4 Operation
4.5 Experimental design
42
MicroCal iTC
200
Operating Instructions
28-9639-77
AA
Be sure to insert the syringe in to the sample cell before starting the experiment. The
instrument will seek experimental temperature, equilibrate to that temperature, start
the titration syringe stirring, wait until the DP signal is steady, and then start performing
injections. The raw data will appear in the
Real Time Plot
tab.
Once a run has finished, the syringe and sample cell should be cleaned as soon as
possible.
Procedures after a run
The MicroCal iTC
200
was designed to have its power on for extended periods of time. This
will keep the system electronics at the normal operating temperature. It is
recommended that the power of the MicroCal iTC
200
cell be turned off during extended
periods of down time, such as holidays and vacations.
After use, clean the sample cell following procedure in
Section 4.7
and fill the sample cell
with distilled water. Wash and dry the syringe using procedure in section
Section 4.7
.
4.5
Experimental design
Figure 4-4.
Experimental design dialogue box.
