background image

1. 

Connect the

probe to the
meter. Make sure
that the cable
locking nut is
securely
connected to the
meter. Turn the
meter on.

2. 

To significantly

reduce the
stabilization time
for reducing-type
samples, put the
platinum disc in
Reducing Solution
for ORP
Electrodes for
3-10 minutes
before the initial
sample
measurement.

3. 

Rinse the probe

with the sample.

4. 

Put the probe in

the sample and
stir gently. Make
sure that the
reference
junctions are
completely
submerged. Do
not put the probe
on the bottom or
sides of the
container. Shake
the probe from
side to side in the
sample to refresh
the reference
junction.

5. 

Push 

Read

.

The display will
show "Stabilizing"
and a progress
bar as the probe
stabilizes in the
sample. The
display will show
the lock icon when
the reading
stabilizes. If
necessary for the
application, record
the sample pH
and temperature.

6. 

Repeat steps

3-6 for additional
measurements.

7. 

When

measurements
are done, store
the probe (refer to 

Storage

on page 11).

Measurement—conversion to SHE reference procedure:

For some applications, it is customary to report redox potential readings relative to the
standard hydrogen electrode (SHE), also called normal hydrogen electrode (NHE). To do
this, select the value in 

Table 1

 that corresponds to the temperature of the solution

measured. Substitute that value Eref into the equation and solve for E

h

:

E

h

 = E + E

ref

where:
E

h

 = oxidation reduction potential of the sample relative to the SHE

E = potential developed by the ORP/Redox electrode
E

ref

 = potential developed by the reference electrode portion relative to the SHE

(

Table 1

).

Table 1

 shows the potentials, E

ref

, developed by the reference electrode portion relative

to the SHE at various temperatures.

Table 1  Standard potential of reference electrode

Temperature (°C)

Electrode potential in mV (E

ref

)

80 

163.1 

75 

167.7 

5

Summary of Contents for Intellical MTC30101

Page 1: ...ng temperature range 0 to 80 C 32 to 176 F Storage temperature range 5 to 40 C 41 to 104 F Junction Ceramic Reference potential versus Standard Hydrogen Electrode 207 mV at 25 C Fill solution 3M KCl w...

Page 2: ...ode with deionized water thoroughly to remove the viscous storage filling solution completely Blot dry with a lint free cloth 4 Remove the protective tape from the filling hole before initial use refe...

Page 3: ...he temperature range of 0 to 30 C 32 to 86 F Light s solution should be read at 25 C 77 F Custom ORP Redox calibration solution values and temperature are user defined The calibration is recorded in t...

Page 4: ...er to the HQd meter manual for more information Regular calibration is required for the best measurement accuracy refer to Calibration on page 3 Prepare the probe for use refer to Preparation for use...

Page 5: ...ation record the sample pH and temperature 6 Repeat steps 3 6 for additional measurements 7 When measurements are done store the probe refer to Storage on page 11 Measurement conversion to SHE referen...

Page 6: ...ation state After each addition of titrant the ORP Redox electrode develops a potential proportional to the logarithm of the ratio of the activities of the two oxidation states At the inflection or en...

Page 7: ...normality of the sample Nx in equivalents per liter Nx Vt x Nt Vx where Nt normality of titrant Eq L Vt volume of titrant at end point mL Vx Volume of sample mL Run Check Standard The Run Check Stand...

Page 8: ...available options and how to change them are given in the screens tables and procedures throughout this section The settings that can be changed are shown in Table 2 Table 2 Parameter specific settin...

Page 9: ...ush and select MTC301 Settings 3 Select Modify Current Settings 4 Select Calibration Options and update the settings Option Description Standard Sets the calibration standard ZoBell s 221mV 25 C Light...

Page 10: ...stom check standard are user defined 5 Select Check Standard Reminder and update the settings Option Description Reminder Repeat Sets the time interval for the check standard reminder Off default 1 d...

Page 11: ...uct overview on page 1 2 Remove the cap from the tip of the filling solution bottle 3 Hold the bottle so that the tip is down Put the tip of the bottle in the filling hole 4 Slowly squeeze the bottle...

Page 12: ...r manual Large number of methods stored on the probe Continue to let the probe connect Do not disconnect the probe Damaged probe Make sure there is connectivity with another probe or meter to confirm...

Page 13: ...onse time Platinum electrode not conditioned for reducing type samples 1 Make sure that the platinum disc is clean and smooth 2 Put the platinum disc in Reducing Solution for ORP Electrodes for 3 10 m...

Page 14: ...e probe downward in the solution sample to remove any air bubbles in the reference junction holes Out of limits Check standard value is outside of limits set in the current method Make sure that the s...

Page 15: ...15...

Page 16: ...ch com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info hach lange de www hach lange de HACH LANGE S rl 6 route de Compois 1222 V se...

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