Bruker NMR, User Manual

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Getting Started
16 Z33085_2_002
Monitoring Mode
The following steps need to be performed:
• Insert sample.
• Tune and match by using the
atma command.
• Lock-in – temperature appears.
• Topshim.
• Selftune.
Figure 4.9: Selftune in Progess.
• Edte – disable NMR Thermometer (if not already done).
• Change target temperature (
edte for instance, a 10K temperature jump).
As an exercise we will perform a temperature jump (e.g. 10K) and follow the different
temperature and other BSMS values (flow/heater) in the monitoring window (
edte -
Monitoring, as well as, activate NMR Sensor Temperature, NMR Thermometer, Target
Temperature, Current Power etc.).
4.3.1