Agilent Technologies G1330B Reference Manual Download

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Specifications

Performance specifications of the ALS
thermostat

Summary of Contents for G1330B

Page 1: ...s2 Agilent 1100 Series Autosampler Thermostat Reference Manual...

Page 2: ...ange without notice Agilent Technologies makes no warranty of any kind with regard to this material including but not limited to the implied warranties or merchantability and fitness for a particular...

Page 3: ...Reference Manual Agilent 1100 Series Autosampler Thermostat...

Page 4: ...tive Reference Manuals This supplemental manual describes only the parts of the autosamplers that are different from the standard versions The manual describes the following installing the thermostatt...

Page 5: ...hermostat 19 Site requirements and installation of the G1330B thermostat 19 Site Requirements 20 Power Consideration 20 Power Cords 20 Bench Space 21 Environment 21 Unpacking the Autosampler 23 Damage...

Page 6: ...ted Autosampler 40 Troubleshooting and Test Functions 41 The thermostatted autosampler s built in troubleshooting and test functions 41 Status Indicators 42 Error Messages 42 Status Indicators 43 Powe...

Page 7: ...9 Exchanging the Power Supply Fuses 60 Removing the Top Cover and Foam 61 Exchanging Heat Exchanger Fan 63 Exchanging the Heatsink Fans 65 Exchanging the Sensors 67 Exchanging the TCA board 70 Assembl...

Page 8: ...ntents Specifications 83 Performance specifications of the ALS thermostat 83 Performance Specifications 84 Safety Information 90 Radio Interference 93 Sound Emission 93 Agilent Technologies on Interne...

Page 9: ...1 1 Theory of Operation Theory of operation of mechanical hardware electronics and instrument interfaces...

Page 10: ...s holds either 100 1 8 ml vials or two wellplates and 10 1 8 ml vials The ALS thermostat contains Peltier controlled heat exchangers A fan draws air from the area above the sample vial tray of the aut...

Page 11: ...ry of Operation Introduction to the Thermostatted Autosampler Figure 1 Overview of the ALS Thermostat Power Supply TCA Board Heat sink fans Heat exchanger Fan Condensation leak drain Heat exchanger He...

Page 12: ...mperature setting A fan draws air from the sample tray area and blows it through the channels of the heating cooling module The fan speed is determined according to the environmental conditions e g am...

Page 13: ...e opposite side of the Peltier element will become very hot and to maintain the performance of the elements they have to be cooled down This is done with large heat exchangers in the back of the ALS t...

Page 14: ...ing and receives the sensor signals from the temperature and fan sensors The TCA board controls the internal assemblies in the ALS thermostat This chapter describes the electronics of the TCA board Fi...

Page 15: ...ators The fans are equipped with hall sensors that allow to determination of the actual speed of the fans The speed of the four heat sink fans is variable and will be set according to the actual tempe...

Page 16: ...ctivities EPROM The EPROM stores all relevant data for the ALS Thermostat e g serial number board revision etc This data are pre set at the factory Figure 4 Block Diagram TCA Board Step Down Switcher...

Page 17: ...used to connect the thermostatted autosampler with a computer The address and control switch module next to the GPIB connector determines the GPIB address of your thermostatted autosampler The switche...

Page 18: ...ules The cable must be installed for operation of the ALS thermostat WARNING DO NOT disconnect or reconnect the autosampler to ALS thermostat cable when the power cords are connected to either of the...

Page 19: ...2 2 Installing the G1330B Thermostat Site requirements and installation of the G1330B thermostat...

Page 20: ...in the rear of the two thermostatted autosampler modules The autosampler module has no externally accessible fuses because automatic electronic fuses are implemented in its power supply The ALS thermo...

Page 21: ...ies system is to be installed on the bench make sure that the bench is designed to carry the weight of all the modules For a complete system including the thermostatted autosampler it is recommended t...

Page 22: ...mm 5 5 13 5 17 inches Line voltage 100 120 or 220 240 VAC 10 Automatic selection Line frequency 50 or 60 Hz 5 Power consumption Autosampler 300 VA ALS Thermostat 260 VA Maximum Maximum Ambient operati...

Page 23: ...arate boxes Upon receipt of your thermostatted autosampler inspect the shipping containers for any signs of damage If the containers or cushioning material are damaged save them until the contents hav...

Page 24: ...cal Agilent Technologies sales and service office If the thermostatted autosampler was ordered as an upgrade G1395A to an existing autosampler the shipment will also contain the required software upgr...

Page 25: ...can ensure optimum performance by installing the thermostatted autosampler in the stack in the position shown in Figure 6 and Figure 7 This configuration optimizes the system flow path ensuring minim...

Page 26: ...Optimizing the Stack Configuration Figure 7 Recommended Stack Configuration Rear View GPIB to LC ChemStation Analog signal to recorder AC power Remote cable CAN bus cable Autosampler Thermostat cable...

Page 27: ...e does not require updating The firmware update must be done with a PCMCIA card that has the newest revision loaded The firmware is not part of the shipment of the thermostatted autosampler Contact yo...

Page 28: ...emove a vial from the gripper when the gripper is positioned below the needle Figure 8 Safety Flap Stage 1 Preparing the ALS Thermostat and Autosampler 1 Place the ALS thermostat on the bench or in th...

Page 29: ...bing exit the module at the front or at the left side of the module Make sure that the leak tube is fully fixed on the outlet WARNING Make sure that the condensation tube is always above the liquid le...

Page 30: ...in the ALS thermostat locks 7 Place the air channel adapter into the autosampler tray base Make sure the adapter is fully pressed down This assures that the cold airstream from the ALS thermostat is...

Page 31: ...ween the autosampler and the ALS thermostat see Figure 5 WARNING Do not disconnect or reconnect the autosampler to ALS thermostat cable when the power cords are connected to either of the two modules...

Page 32: ...onnected to the CAN bus at any of the modules in the system The Agilent Chemstation can be connected to the system by one GPIB cable at any of the modules however it is recommended to connect the GPIB...

Page 33: ...observe appropriate safety procedures for example goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially wh...

Page 34: ...lling the Sample Tray 1 Load the sample tray with sample vials as required 2 Slide the sample tray into the thermostatted autosampler so that the rear of the sample tray is seated firmly against the r...

Page 35: ...ial tray is supported for temperature control of the vials Nevertheless the half trays of the standard autosampler G1313A can be used in the thermostatted autosampler as well However when these trays...

Page 36: ...0 Left hand 15 position tray 1 15 Right hand 40 position tray 101 140 Right hand 15 position tray 101 115 Figure 16 Numbering of Tray Positions Stage 5 Installing Tray Cover and Front Cover 1 Fix the...

Page 37: ...tted autosampler NOTE The power switch stays depressed 1 and a green indicator lamp in the power switch is on when the thermostatted autosampler is turned on When the line power switch stands out and...

Page 38: ...control module and remove the PC card by pressing the card eject button Stage 8 Update of the Agilent ChemStation Software If you have a Agilent ChemStation software version A 05 02 or higher you do...

Page 39: ...to update to A 04 02 insert the A 04 02 CD ROM and select SETUP on the CD ROM using File Manager or Explorer Select Yes to continue with the update 2 After you have updated your system insert the 3 5...

Page 40: ...under the side covers in a central position of the unit If the thermostatted autosampler needs to be shipped to another location via carrier ensure The two modules are shipped in separate boxes The t...

Page 41: ...3 3 Troubleshooting and Test Functions The thermostatted autosampler s built in troubleshooting and test functions...

Page 42: ...tus Indicators on page 43 Error Messages In the event of an electronic mechanical or hydraulic failure the thermostatted autosampler modules generate an error message in the user interface For each me...

Page 43: ...ors are located on the front of the autosampler The lower left indicates the power supply status the upper right indicates the thermostatted autosampler status Figure 18 Location of Status Indicators...

Page 44: ...roubleshooting and Test Functions Power Supply Indicator Power Supply Indicator The power supply indicator is integrated into the main power switch When the indicator is illuminated green the power is...

Page 45: ...indicates a not ready condition The instrument is in a not ready state when it is waiting for a specific condition to be reached or completed for example front cover not installed or while a self test...

Page 46: ...LS thermostat module which requires attention In the event of such a failure the red status indicator at the front of the thermostatted autosampler is switched on and an entry is written into the inst...

Page 47: ...ion numbers of the fans are as follows seen from front of the ALS thermostat fan failed 1 left side fan in front position fan failed 2 left side fan in back position fan failed 3 right side fan in bac...

Page 48: ...uild into the ALS thermostat for efficient cooling heating The electronics monitor the current through the Peltier elements If the Peltier current is out of a specified limit the Peltier element is de...

Page 49: ...e instrument The sensors are connected to both sides of the Peltier elements for control of the cooling heating efficiency As the positioning of the sensor is critical to meet the performance requirem...

Page 50: ...ection between autosampler and ALS thermostat Cable between autosampler and thermostat module not connected Defective electronic board in autosampler or ALS thermostat Suggested Actions Check cable co...

Page 51: ...by the autosampler electronics If this voltage is missing the error message will be generated Probable Causes ALS thermostat module not connected to line power ALS thermostat module fuse s defective...

Page 52: ...eat exchanger fans are not able to blow enough air through the ALS thermostat Ambient temperature too high low Suggested Actions Clean the air filters and heat exchanger fins in the ALS thermostat Swi...

Page 53: ...ve Peltier element s not connected or incorrectly connected e g after repair or maintenance The four main heat exchanger fans are not able to blow enough air through the ALS thermostat Suggested Actio...

Page 54: ...54 Troubleshooting and Test Functions Bad Cooling Heating Performance...

Page 55: ...4 4 Repairing the ALS Thermostat Module Instructions on repair procedures of the ALS thermostat...

Page 56: ...ed WARNING To prevent personal injury the power cable must be removed from the ALS thermostat before opening the Thermostat cover Do not connect the power cable to the ALS thermostat while the covers...

Page 57: ...Cleaning the Thermostat The thermostat covers should be kept clean Cleaning should be done with a soft cloth slightly dampened with water or a solution of water and a mild detergent Do not use an exc...

Page 58: ...lied in the autosampler accessory kit when handling electronic boards and components Using the ESD Strap 1 Unwrap the first two folds of the band and wrap the exposed adhesive side firmly around your...

Page 59: ...Thermostat Module Overview Overview Figure 19 shows the main assemblies and their locations which can be repaired Figure 19 Main assemblies Heat exchanger fan TCA Board Condensation leak drain Heat ex...

Page 60: ...les 3 Insert the flat head screwdriver in the fuse holder slightly press and turn counter clockwise to release the fuse holder from the socket 4 Pull the fuse holder out of the socket 5 Remove the fus...

Page 61: ...of the two modules This will damage the electronics of the modules Tools required Screwdriver Pozidriv 1 Preparations for this procedure Switch off ALS at the main power switch Disconnect ALS and ALS...

Page 62: ...the clips on both sides of the top cover 1 Remove the top cover 2 4 Unscrew the screws on the top plate and remove the plate by lifting its back first and then sliding to the front 5 Unplug all wires...

Page 63: ...emoving the Top Cover and Foam on page 61 item 1 to 4 Parts required Fan PN 3160 1079 1 Unplug the connector at the TCA board and remove the wire from the Top Foam 2 Carefully lift the Fan upwards 3 R...

Page 64: ...64 Repairing the ALS Thermostat Module Exchanging Heat Exchanger Fan 5 Reinstall the fan and route the wire in the appropriate guide channel 6 Reconnect the wire to the connector...

Page 65: ...ired Fan not running Preparations for this procedure Removing the Top Cover and Foam see Removing the Top Cover and Foam on page 61 Parts required Fan part number 3160 0884 1 Carefully lift the pair o...

Page 66: ...e Exchanging the Heatsink Fans 3 Reinsert the Top Foam and route the cables in the guide channels in the Top Foam 4 Reconnect the connectors in the correct order See label on top of Power Supply 5 Rep...

Page 67: ...ations for this procedure Removing the Top Cover and Foam see Removing the Top Cover and Foam on page 61 Parts required Sensor flexboard PN G1330 66504 Heatsink Compound PN 6040 0454 1 Unscrew the six...

Page 68: ...onnectors at the TCA Board careful lift the sensors out of their seat and remove the sensor flexboard 5 Insert some Heatsink Compound into the four sensor seats to assure good contact 6 Install the ne...

Page 69: ...insert the sealing adapter by carefully sliding it in to the seat 8 Reinstall the hardfoam encapsulation 9 Route the cables in the guide channels and reconnect the connectors in the correct order See...

Page 70: ...TCA Board defective Preparations for this procedure Removing the Top Cover and Foam see Removing the Top Cover and Foam on page 61 item 1 to 4 Parts required TCA board part number G1330 66500 1 Remove...

Page 71: ...nging the TCA board 3 By carefully pulling back on the upper part of the TCA board unsnatch it from the holder 4 Remove the TCA board 5 Reinsert the new TCA board 6 Gently push forward on the upper pa...

Page 72: ...72 Repairing the ALS Thermostat Module Exchanging the TCA board 7 Refit the connector screws and reconnect all connectors 8 Replace the top foam section metal cover and top cover...

Page 73: ...e position you may not be able to remove the side from the top part When required If cover is broken Tools required None Parts required Cover kit G1330 68703 includes base top left and right 1 Place t...

Page 74: ...74 Repairing the ALS Thermostat Module Assembling the Main Cover...

Page 75: ...5 5 ALS Thermostat Parts and Materials Lists for identification of parts and materials...

Page 76: ...blies Figure 20 Main Assemblies Table 4 Main Assemblies Item Description Part Number 1 Fuse Power Supply T2 5A 250V CSA UL listed 2110 0015 2 Fuse TCA Board T3A 250V CSA UL listed 2110 0029 3 Front Co...

Page 77: ...hermostat Parts and Materials Accessory Kit G1330 68705 Accessory Kit G1330 68705 Table 5 Accessory Kit Item Description Part Number 1 Waste Tube Reorder Number 5 m 5062 2463 2 Waste Tube Assembly G13...

Page 78: ...arts and Materials Main Assemblies Main Assemblies Figure 21 Main Assemblies Table 6 Main Assemblies Item Description Part Number 1 Heat sink fans 3160 0884 2 TCA Board G1330 66500 3 Heat exchanger fa...

Page 79: ...79 ALS Thermostat Parts and Materials Foam Parts Foam Parts Figure 22 Foam Parts Table 7 Main Assemblies Item Description Part Number 1 Top Foam G1330 40102 2 Bottom Foam G1330 40103 1 2...

Page 80: ...and Materials Plastic Parts Plastic Parts Figure 23 Plastic Parts Table 8 Main Assemblies Item Description Part Number 1 Cabinet Kit includes base top and sides G1330 68703 2 Front Cover 5062 8582 3 L...

Page 81: ...Parts and Materials Heat Exchanger Fan Parts Heat Exchanger Fan Parts Figure 24 Heat Exchanger Fan Parts Table 9 Main Assemblies Item Description Part Number 1 Fan Gasket G1330 44104 2 Heat Exchanger...

Page 82: ...82 ALS Thermostat Parts and Materials Heat Exchanger Fan Parts...

Page 83: ...6 6 Specifications Performance specifications of the ALS thermostat...

Page 84: ...s Performance Specifications Performance Specifications Table 10 Performance Specifications Agilent 1100 Series thermostatted autosampler Type Specification Temperature range setable from 4 C to 40 C...

Page 85: ...fan 65 67 exchanging 70 flow path 25 fuses 20 60 H half tray combinations 35 I injection valve 10 installing the thermostatted autosam pler 28 flow connections 33 peparation 28 power cable and interfa...

Page 86: ...86 Index...

Page 87: ...rranty services are provided at the initial installation point Installation and onsite warranty services are available only in Agilent service travel areas and only in the country of initial purchase...

Page 88: ...mer shall provide 1 access to the products during the specified periods of coverage to perform maintenance 2 adequate working space around the products for servicing by Agilent personnel 3 access to a...

Page 89: ...accordance with the law of your country Please consult your local Agilent office for the period of the warranty for shipping instructions and for the applicable wording of the local warranty Warranty...

Page 90: ...could result in serious personal injury Whenever it is likely that the protection has been impaired the instrument must be made inoperative and be secured against any intended operation Make sure tha...

Page 91: ...priate safety procedures e g goggles safety gloves and protective clothing as described in the material handling and safety data sheet by the solvent vendor especially when toxic or hazardous solvents...

Page 92: ...damage to the equipment Do not proceed beyond a warning until you have fully understood and met the indicated conditions CAUTION A caution alerts you to situations that could cause a possible loss of...

Page 93: ...nd measurement equipment is operated with equipment unscreened cables and or used for measurements on open set ups the user has to assure that under operating conditions the radio interference limits...

Page 94: ...94 Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at http www agilent com go chem...

Page 95: ......

Page 96: ...formation for the individual autosamplers can be obtained from the corresponding autosampler reference manual This supplemental manual describes the following installing the thermostat theory of opera...

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