Drawell DW-TY-9900 Operation Manual Download Page 1

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COMPANY NAME

DW-TY-9900 Inductively Coupled Plasma Atomic Emission

Spectrometer

Operation manual

DRAWELL INTERNATIONAL TECHNOLOGY LIMITED

Chongqing Center

: Suite 2605,Building No.11,Shiyou Road No.1, Yuzhong District, Chongqing, China.

Tel

: 0086-023-63268643

Shanghai Office

: Suite 1101,Lane561 XiuChuan Rd.,PuDong New Area,Shanghai,China

Tel

: 0086-021-50966080

Homepage

: www.drawell.com.cn

Summary of Contents for DW-TY-9900

Page 1: ...manual DRAWELL INTERNATIONAL TECHNOLOGY LIMITED Chongqing Center Suite 2605 Building No 11 Shiyou Road No 1 Yuzhong District Chongqing China Tel 0086 023 63268643 Shanghai Office Suite 1101 Lane561 X...

Page 2: ...iary Material Configuration 4 2 2 1 Stable Power Supply System 4 2 2 2 Power Requirements 4 2 2 3 Grounding Requirements 5 2 2 4 Gas Requirements 5 2 2 5 Cooling Water Requirements 5 2 2 6 Exhaust Req...

Page 3: ...ucts include chemical reagents inorganic materials cosmetics oil gasoline diesel lubricating oil C5 and other synthetic gasoline raw materials oleic acid petroleum catalysts urea solutions 8 Food and...

Page 4: ...nts to ensure the accuracy and sensitivity of the instrument 3 Small matrix effect 99 of the samples do not need to separate the matrix 4 Wide measurement range analysis from ultra micro to constant 5...

Page 5: ...a generally the room temperature is required to be maintained at a fixed temperature between 25 3 and the temperature change should be less than 1 h If the ambient humidity is too high optical compone...

Page 6: ...pply transformer Try not to share a power supply line with large motors large ventilators air conditioners muffle furnaces and other large electrical equipment In order to avoid large fluctuations in...

Page 7: ...ng the smart cooling water tank add 35 liters of distilled or purified water to the PVC water tank of the cooling water tank 2 2 6 Exhaust Requirements The gas exhausted by the plasma chamber is mainl...

Page 8: ...9900 ICP AES from left to right are main ICP power socket ground wire cooling water inlet and outlet two parts plasma gas and carrier gas inlets Fig 1 Fig 3 1 Schematic diagram of the installation po...

Page 9: ...w direction it is open Plasma gas and carrier gas inlet in the picture they are respectively connected to the argon cylinder with a 6 PU tube through an oxygen pressure reducing regulator Fig 3 2 Circ...

Page 10: ...her is the serial port for communication with the computer The power port is directly connected to the 220V power socket and the serial port needs to be connected to the RS232 interface on the back of...

Page 11: ...Trainees should carefully read the operating instructions understand the functions of the various knobs of the instrument and be familiar with the operating methods and steps of the instrument and the...

Page 12: ...ealing ring 2 Sets 1 big 2 small 9 Waste bottle 2 Pcs 10 Torch clamp 2 Pcs 11 Temperature controlled cooling circulating water tank 1 Set 12 Exhaust system 1 Set Axial Fan 13 Host power cord waterproo...

Page 13: ...joint 4 Pcs 27 Direct connection 2 Pcs 6 28 Tee 2 Pcs 6 29 Argon cylinder pressure relief valve outlet connector 2 Pcs Stainless steel quick coupling with trachea 30 Copper plate copper rod and copper...

Page 14: ...y scan change level of light to find zero light select the building method After the analysis of the capillary into the next measurement method of peak search of the standard peak active the looking f...

Page 15: ...cts of the title bar shows the current method name the figure shows the ICP Analysis HG The second line is the menu bar A total of six drop down menu options daily use of measurement including three d...

Page 16: ...15 In the new method enter the method name The following window appears determined...

Page 17: ...16 OK displays the following window...

Page 18: ...ach element needs its own standard input is enter the value you are prepared and STDHIGH STDLOW value your configuration or converted units completed in the daily analysis we need only follow the step...

Page 19: ...18 attenuation measurement standards measure the sample Selection Method...

Page 20: ...19 Double click or select the following points to determine Measurement automatic searching for peak peak with the preparation of standard solution actively look for a good looking peak...

Page 21: ...20 Automatic peak search...

Page 22: ...tenuation measurement in the analysis using standard solutions prepared from standard to high attenuation as shown below The first method requires the establishment of the future does not need automat...

Page 23: ...22 Measurement standards in the analysis and measurement of the sample analysis sample to select multiple windows Testing standards...

Page 24: ...23...

Page 25: ...24 After you finish testing the standard point of exit to save Test sample...

Page 26: ...25 Historical database free to choose to print to analyze data hold down the Ctrl key point to print the number...

Page 27: ...26 Test results and historical data...

Page 28: ...onals can make the sample case tracing the edit icon in the View view of spectrum The line spectrum is easily to identify whether the interference see the letter back ratio can be set to automatically...

Page 29: ...nd that there is a lot of dirt at the nozzle or the center channel is blocked It needs to be used 1 1 acid soaking for 2 hours and then rinsed with pure water and dried 8 Whether the atomizer enters t...

Page 30: ...g if the power is frequently on and the main control board is likely to burn if it rains and thunders 5 2 Precautions for Turn On Off Before turn on the measurement you need to make various preparatio...

Page 31: ...on the working coil such as the torch the high voltage power supply must be turned off or the ICP power supply 2 When performing maintenance on the power box the operator must shut it down for 30 minu...

Page 32: ...tactor is damaged or the auxiliary contact wiring is disconnected falling off etc Replace the contactor or restore the normal connection after finding the wiring fault High voltage cannot be turned on...

Page 33: ...ite re ignite after preloading gas Air leakage at the junction of pipe and atomizer Tighten the connector if the atomizer is damaged contact the manufacturer for replacement Insufficient tube power Re...

Page 34: ...pipe connecting the ICP and the water tank Open the ICP back shell Open the high frequency box and gradually remove the parts connected to the tube After changing the tube install it again Reconnect...

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