Bruker Anton Paar, User Manual

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List of Figures
DOC-M88-EXX268_V1_12.2016 7
List of Figures
Figure 2.1: Temperature dependence of lattice parameter a0 of MgO...................................... 23
Figure 3.1: Mounting the Edwards turbomolecular pump to the flexible bellow......................... 28
Figure 3.2: Connecting the vacuum tube to the HTK 1200N chamber ...................................... 28
Figure 3.3: Mounting the Edwards backing-pump to the flexible vacuum line ........................... 29
Figure 3.4: Back sides of: Edwards turbomolecular instrument controller (TIC, left side) and
Edwards relay box (right side) ................................................................................
30
Figure 3.5: Starting screen for the TIC Controller ...................................................................... 31
Figure 3.6: Vacuum sensor, flooding valve, tube to chamber and mist-filter mounted .............. 32
Figure 3.7: Display and backside of the vacuum indicating instrument ..................................... 33
Figure 4.1: Rocking curve to check chamber rotation error ....................................................... 38
Figure 4.2: Final position after rotation correction...................................................................... 39
Figure 4.3: Insert a deflection angle in CONFIGURATION for the temperature stage .............. 40
Figure 4.4: Z-scan over a wide range to roughly determine the right sample height ................. 41
Figure 4.5: More accurate Z-scan to determine the right sample height ................................... 42
Figure 4.6: Rocking curve at correct sample height................................................................... 43
Figure 4.7: Inserting the temperature depending Z-positions .................................................... 46
Figure 5.1: Removing the covers for rack mounting .................................................................. 47
Figure 5.2: Fixing the guide bars on both sides of the Paar controller....................................... 47
Figure 5.3: Removing the supporting feet for rack mount.......................................................... 48
Figure 6.1: HTK 1200N mounted on a goniometer .................................................................... 50
Figure 6.2: Red dots for the bayonet fixture in the “locked” position.......................................... 51
Figure 6.3: Fixing screws for the TTK 600 adapter.................................................................... 51
Figure 6.4: HTK 1200N mounted on a goniometer .................................................................... 52
Figure 6.5: TCU series controller with built-in Eurotherm 2604 controller ................................. 53
Figure 6.6: CCU series controller............................................................................................... 53
Figure 6.7: Front view of TCU110C mounted in a D8 DISCOVER ............................................ 54