Genevac HT-24, User Manual, Page: 46 / 60

Genevac HT-24 User Manual
44
10-1562 Issue 3-7 March 2014
Example 3. Mixture of High and Low Boiling Point Solvents
Method consists of three runs linked together to form a multi stage run, with settings as
follows:
Stage 1
Remove Organic
Phase Stage 2
Dry High BP
Solvent Sage 3
Final Drying
Run No.
1 2 3
Run Data Protection
N N N
Next Run Number (0 for none)
2 3 0
Run Name
High - Low Mix High - Low Mix 2 High - Low Mix 3
Sample Holder Type
Your Holder Your Holder Your Holder
Sample Volume (ml)
Your Volume Your Volume Your Volume
Solvent
DMSO or DMF & DCM DMSO or DMF & DCM DMSO or DMF & DCM
SampleGuard Control Temp (°C)
40 40 40
SampleGuard Control Channel
1 1 1
CoolHeat Enable Pressure (mbar)
50 50 50
Chamber Temperature control (°c)
preheat to 15 preheat to 40 preheat to 30
Rotor Speed
High High Low
Heat-Off Option
Elapsed Time Heat Flow Elapsed Time
Heat-Off Elapsed Time (HH:MM)
01:00 to 1:30 - 00:00
End-of-Run Option
Elapsed Time - Elapsed Time
End-of-Run Elapsed Time (MM:MM)
01:00 to 01:30 - 01:00 to 03:00
Auto Defrost & Drain
Y N Y
Pressure Control Regime
Variable Dri-Pure Full Vacuum Full Vacuum
Dri-Pure Start Pressure (mbar)
750 - -
Dri-Pure End Pressure (mbar)
70 - -
Dri-Pure Ramp Time (MM)_
55 - -
Final Control Pressure (mbar)
65 - -