
CHAPTER 13 Dummy cell
81
C H A P T E R 1 3
Dummy cell
External dummy cell
A successful dummy cell test confirms that the controller, including the cell
cable, functions properly. If the result of the noise measurement with the
dummy cell is within specs, the controller is excluded in a trouble shooting
procedure.
The dummy consists of a resistor (R) of 300 M
and a capacitor (C) of 0.47
F in parallel. The current is measured over the resistor according to Ohm’s
law (V = I x R), hence with a working potential of 800 mV the current drawn
will be about 2.67 nA. Slight differences as to this (ideal) value are due to the
tolerance of the resistor (± 1%). The capacitor functions as a ‘noise
generator’ and in fact resembles the capacitance of a well-functioning VT-03
flow cell in an ideal HPLC set-up.
The noise generated via the dummy should be less than 2 pA if the filter of
the controller is set to off, provided that the dummy is within the fully closed
Faraday shield at the same position as the flow cell (see Table XII for
settings). With a 1 second risetime the noise should be better than 1 pA.
Table XII. Dummy cell test settings.
Parameter
Setting
Cell potential 800 mV
Cell current
2.67+/- 0.05 nA (read-out)
Oven
30 °C, stable
Filter
off (or as specified)
Range
100 pA/V
The results of the dummy test must be comparable with the test sheet
supplied with your controller. If not, please consult your supplier.
Summary of Contents for DECADE II 171
Page 12: ...12 DECADE II user manual ed 11...
Page 18: ...18 DECADE II user manual ed 11...
Page 32: ...32 DECADE II user manual ed 11...
Page 48: ...48 DECADE II user manual ed 11...
Page 54: ...54 DECADE II user manual ed 11...
Page 71: ...CHAPTER 8 Optimisation of working potential 71...
Page 72: ...72 DECADE II user manual ed 11...
Page 76: ...76 DECADE II user manual ed 11...