September 21
st
, 2021
Version 1.1
Page 1: ...September 21st 2021 Version 1 1...
Page 2: ...nent Identification 3 Menu Structure 5 Chapter II Specifications 10 Models 10 Performance 10 Sample Requirements 10 Solvent Requirements 10 Signal Inputs Outputs 11 Utility Requirements 11 Analyzer En...
Page 3: ...Factory Setup 32 Chapter V Normal Operation 33 Main Run Screen 33 Signal Outputs 34 Alarms 35 Solvent Supply 36 Taking the Analyzer Offline 36 Validation 37 Sample Streams 39 Loss of Power Restart 39...
Page 4: ...P 600 SIC Analyzer Manual Assembly Drawings 49 Chapter VII Spare Parts 53 Spare Parts Kits 53 Replacement Parts 54 BARTEC ORB 4724 South Christiana Avenue Chicago IL 60632 USA...
Page 5: ...cident or improper application or installation Any product not used in accordance with the instructions furnished by Bartec Orb Freight charges to return merchandise to Bartec Orb Freight charges on e...
Page 6: ...600 SIC Analyzer Manual Foreword ii Revision History Rev Description Changes Date 1 0 First version of the new Manual May 22nd 2020 1 1 Revised Spare Parts Numbers Added Solvent Fill September 21st 20...
Page 7: ...m micro volume solenoid valves and a measurement chamber equipped with a high resolution conductivity probe and temperature control Measurement chamber temperature is monitored and held constant at a...
Page 8: ...ment cycle Cleaning frequency is adjustable See State Table in Chapter IV Figure 1 1 Analyzer Flow Schematic Figure 1 2 Sample Spider Valve Flow Air OUT to Pumps Drain atm Air IN Sample IN Sample OUT...
Page 9: ...0 SIC Analyzer Manual Chapter I Introduction 3 Figure 1 3 Solvent Flow Schematic Component Identification Figure 1 4 Upper Control Enclosure 5 psi Air IN Air IN Filling Pumps and Ports Maintenance Val...
Page 10: ...P 600 SIC Analyzer Manual Chapter I Introduction 4 Figure 1 5 Front View...
Page 11: ...Submenu Items Choices Settings Comments Analyzer Status Online Offline Alarm History Reset Reset Alarms log Validation History Reset Req Valid Reset Validation log Request Validation Service Sys Temp...
Page 12: ...operation of relays Setup Output Settings 4 20mA Outputs 4 20 Out 1 Type 4mA 20mA Offset 4 20 Out 2 Type 4mA 20mA Offset Graphics Clear All Period Salt in Crude Cell Temp Conductance Validation Progra...
Page 13: ...onc Units Temp Units Stdby Mode Come Read Num Cycles Max Cycles Validation Value Margin Offset Stream Select Type Rinse Time Str 1 Reps Str 2 Reps Digital Inputs Cust Al Rem Stdby Valid Strm Sel Scree...
Page 14: ...tings 9600 19200 38400 Modbus TCP IP settings Analyzer s IP address Router Address Network Mask State Table Setup Reset Defaults Line State Type Data Loads default state table 1 16 states Wait Clean M...
Page 15: ...P 600 SIC Analyzer Manual Chapter I Introduction 9 Main Menu Submenu Items Choices Settings Comments Setup Factory Setup For factory use only Security Disable Enable...
Page 16: ...y Accuracy 0 5 of full scale Temperature Accuracy 0 1 C 0 2 F of full scale Operating Temperature Range Minimum 20 C 4 F Maximum 40 C 104 F Sample Requirements Sample Conditions Homogeneous single pha...
Page 17: ...mable Modbus Optional Ethernet TCP IP or RS 485 RTU Consult Bartec Orb for details Utility Requirements Power 110 120VAC 10 50 60 Hz 5A 230 240VAC 10 50 60 Hz 2 5A Purge Gas Supply Clean dry instrumen...
Page 18: ...ding rack housed It should be located on a flat vertical surface and isolated from intense vibration Ample space should be provided on all sides of the analyzer for access to connections solvent reser...
Page 19: ...P 600 SIC Analyzer Manual Chapter III Installation and Startup 13 Figure 3 1 Dimensional Drawing...
Page 20: ...ck for the measurement and cleaning solvents see Figure 3 4 These reservoirs will hold approximately 36 liters 9 5 gallons each of liquid The reservoir filling ports are located at the top front of ea...
Page 21: ...his purpose The solvent lines are bled as follows 1 Place a suitable container under the bleed tube associated with the valve 2 Rotate the 3 way valve 180 so that the handle points to the left away fr...
Page 22: ...OWER WARNING This Analyzer is designed to meet the requirements of either the National Electrical Code NEC for installation in CSA CUS Class I Division1 Group B C and D or ATEX II 2G Ex db IIB H2 T6 G...
Page 23: ...ections box attached to the upper left of the top enclosure see Figure 3 2 CAUTION It is the installer s responsibility to verify that the jumpers on HD2 798112 Rev B in Customer Connection Box are co...
Page 24: ...ction is made in the Customer Connections Enclosure Figure 3 5 Serial communication operates at a selectable baud no parity 8 start bits 1 stop bit Data is comma delimited and output in the following...
Page 25: ...tion Request This connection is used to initiate a validation cycle Stream Select This connection is used to switch to Stream 2 sample Low Naphtha This connection is used for Analyzer s operation Low...
Page 26: ...fy that sample supply pressure is between 2 and 10 bar 29 and 145 psi Check for sample leaks at external connections and within the measurement enclosure itself 5 Apply power to the Analyzer NOTE Upon...
Page 27: ...he atmospheric drain is working 11 You are now ready to run analysis using the factory default settings or program the instrument with your desired operational parameters see Chapter IV Programming 12...
Page 28: ...between Main Menu and Main Run screen It is also used to decline window messages Index Key scrolls through the various items available within a specific screen The active menu line is highlighted whi...
Page 29: ...provides access to the Validation History which lists validation measurements that have been performed Validation is described in further detail in Chapter V Normal Operation Touch the Enter key to a...
Page 30: ...d a password must be entered to gain access to the various menus Setup Submenu The Setup submenu is used to enter the Analyzer s various settings screens Use the Index key to move to the desired highl...
Page 31: ...menu selection allows you to offset the analog output signal by the programmed value For example if the offset is set to 1 5 the Analyzer will generate an analog signal corresponding to 10 5 when the...
Page 32: ...exceeds the indicated value Low This menu item allows you to establish a low alarm level Salt concentration measurements below this value generate a warning alarm signal message Analysis will continu...
Page 33: ...s you to select the temperature scale The choices are C or F Stdby Mode this controls how the Analyzer will operate upon application of power When OFF is selected the instrument will begin performing...
Page 34: ...ore performing analysis to make sure the new stream sample reached the Analyzer Digital Inputs These menu items allow you to enable and disable the Analyzer s customer controlled digital inputs NOTE A...
Page 35: ...assed Conditions This designates whether the alarm relay will energize or de energize when an alarm condition is detected When Normal is selected power will be applied to the relay when an alarm condi...
Page 36: ...this port 9600 19200 38400 Ethernet Setup This allows you to configure the Analyzer s IP router and network mask addresses when Ethernet Modbus communications is selected Our IP Address This is the I...
Page 37: ...ly mix the crude solvent mixture It is set in seconds Read This step is used to read and calculate the SIC value The programmed time period associated with this step allows the reading to stabilize It...
Page 38: ...The selections are US month day year or EU day month year Touch the Up Down Arrow keys to change the displayed value Date This menu item allows you to program the Analyzer with the current date To ch...
Page 39: ...asurement data are displayed in either PTB or mg liter and are updated at the end of each measurement cycle Date Time The current date and time as tracked by the Analyzer s internal calendar and clock...
Page 40: ...A second analog output is available as an option RS 232 Serial Output The Analyzer can output an RS 232 serial signal to capture and log measuring information Data are output according to the followin...
Page 41: ...es settings Maintenance Informative Validation Requested Validation cycle has been requested Informative Validation in progress Analyzer is in validation cycle In Validation Informative Remote Standby...
Page 42: ...e event that either the flow of xylene or alcohol is disrupted salt in crude analysis will stop and a critical alarm will be issued If the flow of naphtha is disrupted a warning alarm will be issued a...
Page 43: ...tem Settings Screen 8 PTB Programmed Margin In System Settings Screen 1 PTB Results from Validation Test 1 6 9 7 6 6 8 8 4 9 1 FAIL Results from Validation Test 2 6 9 7 6 7 9 PASS Request of Validatio...
Page 44: ...rially it would be as shown below Pre Rinse State The analyzer allows the user to program in a time period for a pre rinse command This variable is located in the Factory Setup menu This will allow th...
Page 45: ...ntrol room digital input contact closure see Chapter III When the signal is removed the instrument goes back to analyzing stream 1 The Analyzer can also be programmed to alternate between two streams...
Page 46: ...al sample leak occur accumulation of fluid in the bottom of the enclosure activates the leak detector and immediately removes power from the Measurement and Control enclosures To restore power once th...
Page 47: ...ing the instrument s enclosures WARNING To prevent injury the Analyzer must be shut off from the process Personnel must avoid contact with hot equipment or sample Recommended Routine Maintenance Sched...
Page 48: ...ully pour your solvent into the tank Use the color coded liquid level indicators on the tank s front face as a guide Repeat for other tanks as necessary The tanks hold roughly 10 gallons 37 8 liters R...
Page 49: ...tions Service and Operational Checks The P 600 Salt in Crude Analyzer incorporates a special Service screen from which the operator can perform a variety of verification and diagnostic functions inclu...
Page 50: ...6 1 Naphtha SOV3 controls the flow of xylene or naphtha to Alcohol SOV2 Purge Valve controls the solenoid that pressurizes the detection cell Mixer Valve controls the flow of instrument air to the sam...
Page 51: ...up down arrow keys to increase decrease the output value NOTE The Analyzer must be equipped with the optional second 4 20mA output in order for the 4 20 Out 2 menu item to function Conductivity System...
Page 52: ...able clear the whole table SiC Offset offset applied to the final measurement result 5 0 to 5 0 Entries number of data point for calibration table SiC Salt in Crude concentration value y point Conduct...
Page 53: ...e lab Use the following formula to calculate higher Salt in Crude concentration data point Slope Conductance Conductance SiC SiC Intercept 15 8 zero point Calculated Conductance Desired SiC x Slope In...
Page 54: ...w No sample Faulty electrode Check sample line for blockage and clear as required Check sample valve for proper operation and replace as required Check and replace as required Salt concentration resul...
Page 55: ...ket 4 1 701389 Measurement Assembly 5 1 650019 4 way Air Solenoid Valve 6 1 650218 1 8 Quik Connect Elbow 7 1 650219 1 8 Quik Connect 8 1 650199 4 way Air Solenoid Bracket 9 1 650184 6 port Spider Val...
Page 56: ...50 STEPPER MOTOR ASSEMBLY Item No Quantity Part Number Description 1 1 702654 SIC Stepper Motor Assembly 2 5 651139 3 Way Solenoid 4 1 700100 Optical PCB 5 1 640001 Stepper Motor 8 1 702213 Syringe A...
Page 57: ...Power Distribution PCB 1 2 2 620038 Power Supply 24 VDC 1 2 3 620037 Power Supply 5 12VDC 1 3 701911 Fish Paper for Main PCB 1 4 620076 Line Filter 1 5 700318 Main PCB 1 6 620081 RTD Input Module 0 1...
Page 58: ...ty 13 701321 Keypad Overlay 1 14 798030 Magnetic Keypad 1 15 620600 Backlight Driver PCB 1 16 700348 Magnetic Pencil Holder 1 17 700701 Magnetic Pencil Assembly 1 18 798063 Display Controller PCB 1 19...
Page 59: ...139 4 way Solenoid 1 each 650019 Drain Solenoid 1 each 651006 5 mL Syringe 2 each 690024 Salt in Crude Tubing Kit 1 each 700633 2 YEAR PARTS KIT 700642 3 way Solenoid 5 each 651139 4 way Solenoid 1 ea...
Page 60: ...ght Driver PCB 1 620600 Cable Assembly 1 700289 Main Control PCB 1 700318 Power Supply 24 VDC 1 620038 4 way Solenoid 1 650019 Drain Solenoid 1 651006 Spider Valve 1 650184 5 mL Syringe 1 690024 Salt...
