turned off Spectrum Peaks and val...

Page 80: ...ard curve Quantitation Curve fit enables the curve fit to be adjusted Quantitation Sigma icon Displays curve statistics Quantitation Create new standard curve Quantitation Tick icon Read Standard Quantitation Back icon Re measure previous standard Quantitation Cross icon Cancel creation of new standard curve Quantitation Curve statistics used in print setup Kinetics Settings menu Kinetics Hand ico...

Page 81: ...o single cell Method created on a unit with a single cell accessory fitted Accessories 8 cell turret icon the automatic 8 cell turret is in use Accessories Error finding cell position 0 on turret Accessories No turret Method created on a unit with a turret accessory fitted Accessories C Degrees Celsius Accessories F Degrees Fahrenheit Accessories Peltier accessory in use current temperature is bel...

Page 82: ...es Increase sample uptake increase air gap Accessories No sipper Method created on a unit with a sipper accessory fitted Accessories Sipper peltier pump in use Accessories No sipper peltier Method created on a unit with a sipper peltier accessory fitted Accessories PC comms shown when the instrument is connected to a PC and communicating via the PC software Error Spanner Refer to section 13 84 ...

Page 83: ...t setup 19 Contrast 23 Expanded operating menu 19 GLP settings 22 Lamp save 23 Mode selection 22 Navigating 19 Utility toolbar 20 KINETICS 44 CALIBRATION 48 DATA ANALYSIS 49 METHOD SET UP 45 MODE SPECIFIC PARAMETERS 44 SAMPLE MEASUREMENT 48 Lamp replacement Tungsten halogen lamp replacement 71 Xenon lamp module replacement 71 Language 56 PHOTOMETRICS 25 CALIBRATION 26 METHOD SET UP 27 MODE SPECIFI...

Page 84: ...S 51 SAVING RESULTS 53 Screen setup 19 SERVICE 71 Spare parts 70 SPECTRUM 31 CALIBRATION 34 DATA ANALYSIS 35 METHOD SETUP 32 MODE SPECIFIC PARAMETERS 31 SAMPLE MEASUREMENT 34 Technical specification 8 Technical support 75 Theory and practice of spectroscopy measurements 16 Spectroscopy measurement 16 Theory of spectroscopy measurements 16 Troubleshooting 73 Utility toolbar 20 86 ...

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