Endress+Hauser StamoLys CA 71 HY Operating Instructions Manual Download Page 1

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BA362C/07/en/07.06
51517621

Valid as of:
Software version 5.9

Operating Instructions

Stamolys CA71HY

Analyzer for Photometric Determination of Hydrazine

Summary of Contents for StamoLys CA 71 HY

Page 1: ...BA362C 07 en 07 06 51517621 Valid as of Software version 5 9 Operating Instructions Stamolys CA71HY Analyzer for Photometric Determination of Hydrazine...

Page 2: ...meter SCHRITTMOTOR SCHRITTMOTOR LECKF LECKF ALARM 2 ALARM 2 OPTION OPTION ST RUNG ALARM 1 ALARM 1 F5 F4 M 0 2 A M 0 2 A M 0 2 A M 0 2 A COM NC NO COM NC NO Kanal 1 Kanal 1 Kanal 2 Kanal 2 Channel 2 Ch...

Page 3: ...2 Local operation 22 5 3 Calibration 29 6 Commissioning 31 6 1 Function check 31 6 2 Switching on 31 7 Maintenance 33 7 1 Maintenance schedule 33 7 2 Replacing reagents 33 7 3 Replacing pump hoses 34...

Page 4: ...lectrical cables and hose connections are not damaged Do not operate damaged products and secure them against unintentional commissioning Mark the damaged product as defective Faults at the measuring...

Page 5: ...alerts you to hazards They could cause serious injuries as well as damage to the instrument if ignored Caution This symbol alerts you to possible faults which could arise from incorrect operation The...

Page 6: ...er specifications Sample transfer 1 From one measuring point one channel version 2 From two measuring points two channel version Power supply 0 230 V AC 50 Hz 1 115 V AC 60 Hz 2 115 V AC 50 Hz 3 230 V...

Page 7: ...nch 1 6 mm x 3 2 mm 0 06 inch x 0 13 inch 6 4 mm x 3 2 mm 0 25 inch x 0 13 inch 2 T hose connectors of each 1 6 mm x 1 6 mm x 1 6 mm 0 06 inch x 0 06 inch x 0 06 inch 3 2 mm x 3 2 mm x 3 2 mm 0 13 inc...

Page 8: ...supply from canister with standard Hose at rear supply from canister with cleaner a0006574 Fig 2 Analyzer cabinet version without hoses 1 2 3 4 5 Reagent pump P2 supply from canister Display Serial i...

Page 9: ...it reliably against impact and moisture for storage and transportation The original packaging provides optimum protection In addition the permitted ambient conditions must be observed see Technical da...

Page 10: ...6 30 250 9 84 125 4 92 165 6 50 21 0 83 26 1 02 21 0 83 119 4 69 78 3 07 47 1 85 648 25 5 360 14 2 436 17 2 243 9 57 200 7 87 120 4 72 326 12 8 16 0 63 27 1 06 120 4 72 555 21 8 465 18 3 500 19 7 7 11...

Page 11: ...hannel version level monitoring is only possible for one channel One collecting vessel can be mounted on the housing A second vessel would have to be made available near the device a0001363 Fig 6 Coll...

Page 12: ...ws 6 mm 0 24 For the installation dimensions please see the previous chapter 2 Using a spirit level check that the cabinet is hanging or standing straight Only in this way can any air bubbles present...

Page 13: ...itioning using ultrafiltration for contaminated media e g from the primary settling tank For questions regarding sample conditioning and its automation please contact Service or the sales center respo...

Page 14: ...e for both analyzers Bear this in mind when selecting maintenance intervals for CAT430 and when setting the buffer volume at the collecting vessel a0001728 Fig 13 Installation example 1 Sample from CA...

Page 15: ...e frame of the analyzer to reach the terminal block Beforehand release the hoses from the outlet pipe Otherwise there is a danger of flooding Connect the hoses again after folding the frame back in Fo...

Page 16: ...emmen f hren auch bei ausgeschaltetem Ger t Spannung Terminals voltage to ground even when the unit is switched off Terminals voltage to ground even when the unit is switched off V 4 V 4 31 30 29 0V n...

Page 17: ...ready To start measurement the voltage must stay at 0 V for at least 5 seconds Function Designation Terminal One channel version Terminal Two channel version Mains L 3 3 N 2 2 PE1 1 Brass screw with b...

Page 18: ...t analog output 1 and analog output 2 route the cable cores of the two data cables through the interference suppressor 4 2 2 One channel version a0001746 Fig 18 Interference protection of the signal c...

Page 19: ...nished 5 s Analog output l 1 channel 1 0 or 4 mA start of measuring range 20 mA end of measuring range l 2 channel 2 0 or 4 mA start of measuring range 20 mA end of measuring range Channel selection M...

Page 20: ...uired not a crossed one The interface does not have to be configured at the analyzer The following commands can be sent from the PC in order to read out data D Data memory Measured values C Data memor...

Page 21: ...easure the current values at the terminals of the analyzer and not at the PLC DSC or data logger If these current values are correct please check your PLC DCS the data logger and or the electrical cab...

Page 22: ...on Indicator LED function H Auto measuring option Back to the main menu from all sub menus Alarm value 1 exceeded Backwards in the sub menu horizontal see Appendix Alarm value 2 exceeded V Backwards i...

Page 23: ...et been reached or The measuring interval has not yet elapsed Note Measuring flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample coll...

Page 24: ...sults from factors such as reagent aging aging of constructive components etc The calibration factor compensates for these effects CA 71 checks the registered calibration factor logically If the facto...

Page 25: ...for alarm value 2 channel 1 works as an NO or NC contact Alarm value AV 1 2 Two channel version only Setting as to whether the contact for alarm value 1 channel 2 works as an NO or NC contact Alarm v...

Page 26: ...m After each change the instrument does not wait for the measuring interval If the measurement is to start immediately set the time in the past Measuring interval 2 to 120 minutes 10 Time between two...

Page 27: ...automatically deleted If this does not happen automatically error messages can be deleted by quickly switching the analyzer off and back on again 1 flushing 01 01 96 00 00 to 31 12 95 23 59 Time of 1...

Page 28: ...that they run in the same ratio as for filling the sample reagent mixture in measurement mode s stop and g go Note G can only be selected if P1 and P2 are Off The following valve combinations are poss...

Page 29: ...g table provides an overview of the standard calibration data Note Compare these values to your own data After changes in the CONFIGURATION menu and in the event of software updates you can check and...

Page 30: ...value and then press H twice to return to the main menu AUTO MEASURING 6 Press F again This takes you back to the measuring mode The calibration is now carried out automatically Caution After the cal...

Page 31: ...t the device parameters proceed as follows 1 Plug in the analyzer s plug with grounding contact into the socket 2 Press the H key until AUTO MEASURING is displayed 3 Select the CONFIGURATION menu and...

Page 32: ...lect V1 S V2 R with F or K switch to R or S with V and then switch the P1 sample pump on Leave the pump running until you can tell that there is cleaning agent at the T hose connector Switch P1 back o...

Page 33: ...splash and heat may build up If you store the reagents correctly in the dark not over 20 C they will keep unopened for a minimum of 12 weeks from the date of production batch number When this period...

Page 34: ...ple see CONFIGURATION The value determined is saved by the analyzer as the frequency offset 7 Then carry out a calibration see chapter Calibration 7 3 Replacing pump hoses Warning When removing hoses...

Page 35: ...CONFIGURATION and carry out calibration Calibration Caution Make sure you connect the new pump hoses to the correct connections at the T hose connector For the order numbers of the pump hoses see the...

Page 36: ...ack hoses press the black button on the valve and disconnect the hoses 3 Spray the new hoses and valves with silicone spray before inserting them 4 Reverse the sequence of operations to install the ne...

Page 37: ...assemblies Removing the old cell 1 Rinse first with water and then with air see SERVICE 2 Switch the analyzer off 3 Unscrew the four screws on the photometer housing and remove it 4 Release the nuts...

Page 38: ...the instrument out of service thoroughly rinse all the lines with clean water Proceed as follows 1 Remove the reagent and standard hoses from the canisters and immerse them in a tank containing clean...

Page 39: ...HY1 active 1 l Order No CAY540 V10AAE Reagent HY1 inactive 1 l Order No CAY540 V10AAH Cleaner 1 l Order No CAY541 V10AAE Standard 400 g l N2H4 Order No CAY542 V10C50AAE Note Please note the disposal i...

Page 40: ...reagents Standard dosing defective Check the valves for contamination obstructions visual inspection Replace valve hoses if necessary Incorrect photometer Check the setting in the CONFIGURATION menu...

Page 41: ...lush with 12 5 bleaching lye first and then with 5 hydrochloric acid Measured values inaccurate Standard is dosed to the sample Check the valves and valve settings Replace valve hoses if necessary Cou...

Page 42: ...nt precipitation EDTA not with CA71HA Not enough sample conditioning Shorten the cleaning intervals of sample conditioning Error Possible cause Tests and or corrective measures a0006410 Fig 24 Overvie...

Page 43: ...512088 Item Spare part Order number 130 133 Maintenance kit CAV740 1 set of pump hoses blue yellow item 113 12 piece 51506434 1 set of pump hoses black black 12 piece 51506497 1 pack of hose connector...

Page 44: ...SI Shortened reaction time AM C 90 s SI A 0 Hz signal error only after 90 s Reason for crashing during frequency display in SERVICE eliminated Restart after power failure BA364C 07 xx 06 04 03 2004 5...

Page 45: ...ent consumption Approx 0 2 A at 230 V Approx 0 5 A at 115 V Fuses 1 x slow blow 0 5 A for analyzer electronics 2 x semi delay 0 2 A for photometer Time between two measurements tmeas reaction time rin...

Page 46: ...pplied Degree of protection IP 43 Sample temperature 5 to 40 C 40 to 100 F Sample flow rate Min 5 ml min 0 0013 gal min Consistency of the sample Low solid content dry matter 50 mg l ppm Sample inlet...

Page 47: ...Stamolys CA71HY Technical data Endress Hauser 47...

Page 48: ...Appendix Stamolys CA71HY 48 Endress Hauser 11 Appendix 11 1 Operating matrix One channel version a0001907 en...

Page 49: ...Stamolys CA71HY Appendix Endress Hauser 49 a0001908 en...

Page 50: ...Appendix Stamolys CA71HY 50 Endress Hauser Two channel version a0001909 en...

Page 51: ...Stamolys CA71HY Appendix Endress Hauser 51 a0001910 en...

Page 52: ...131 132 133 134 10 pieces each C Flex hose for valves 1 40 m Quantity Order No Designation CAY540 V10AAE Reagent HY1 active 1 l CAY540 V10AAH Reagent HY1 inactive 1 l CAY541 V10AAE Cleaner 1 l CAY542...

Page 53: ...51506491 10 T hose connector 6 4 mm x 6 4 mm x 6 4 mm 51506493 10 Hose connector 6 4 mm x 6 4 mm 51506494 133 10 Hose connector 3 2 mm x 6 4 mm 51506492 134 10 Y hose connector 1 6 mm x 1 6 mm x 1 6...

Page 54: ...tion Delay to sample s Analog output 0 20 mA 4 20 mA AV 1 NC NO AV 2 NC NO Error contact NC NO Frequency offset Hz Zero frequency base line dist water without reagent Hz Measuring range start mg l g l...

Page 55: ...sing Filling time Reaction time RPM K floating mean N Points C1 mg l g l F 1 Hz C2 mg l g l F 2 Hz C3 mg l g l F 3 Hz C4 mg l g l F 4 Hz C5 mg l g l F 5 Hz C6 mg l g l F 6 Hz C7 mg l g l F 7 Hz C8 mg...

Page 56: ...Appendix Stamolys CA71HY 56 Endress Hauser 11 4 Maintenance schedule a0001911 en...

Page 57: ...Housing GFR 10 Stainless steel 9 Without 10 I Icons 5 Incoming acceptance 9 Input 45 Installation 4 8 Examples 14 Installation instructions 9 12 Interference suppressor 18 39 L LANGUAGE 27 Level monit...

Page 58: ...Valve hoses 36 Return 4 44 S Safety conventions 5 Scope of delivery 7 Serial interface 20 SERVICE 28 Shielding 18 Signal connections 18 Software history 43 Spare parts 42 Stainless steel housing 9 Sta...

Page 59: ......

Page 60: ...www endress com worldwide BA362C 07 en 07 06 Printed in Germany FM SGML 6 0 DT 51517622...

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