Device User’s Guide
8. Synchronization with other instrument
28
③
Since the absorbance will be measured, set the instrument in the same way as
Absorbance/Transmittance measurement example: 1. Using cuvette.
④
Warming up the light source in the same way as example: 1.
⑤
As shown in Figure8-1, set the reference solution in a dedicated quartz cuvette and
set it in the cuvette holder. Set the working electrode, counter electrode, reference
electrode in the cuvette. Open the shutter and acquire the reference spectrum
(
※
)
.
⑥
Close the shutter and acquire the dark spectrum
(
※
)
.
⑦
Open the shutter, fill the reference solution and the sample to be measured, set the
electrode and set it on the cuvette holder. Connect the cell cable from Model 2325
Bi-Potentiostat to the corresponding working, counter and reference electrode,
respectively.
⑧
Set the measurement conditions of
Strip Chart
or
Time Sequence
to be measured
from SpectraSmart.
⑨
Select
SW Level Trigger
or
SW Continuous Trigger
in the trigger setting and put it in
the measurement standby state.
⑩
Model 2325 is set to transmit external signals of 0 V before and after measurement
and 5 V during measurement. Open the
Setup
screen of Model 2325 software. In the
case of model 2325, as shown in Fig. 26, enter "Rotation speed (rpm)" of "RDE
setting" as 5000, check "RDE rotation" under "Measuring", and click "OK".
Figure 8-5: Model 2325 setup screen
