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Hach HIAC 9705, Operator'S Manual

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HIAC 9705
LIquId PArtICLe CountIng SyStem

Operator Manual

Summary of Contents for HIAC 9705

Page 1: ...HIAC 9705 Liquid Particle Counting System Operator Manual...

Page 2: ...9705 KSS March 2006 Edition 1 Operator Manual...

Page 3: ...Changing the Language 24 3 3 Display Settings 25 3 4 Changing the Date and Time 26 3 5 Setting Particle Sizes 27 3 5 1 Adding a Size 27 3 5 2 Editing a Size 28 3 5 3 Deleting a Size 28 3 6 Setting Fl...

Page 4: ...inting Results 58 4 6 1 Automatically Printing Results 58 4 6 2 Manually Printing Results 59 4 7 Operating with PharmSpec 59 5 Maintenance Procedures 5 1 Overview 61 5 2 Cleaning the 9705 61 5 3 Flush...

Page 5: ...9705 Table of Contents 5 of 82 KSS March 2006 Edition 1 HIAC Operator Manual Appendix C Certifications C 1 Overview 75...

Page 6: ...6 of 82 Table of Contents 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 7: ...r by any means without the written permission of Hach Ultra Safety Conventions WARNING A warning is used to indicate a condition which if not met could cause serious personal injury and or death Do no...

Page 8: ...any instrument covered under this warranty proves defective during this period Hach Ultra will at its option either repair the defective product without charge for parts and labor or provide an equiva...

Page 9: ...TS IS THE SOLE AND EXCLUSIVE REMEDY PROVIDED TO THE CUSTOMER FOR BREACH OF THIS WARRANTY HACH ULTRA ANALYTICS AND ITS VENDORS WILL NOT BE LIABLE FOR ANY INDIRECT SPECIAL INCIDENTAL OR CONSEQUENTIAL DA...

Page 10: ...10 of 82 Manual Overview 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 11: ...Product Overview The Model 9705 Liquid Particle Counting System combines proven technology and application knowledge in a compact syringe sampler This instrument precisely measures particles from smal...

Page 12: ...he screen A button is an area of the touch screen that should be touched to invoke another screen or execute an action such as performing a sample run or clearing the buffer A field indicates an area...

Page 13: ...tside of the carton for signs of damage dents tears etc that may have occurred during shipping and bring the damage to the attention of the shipper Save this carton for reshipping the 9705 Inspect the...

Page 14: ...mmunications connections are complete 2 3 Fluid Connections 2 3 1 Connecting the Drain Line 1 Attach the drain line to the back of the unit 2 Be sure the connection is secure before powering on the un...

Page 15: ...f the power cord to the male socket on the rear panel of the 9705 Plug the power cord into an appropriately rated AC line Attach the AC power cable supplied with the unit to the AC power socket Do not...

Page 16: ...n the right of the 9705 upward to open it and gain access to the syringe cavity 3 Be certain that the syringe is of an appropriate size Remove the drive bolt from the syringe drive mechanism 4 Fasten...

Page 17: ...tamper with the door interlock Do not attempt to operate the 9705 with the door open Note When changing syringe sizes adjust the 9705 s settings to make sure the syringe installed matches the syringe...

Page 18: ...icon to invoke the Setup screen shown in Figure 2 6 10 From the Setup screen select the Syringe icon to invoke the Syringe Settings screen shown in Figure 2 7 11 Check that the syringe size listed ma...

Page 19: ...h the Return icon to exit the Syringe Settings screen and return to the Setup screen then press Return again to return to the Main Screen 2 6 Loading Printer Paper The 9705 features an internal printe...

Page 20: ...ter paper 1 Locate the printer on the left of the unit shown in Figure 2 8 2 Pull up the green handle in the center of the paper cover until a click is heard 3 Fold the door down and remove the cardbo...

Page 21: ...r after a print command has been sent double check paper direction 2 7 Initial Power On Once the unit is powered on the screen appears like the one shown in Figure 2 9 Refer to Operating the 9705 on p...

Page 22: ...22 of 82 Initialization 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 23: ...The 9705 s functions are accessed via an icon bar shown in Figure 3 1 Many of the 9705 s settings are accessed via the Setup icon shown in Figure 3 1 Touching the Setup icon invokes the Setup screen s...

Page 24: ...nge size Changing flow rate Changing the Syringe Size on page 49 Setting Flow Rate on page 28 Display Setting these parameters Count display Scaling Number of runs to display Display Settings on page...

Page 25: ...om the dropdown menu 4 A warning message will appear to ask for confirmation that the language will change If the language selected is correct press OK 5 Press Return to save changes and exit 3 3 Disp...

Page 26: ...e the System Settings screen shown in Figure 3 5 2 To change the date touch the Date field to invoke a keypad entry screen 3 Enter the current date by pressing the number keys in YYYY MM DD format Be...

Page 27: ...izes icon to invoke the Size Settings screen shown in Figure 3 6 These functions are accessed through the icons on this tab Adding sizes Editing sizes Deleting sizes The minimum size that may be enter...

Page 28: ...n microns to be measured up to two decimal places such as 1 55 5 Press Enter to save changes and close the Particle Size Entry screen 6 Press the Return icon to return to the main screen 3 5 3 Deletin...

Page 29: ...ntry between 10 and 60 mL Touch OK to close this window and return to the Flow Rate Entry screen 4 Press Enter to save changes and return to the Syringe Settings screen 5 Press the Return icon to retu...

Page 30: ...ght Timeout Entry screen This sets the amount of time in minutes the 9705 is inactive before the unit display goes dark to conserve screen life Note A setting of zero 0 will prevent the backlight from...

Page 31: ...vailable choices are listed in Table 3 3 Fig 3 9 Sound Settings Screen Table 3 3 Sound Tab Field Descriptions Field Description Entries User Feedback Sound effect for any action taken by the user None...

Page 32: ...vent needle is used to sample 5 30 mL bottles The longer vent needle is used to sample 50 125 mL bottles The vent needle must be removed to use the Large Volume Adapter LVA this process is described i...

Page 33: ...Operator Manual 3 Carefully slide the removal tool over the longer needle 4 Seat the tabs of the removal tool into the slot of the needle screw and turn counterclockwise to remove the needle Fig 3 11...

Page 34: ...2006 Edition 1 Operator Manual HIAC 5 Remove the needle from the bottle dock carefully slide it out of the tool and place it in the protective sleeve that it was originally supplied with Fig 3 13 Seat...

Page 35: ...ting the Large Volume Adapter The 9705 can also be used with a Large Volume Adapter to sample from vessels greater than 125 mL Using the Large Volume Adapter LVA requires these steps 1 Remove the vent...

Page 36: ...rator Manual HIAC 3 Carefully slide the removal tool over the long needle 4 Seat the tabs of the removal tool into the slot of the needle screw and turn counterclockwise to remove the needle Fig 3 16...

Page 37: ...2006 Edition 1 HIAC Operator Manual 5 Remove the needle from the bottle dock carefully slide it out of the tool and place it in the protective sleeve that it was originally supplied with Fig 3 18 Seat...

Page 38: ...se This opens the internal O ring 7 With the O ring opened align the adapter as shown in Figure 3 21 such that the peg on the bottom aligns with the threaded hole in the bottle dock Position the hole...

Page 39: ...8 Fully seat the adapter over the short needle such that the bottom sits firmly on the base of the bottle dock Turn the adapter handle fully clockwise This closes the internal O ring 9 Pass the adapte...

Page 40: ...KSS March 2006 Edition 1 Operator Manual HIAC 10 The large volume adapter is now ready to be connected to an external sampling probe sample bag or other vial Fig 3 23 Install the Bottle Guide Fig 3 2...

Page 41: ...2006 Edition 1 HIAC Operator Manual 3 10 2 Connecting the Large Volume Adapter to the Sampling Probe 1 The sampling probe will be attached to a lab stand Assemble the lab stand components as shown in...

Page 42: ...pling probe on to the 20 threaded stud on the end of the horizontal support rod 3 Connect the large volume adapter fitting to the sampling probe Finger tighten the connection clockwise until it bottom...

Page 43: ...9705 System Setup 43 of 82 KSS March 2006 Edition 1 HIAC Operator Manual Fig 3 27 Connect the LVA Fitting to the Probe Fig 3 28 Large Volume Adapter Assembly...

Page 44: ...d then proceed through the following steps 1 Leave the tube connected to the Large Volume Adapter Cut the sampling probe end to the desired length Make this cut clean and square Leave the fitting nut...

Page 45: ...March 2006 Edition 1 HIAC Operator Manual 3 Orient the two ferrule pieces as shown and slide them onto the tubing in the order shown Fig 3 31 Flat End Fig 3 32 Sharp End Fig 3 33 Slide Ferrule Pieces...

Page 46: ...held flush with the bottom of the port while the ferrules are pushed in and the nut is tightened 5 Remove the tube from the sampling probe and inspect the ferrule crimp It should look the same as the...

Page 47: ...it completely by hand 3 10 4 Alternate Use of Lab Stand as Sample Bag Hanger The optional ram s horn hook can be fastened to the Lab Stand for hanging flexible bags such as IV bags The user will need...

Page 48: ...ulating Tare Volume The tare volume when using the adapter can be calculated by adding the fixed component volume of 0 83 mL to the volume of the adjustable length tube To calculate the volume of the...

Page 49: ...selection Valid entries include 5 Press the Return icon to save changes and return to the main screen 3 12 Changing Sample Parameters 1 To change the sample parameters touch the upper right section o...

Page 50: ...hing the field to invoke the menu then touching the desired setting to highlight it Table 3 4 Sample Settings Fields Field Name Description Valid Entries Number of runs The number of samples taken fro...

Page 51: ...can be used when sampling volumes larger than the syringe size These sample volumes require the liquid to be brought to speed before the sample is taken 0 0 through 25 0 Dilution Factor Ratio of fluid...

Page 52: ...ctions listed in Table 3 5 to only be accessible once a password has been entered When security is enabled users must enter a password to access most functions 3 14 1 Enabling Password Protection 1 Fr...

Page 53: ...gure 3 41 2 Press the Change Password icon to invoke the Change Password screen 3 Touch the Enter New Password field A keyboard entry screen appears 4 Enter the new password from the keyboard entry sc...

Page 54: ...he Main screen select the System icon Security icon to invoke the Security Settings screen shown in Figure 3 41 2 From the Security Settings screen touch the Enabled Security checkbox to remove the ch...

Page 55: ...llow scrolling through the notes The upper right corner of the screen shows the current settings for Sample volume Flow rate Number of runs Dilution factor The lower half of the screen shows the parti...

Page 56: ...the septa and use the hand crimper to seal the bottles WARNING Be careful when crimping the seals to avoid pinching fingers 4 3 Loading Samples into the Accu Swirl WARNING Needles are sharp Avoid cont...

Page 57: ...arameters cannot be changed Click on the lower portion of the main screen to toggle between viewing the data in a chart form and in a graph form In the chart form use the blue arrows at the right of t...

Page 58: ...touch the Add Notes icon to invoke a keyboard entry screen Notes are limited to 24 characters per line 3 Press Enter to return to the Notes screen 4 Press the Return icon to return to the main screen...

Page 59: ...or standard deviation to print by clicking the boxes 4 Press Return to return to the Setup screen 4 6 2 Manually Printing Results 1 From the main screen select the Print icon 2 The currently displayed...

Page 60: ...60 of 82 Operating the 9705 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 61: ...ris remains wipe with a soft cloth moistened with a mild cleaning solution or alcohol CAUTION Do not spray the touchscreen with solution as the solution may penetrate the electronics and damage the 97...

Page 62: ...each use If the plunger is removed from the syringe wipe the plunger with alcohol before replacement Clean the syringes periodically with a mild detergent Allow the detergent to sit in the syringe for...

Page 63: ...push the brush into the sensor with a twisting motion 5 Once the cell has been cleaned with the brush remove the brush and reinstall the clean out port cap Tighten cap snugly Do not over tighten 6 Fl...

Page 64: ...64 of 82 Maintenance Procedures 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 65: ...lems 6 3 Diagnostics Screen Table 6 1 Error Messages Error Message Cause Solutions Syringe door open Occurs when the syringe door is ajar Close syringe door Communication error Occurs when communicati...

Page 66: ...he 9705 has a limited number of user serviceable parts the Diagnostics tab lists information that may be useful either to the end user or Technical Support The Diagnostics screen is divided into four...

Page 67: ...Fields Field Description Laser Current Displays the laser current value Laser Current Status Normal Low exceeds minimum High exceeds maximum Laser Cal Displays the laser calibration voltage Laser Cal...

Page 68: ...ion data thresholds for each particle size channel in the 9705 as shown in Figure 6 4 This tab is for factory use only 6 3 3 Factory Tab The Factory tab lists factory set information such as the model...

Page 69: ...mber of the 9705 Read only View Volume View volume of the sensor 1 through 100 Calibration Date Date the 9705 was calibrated Read only Calibration Due Date Date the 9705 s calibration expires Read onl...

Page 70: ...s and Troubleshooting 9705 KSS March 2006 Edition 1 Operator Manual HIAC 6 3 4 Sensor Log Tab The Sensor Log tab lists laser current and calibration information for the 9705 as shown in Figure 6 6 Fig...

Page 71: ...personal injury and or damage to the unit Before shipping or storing the unit run a test without attaching a sample vial to purge the unit of all liquid All analyzers returned for repair or replaceme...

Page 72: ...72 of 82 Service Procedures 9705 KSS March 2006 Edition 1 Operator Manual HIAC...

Page 73: ...5 x 20mm Dimensions H x W x D 40 5 x 30 1 x 34 3 cm 16 0 x 11 9 x 13 5 in Weight 10 7 kg 23 5 lbs Sample Bottle Clearance 11 8 cm 4 6 in Tare Volume 0 54 mL Volume Accuracy 2 Flow Rate Accuracy 3 Sam...

Page 74: ...edle printer paper 2088030 XX Sample Prep Kit Capper tool decapper tool 20 bottles 100 caps and seals adapter ring Specify bottle and adapter ring size 2087809 02 Large Volume Adapter w Integrated Sti...

Page 75: ...IAC Operator Manual Appendix C Certifications C 1 Overview This section contains the WEEE statement and any Certificates of Conformity For more information contact a local Hach Ultra representative or...

Page 76: ...ateurs de mat riel lectrique en Europe doivent d sormais retourner le mat riel us ou p rim au fabricant pour limination sans frais pour l utilisateur Remarque Veuillez vous adresser au fabricant ou au...

Page 77: ...ruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen Nota Als u apparatuur voor recycling terugbreng...

Page 78: ......

Page 79: ...izes Tab 27 Fig 3 7 Syringe Settings Screen 29 Fig 3 8 System Settings Screen 29 Fig 3 9 Sound Settings Screen 31 Table 3 3 Sound Tab Field Descriptions 31 Fig 3 10 Tilt Bottle Dock 32 Fig 3 11 Remove...

Page 80: ...40 Print Tab 52 Table 3 5 Functions Affected by Password Security 52 Fig 3 41 Security Settings Screen 53 Fig 4 1 Main Screen 55 Fig 4 2 Main Screen with Red Status Light 57 Fig 4 3 Notes Tab 58 Fig...

Page 81: ...9705 User Notes 81 of 82 KSS March 2006 Edition 1 HIAC Operator Manual User Notes...

Page 82: ...iel lectrique en Europe doivent d sormais retourner le mat riel us ou p rim au fabricant pour limination sans frais pour l utilisateur Remarque Veuillez vous adresser au fabricant ou au fournisseur du...

Page 83: ...van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen Nota Als u apparatuur voor recycling terugbrengt moet u...

Page 84: ...ch Company P O Box 389 Loveland Colorado 80539 0389 USA Phone 800 227 4224 Fax 970 669 2932 techhelp hach com Dieses Informationsblatt enth lt Angaben die ausschlie lich f r den Export dieses Ger tes...

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