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11

4 Photometry 

4.1 Measuring the Concentration 

1. Prepare the meter to receive the cell size of choice (See Section 3.2)
2. Turn the meter on by pressing the 

ON/OFF

 key. 

3. Press the 

-M- 

key until Photometry\Concentration is displayed on the top line of the display. After the first

concentration measurement, the last program used is automatically displayed. 

Photometry\Concentration

Photometry\Concentration

#

 

Select program

     with <PROG>

#

 

Select program

     with <PROG>

    

or with 

 

 

15: K1503

NH3-N

13 mm

0.00 - 7.00 mg/l

11.30.13 15:12

11.30.13 15:12

               

First concentration measurement (#1)

        

All subsequent concentration Measurements (#2)

NOTE

:

From display #2 above, use the 

FORM

 key to change the chemical form being reported for the program

displayed and use the 

UNITS

 key to change the reporting unit. (See Section 1.3).  

4. Use the 

 or 

 keys to toggle through the last ten programs used or press the 

PROGRAM

 key and enter the

desired program number, then press 

START/ENTER

.  

5. Zero adjustment (zeroing the photometer at all wavelengths) is required each time the meter is turned on,

unless the photometer is docked in a Power LabStation (See Section 1.7).  Zero adjustment must employ the
cell size for the test that is being run (See Section 1.6). If zeroing is necessary, the required cell size and the

following message are displayed:  “ 

 No valid zero adjustment is available”. The user is prompted to

 

i

 

perform the zero adjustment. The prompts are highlighted across the bottom of the display. To proceed to
each next prompt, press 

START/ENTER

.

NOTE

:

To perform the zero adjustment for Vacu-vials® Test Kits, use the factory sealed ZERO ampoule supplied with
each kit. For 

MDL+ 

Test Kits, fill a sample cell with distilled water to perform the zero adjustment.  

6. In addition to zero adjustment, some programs also require a reagent blank (indicated in the individual kit

instructions):

#

If a blank measurement 

has NOT 

previously been made (stored) for a program, the menu prompts the

user to measure a blank value. The prompts are highlighted across the bottom of the display. To
proceed to each next prompt, press 

START/ENTER

.

#

If a blank measurement 

has

 previously been made (stored) for a program, the previously stored blank

value will automatically be applied to the new sample measurement unless the user deletes or changes
the blank value. To delete the old blank value or generate a new blank value, press the 

CAL/ZERO

 key

and follow the choices/prompts.

NOTE

:

When a blank value has been applied to a test result, [BV] is displayed on the screen with the test result.

Photometry\Concentration

0.74

[BV]  

mg/l

187: K9903

Zn

13 mm

0.00 - 3.00 mg/l

11.30.13 15:12

7. Insert the clean, dry sample vial or ampoule as prompted and press 

START/ENTER

. The test result is

displayed.  

NOTE

:

If the measured test result is above the upper limit of the test range, the display will show > XX ppm. However,
immediately above that in a smaller font, the actual test result will be displayed

Summary of Contents for V-3000

Page 1: ...OPERATOR S MANUAL V 3000 PHOTOMETER CHEMetrics Inc 4295 Catlett Road Midland Virginia 22728 Toll Free 1 800 356 3072 Phone 540 788 9026 Fax 540 788 4856 Web www chemetrics com Jan 18 Rev 8...

Page 2: ...3 1 Turning the Photometer On 8 3 2 Inserting a Cell 8 3 3 Operating Modes 9 3 4 Navigation 9 3 5 Menu Overview 10 4 Photometry 4 1 Measuring the Concentration 11 4 2 Analysis Timer 12 4 3 Timer 12 4...

Page 3: ...ic Range 0 200 to 2 000 absorbance units Operating Temperature 0EC to 50EC Humidity 75 Yearly Mean up to 30 days at a maximum of 95 Waterproof IP67 Power Supply 4 X 1 5 V AA approximately 5000 measure...

Page 4: ...entration direct read mode toggle through available chemical forms for a particular analyte example NH3 NH3 N NH4 UNIT key In Photometry Concentration direct read mode toggle through available reporti...

Page 5: ...g l Measured value with unit 15 K1503 NH3 N Program no Catalog no and Chemical form 13 mm 0 00 7 00 mg l Diameter of the cell and measuring range 11 30 13 15 12 Status line with date and time 1 5 Sock...

Page 6: ...Y 436 0 40 0 Ferric Thiocyanate Chlorine 32 K 2513 13 N 517 0 5 00 DPD Chlorine 33 K 2523 13 N 517 0 5 00 DPD Chlorine Dioxide 37 K 2703 13 N 517 0 11 00 DPD Chromate 42 K 2803 13 N 557 0 3 50 as CrO...

Page 7: ...0 as NO3 Cadmium Reduction Nitrite 125 K 7003 13 N 517 0 1 00 as N Azo Dye Formation Ozone 133 K 7423 13 N 517 0 5 00 DPD Oxygen 140 K 7503 13 N 610 0 2 00 Indigo Carmine Oxygen 141 K 7513 13 N 517 0...

Page 8: ...hargeable Battery Pack PC Interface Cable 9 pin to 9 pin The Power LabStation provides the following features When the photometer is placed in the Power LabStation which is plugged into an electrical...

Page 9: ...when the photometer is not in use To install batteries carefully loosen the two screws on the battery compartment on the back of the instrument Remove the battery compartment cover and insert the four...

Page 10: ...the dust cover is pushed upward Insert a 28 mm cell into the sample compartment using downward pressure to ensure that it is fully seated Inserting a Vacu vials Ampoule 13 mm Requires installation of...

Page 11: ...ed in the status line of the display There are choices for date format presentation day month year dd mm yy or month day year mm dd yy When storing measured values and calibrating the current date and...

Page 12: ...ay RS232 Download Data Filter Filter ID Program Date Delete of 100 occupied i Filter No filter i Display Illumination Auto off On Off Contrast 0 100 Brightness 0 100 Reset Restore basic settings Inter...

Page 13: ...d to i perform the zero adjustment The prompts are highlighted across the bottom of the display To proceed to each next prompt press START ENTER NOTE To perform the zero adjustment for Vacu vials Test...

Page 14: ...s line of the display When the selected time expires the meter beeps Press START ENTER to stop the beeping 4 4 Measuring Diluted Samples If the concentration of a sample exceeds the measuring range of...

Page 15: ...ured value memory capacity is full the meter will offer the option to overwrite the oldest stored measurement with the new storing command Another option is that all stored values can be deleted using...

Page 16: ...1 55 06 0 15 NH3 N 4 50 mg l VALID Description of data separated by semi colons in CSV format Data storage number Date of storing Time of storing User assigned ID Program number only for the concentra...

Page 17: ...fer Click on Capture Text Enter the path and name of the file created in Step 1 Click on Start 12 Make sure that the desired V 3000 output format has been chosen See Section 6 1 13 To download individ...

Page 18: ...es varies among different operating systems and individual PCs Consult with an IT Specialist for detailed instructions 3 With the V 3000 power off connect the V 3000 to the computer using the supplied...

Page 19: ...Error uploading method update Never press cancel during a method update Contact CHEMetrics for assistance Program number invalid Program number not recognized Only use program appropriate program numb...

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