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Agilent Technologies 3200D, Operating Manual

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Agilent Technologies 3200D Operating Manual Download Page 94

94

3200D 

溶解氧测定仪用户手册

2

 
 

其中显示屏上方显示有当前的测量模式、系统时间；溶解氧测量结
果以及对应的溶解氧电流值和当前温度值；下方为上次的标定结
果。

测量和显示方法会随不同的测量模式而略有不同。在测量过程中，
用户可以重新标定电极、设置测量参数等；测量结束后，用户可以
贮存、打印测量数据。按

“

取消

”

键结束测量。

饱和度的测量方法

类似于溶解氧的测量方法，首先选择合适的测量模式、饱和度测量
参数，具体设置参见

“

设置测量模式

”

章节。

开始测量后，仪器显示饱和度的值，其操作方法类似于溶解氧测量
方法，具体参见溶解氧测量方法。

温度的测量方法

在任意测量状态下，仪器将直接显示当前溶液的温度值。具体操作
参见溶解氧的测量章节。

图

14

Summary of Contents for 3200D

Page 1: ...Agilent Technologies Agilent 3200D Dissolved Oxygen Meter Operating Guide...

Page 2: ...d warranties of merchantability and fitness for a par ticular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connec tion with the furnishing use or per fo...

Page 3: ...adaptor 12 Installing the optional ground line 13 Installing Optional Software 14 2 Operation 15 Introduction 16 Where to find information 16 Term definitions 16 Proper use 17 Features 18 Specificati...

Page 4: ...asure temperature 42 To view other parameters while measuring 42 Managing Data 44 To save data 44 To delete data 44 To output data 44 To view data 45 Turn off the 3200D Dissolved Oxygen Meter 50 Softw...

Page 5: ...perating Guide 5 Check other possible causes 57 Meter Self Diagnostics and Messages 58 Severe errors 58 Error warning 59 Maintenance 61 Probe maintenance 61 Short term storage 61 Long term storage 61...

Page 6: ...6 3200D Dissolved Oxygen Meter Operating Guide Contents...

Page 7: ...ter Operating Guide 1 Installation Tools and Components for Installation 8 Installing the 3200D Dissolved Oxygen Meter 9 Installing Optional Software 14 The tools and accessories necessary for install...

Page 8: ...Installation Tools and Components for Installation Agilent provides the tools needed for installation The following accessories are included in the shipping case Multifunction electrode holder G4389A...

Page 9: ...s Installing the electrode holder 1 Place the electrode holder near the meter and move the arm into position Use the thumbscrews shown in Figure 1 to secure the arm in place 2 Clip the DO dissolved ox...

Page 10: ...10 3200D Dissolved Oxygen Meter Operating Guide 1 Installation 3 Route the probe cable as shown Figure 2 Figure 2 Installed meter and probes Probes Meter Probe socket...

Page 11: ...4 Locate the DO Temp probe socket on the back of the meter Plug the DO probe connector 5190 3997 into the DO Temp socket on the rear of the meter See Figure 3 Figure 3 The back view of the 3200D Disso...

Page 12: ...back panel of the meter Insert the probe connector into the socket 2 Feed the probe cable through the hole of the multifunction electrode holder Installing the power adaptor The universal power adapt...

Page 13: ...the power adapter to the power input on the meter A click will be heard when the plug is properly engaged Installing the optional ground line The meter ships with an optional ground line During use i...

Page 14: ...nect the computer to the meter with a USB cable See the G4390A software documentation for more information If not using the G4390A software Agilent provides downloadable data printing software on the...

Page 15: ...ent Control 23 Turn on the Meter 25 Setup 26 Prepare the DO Probe 37 Calibrate the DO Probe 39 Perform a Measurement 41 Managing Data 44 Turn off the 3200D Dissolved Oxygen Meter 50 Software Operation...

Page 16: ...izable services as well as information related directly to your Agilent products and orders Log onto the portal at http www agilent com chem Term definitions Dissolved oxygen concentration The extent...

Page 17: ...ot soak the DO probe in sodium sulfite solution If a probe is out of use for more than 6 hours rinse and store it in a protective container CAUTION Do not expose to corrosive gas Keep the sockets on t...

Page 18: ...Zero Point and Full Scale A clear dot matrix LCD display Supports GLP standards Requires an operator number Records views and prints calibration data Stores 200 sets of measuring data Can view print a...

Page 19: ...acy of electric unit DO concentration 0 10 mg L DO saturation 2 0 Temperature 0 1 C Normal working conditions Environmental temperature 0 40 C Relative humidity 85 Power supply Power adaptor 5185 8389...

Page 20: ...a meter and a probe system The probe system is held in place by the electrode holder See Figure 6 Figure 7 and Figure 8 Figure 6 The meter electrode holder and probe Figure 7 The front view of the 32...

Page 21: ...1 The Display The display shows the working condition and current setting of the 3200D Dissolved Oxygen Meter Figure 8 The back view of the Agilent 3200D Dissolved Oxygen Meter Figure 9 The initial st...

Page 22: ...erating keys The keys are shown in Figure 10 and described in Table 1 on page 23 Most keys have two values a numeric entry and a function Which one applies depends on the display if it is waiting for...

Page 23: ...election cursor upward when selecting Type the number 3 Store measurement data Type the number 4 Move the selection cursor left when selecting Type the number 5 Opens the Setup menu from the initial s...

Page 24: ...Operating Guide 2 Operation Type the number 0 Begin measurement Type a decimal point Calibrate the DO probe Type a negative number Delete the data being viewed Meter power switch Table 1 Keypad functi...

Page 25: ...on the display shows the Agilent name the meter model and other information 2 After the system self check the meter goes to the initial state shown in Figure 11 The left of the screen shows the curren...

Page 26: ...reen appears See Figure 12 Measuring Mode Sets up current measuring mode Continuous Mode Timed Reading Mode Auto Lock Reading Mode and measuring parameter Set Condition Use this mode to set condition...

Page 27: ...ys to highlight the desired parameter and press Setup to select it A check appears next to the selected parameter During measurement you can still view save and print the other parameter See To view o...

Page 28: ...save or print results at any time during measurement To end a measurement run press Cancel followed by Enter Timed Reading The meter will automatically save measurement data periodically while measur...

Page 29: ...ge 30 When the measurement begins the meter automatically measures calculates and displays the results Once the measurements meet the preset Auto Lock condition the measurement finishes and the screen...

Page 30: ...screen locks displaying the final reading To set the conditions 1 From the initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow keys to navigate to S...

Page 31: ...initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow keys to navigate to System Setup 3 Press Enter to select System Setup or press Cancel to exit T...

Page 32: ...een 7 Once all of the system settings are made press Enter to save the new setup exit and return to the initial state Press Cancel to exit without saving changes Descriptions of the System Setup setti...

Page 33: ...If Auto Delete is not enabled the meter does not save new data when its memory is full For example the meter permits up to 200 sets of data When you want to store the 201st set of data if Auto Delete...

Page 34: ...screen appears on the display Use the arrow keys to choose either Chinese or English and press Enter To set the air pressure barometric pressure You do not usually need to set barometric pressure The...

Page 35: ...er can power off automatically after a set time period To set the Auto Power Off time 1 From the initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow...

Page 36: ...e display Press Enter to restore parameters to their original settings Table 2 Default values for meter parameters Parameter Default value DO calibration data Zero Oxygen 0 nA Full Scale 1000 nA Calib...

Page 37: ...atinum tip 7 Polarize the DO probe before use Connect the DO probe with a powered on 3200D DO meter Polarization takes 60 minutes The DO probe is always being polarized when connected with the meter s...

Page 38: ...ng upon application conditions Refill the DO filling solution every 2 weeks to 2 months CAUTION There should not be any damage to the membrane Avoid touching the membrane to any solid or hard material...

Page 39: ...lution or as described in the instruction manual for the DO probe 2 From the initial state or while measuring press Calibrate 3 Select Calib Zero Press Enter to select Zero Point Calibration as shown...

Page 40: ...From the initial state or while measuring press Calibrate 6 Select Full Scale Press Enter to open Full Scale Calibration as shown in Figure 22 During calibration press Setup to set calibration paramet...

Page 41: ...e Measuring Mode on page 26 4 Put the probe in the sample solution and press Measure to start taking a measurement according to the selected mode See Figure 23 The upper area of the screen shows the c...

Page 42: ...according to the selected mode 5 After a measurement press Save to save data Press Output to print data Press Cancel to end measurement To measure temperature In any measuring state the meter directly...

Page 43: ...Oxygen Meter Operating Guide 43 2 Press 4 or 6 to switch the view to the other parameter 3 If you do not press a key for a few seconds the meter will automatically exit from viewing mode and return to...

Page 44: ...me stable In timed reading mode you can still save data manually but the meter automatically saves measuring data at a fixed periodic time interval See Measuring Mode on page 26 To delete data You can...

Page 45: ...d data meets GLP standards The meter can store 200 sets of measurement data 1 In the initial state press View 2 Navigate to the type of data to view and press Enter See Figure 25 To View DO Data The m...

Page 46: ...lay format depends on the viewing mode 2 The data displayed include save time and operator no Press the arrow keys to scroll through the saved data 3 Press Delete to delete data 4 To output stored dat...

Page 47: ...10 06 20 OPERATOR NO 000 STORED NUM 002 NO 001 OPERATOR NO 000 STORED TIME 10 43 00 2010 06 20 PRESSURE 101 3kPa SALINITY 0 0g L ZERO 0nA FULL 1000nA CURRENT 0nA DO 0 00mg L SATURATION 0 0 TEMP 25 0c...

Page 48: ...ss Enter The display is shown in Figure 28 The upper area displays last calibration data The bottom area displays current calibrated parameters 2 To print current data connect the meter with the PC Pr...

Page 49: ...e 49 Figure 29 Output format MODEL 3200D DISSOLVED OXYGEN METER SOFTWARE VER 1 00 PRINT TIME 09 14 03 2010 06 20 OPERATOR NO 000 DO CALIB DATA CALIB TIME 08 12 00 2008 01 09 OPERATOR NO 000 PRESSURE 1...

Page 50: ...line and salt solution The input terminal of the meter connector of the DO ATC probe must be kept clean and dry If the DO probe is used in a strongly humid place wipe the DO probe plug with clean gauz...

Page 51: ...the software will recognize the meter model and type The software provides the functions corresponding to the meter type Refer to the software documentation for details To use the Data Printing softw...

Page 52: ...52 3200D Dissolved Oxygen Meter Operating Guide 2 Operation...

Page 53: ...Maintenance Troubleshooting the 3200D Dissolved Oxygen Meter 54 General Troubleshooting Procedure 56 Meter Self Diagnostics and Messages 58 Maintenance 61 Consumables and Ordering Information 62 This...

Page 54: ...meet with the requirements 3 The power adaptor is damaged 4 The power socket has poor contact 5 The LCD is damaged After start up for a few minutes the user can hear a buzzing sound after pressing On...

Page 55: ...king strong electromagnetic field an so forth 1 Replace the probe 2 Remove the electrical signal interference source Lift or move the beaker away from the source of interference Shield the meter and b...

Page 56: ...ions For best results follow the troubleshooting order shown below Check the current response 1 Connect the meter to the ATC temperature diagnostic tool 5185 8390 shipped with the meter 2 Turn on the...

Page 57: ...meter displays a temperature reading significantly different from 50 C there is a problem with the meter Contact Agilent service Check other possible causes If the meter is functioning properly that i...

Page 58: ...er unable to finish necessary tasks In this case replacement or maintenance of the meter is required Minor errors which are prompts or warnings are caused by various reasons and can be corrected in se...

Page 59: ...Error warning NOTE This table describes all error messages which may occur in use These error messages have different definition for different meters Table 4 Error warning codes Code Description Solu...

Page 60: ...buffers 28 Temperature of pH buffer is out of range Cool or heat buffer 29 Calibrate the same buffer repeatedly Replace the buffer Due to incorrect operation 30 Number of pH buffers exceeds maximum R...

Page 61: ...parts of the stem with distilled or deionized water and dry with a soft tissue Short term storage Between tests immerse the measuring tip in distilled water or calibration solution while the probe is...

Page 62: ...n with stable and precise speed with a large adjustable range G4389A 3200EA Electrode Holder It is used to support several electrodes 5185 8389 AC Adaptor 100 240VAC 1A 50 60Hz G4388 27000 Stirring Ba...

Page 63: ...Agilent Technologies Agilent 3200D...

Page 64: ...3200D Agilent Technologies Inc 2012 Agilent Technologies Inc 5973 1779 2012 3 412 800 820 3278 Agilent Agilent Agilent...

Page 65: ...3200D 65 3200D 67 68 3200D 69 69 70 71 71 72 73 3200D 75 76 76 Agilent 76 76 3200D 77 3200D 78 79 81 81 81 83 83 83 91 95 3200D 99 100...

Page 66: ...66 3200D 101 101 101 101 101 3200D 103 104 105 105 105 105 106 106 107 109 110 111 111 111 3200D 113...

Page 67: ...67 Agilent Technologies Agilent 3200D 1 3200D 68 3200D 69 72 73...

Page 68: ...68 3200D 1 Agilent G4389A D6111 DO Probe 5190 3997 5185 8389...

Page 69: ...1 3200D 69 3200D 3200D 1 2 3 4 5 6 7 8...

Page 70: ...70 3200D 1 5190 3997...

Page 71: ...1 3200D 71 100 240 VAC 1 A 50 60 Hz DC501...

Page 72: ...72 3200D 1 G4390A USB...

Page 73: ...1 3200D 73 3200D...

Page 74: ...74 3200D 1...

Page 75: ...75 Agilent Technologies Agilent 3200D 2 3200D 76 83 101 3200D...

Page 76: ...76 3200D 2 Agilent 3200D 3200D 60 Agilent Agilent Web Agilent http www agilent com chem DO kPa g L...

Page 77: ...2 3200D 77 5 3200D 3200D GLP GLP 200 USB PC PC bug...

Page 78: ...78 3200D 2 3200D 3200D 0 00 45 00 mg L 0 0 300 0 5 0 110 0 C 0 01 mg L 0 1 0 1 C 0 10 mg L 2 0 0 1 C 0 40 C 85 5185 8389 100 240 VAC 1 A 9 VDC 1 A mm 190 190 105 kg 1 kg...

Page 79: ...2 3200D 79 3 3200D 3200D...

Page 80: ...80 3200D 2 3200D 1 2 3200D 1 2 3 USB 4...

Page 81: ...2 3200D 81 3200D On Off 3200D 15 1 2 3 4 5 6 7 8 9 0 1 1 2 4 8 6 2 4 8 6 3 3 5 5 7 7...

Page 82: ...82 3200D 2 9 9 0 0...

Page 83: ...2 3200D 83 3200D 3200D 3200D 3200D 3200D 3200D 3200D On Off...

Page 84: ...84 3200D 2 1 2 GLP 1 2...

Page 85: ...2 3200D 85 3 4 3 4...

Page 86: ...86 3200D 2 5 4 6 4 6 30 USB PC 1 99 10 5...

Page 87: ...2 3200D 87 6 1 0 1 0 s 1 200 GLP 7 h 6...

Page 88: ...88 3200D 2 000 200 7 200 201 201...

Page 89: ...2 3200D 89 8 9 101 3kPa 8 9...

Page 90: ...90 3200D 2 10 0 0g L 10 480min 0 nA 1000 nA 25 0 C 101 3 kPa 0 0 g L 10 min 000 1 0 10...

Page 91: ...2 3200D 91 5 s 0 1 2 3 5190 0547 4 5 60 1 1 25 20 80 cm 2 2...

Page 92: ...92 3200D 2 11 5 12 11 12...

Page 93: ...2 3200D 93 13 14 13...

Page 94: ...94 3200D 2 14...

Page 95: ...2 3200D 95 200 200 USB PC PC...

Page 96: ...96 3200D 2 3200D 15 GLP 200 16 10 USB PC MODEL 3200D DISSOLVED OXYGEN DETERMINATOR VER 1 00 PRINT TIME 09 03 28 15...

Page 97: ...00 STORED NUM 003 NO 001 OPERATOR NO 000 STORED TIME 10 43 00 2010 06 20 PRESSURE 101 3kPa SALINITY 0 0g L ZERO OXYGEN 0nA FULL OXYGEN 1000nA CURRENT 0nA DO 0 00mg L SATURATION 0 0 TEMP 25 0c NO 002 O...

Page 98: ...98 3200D 2 17 USB PC MODEL 3200D DISSOLVED OXYGEN DETERMINATOR VER 1 00 PRINT TIME 16 17...

Page 99: ...00D 99 09 14 03 2010 06 20 OPERATOR NO 000 DO CALIB DATA CALIB TIME 08 12 00 2008 01 09 OPERATOR NO 000 PRESSURE 101 3kPa SALINITY 0 0g L ZERO OXYGEN 0nA FULL OXYGEN 1000nA TEMP 25 0c 3200D On Off 1 2...

Page 100: ...100 3200D 2 5 6 7 60...

Page 101: ...2 3200D 101 3200D 3200D G4390A PC DVD 1 On Off 2 USB PC 3 PC 1 On Off 2 PC 3 PC...

Page 102: ...102 3200D 2...

Page 103: ...103 Agilent Technologies Agilent 3200D 3 3200D 104 105 106...

Page 104: ...104 3200D 3 1 1 2 3 4 5 1 2 3 4 5 2 1 2 1 2 3 1 2 1 2 4 1 2 1 2...

Page 105: ...3 3200D 105 ATC 5185 8390 680 720nA 0 5nA 300 1000nA ATC 5185 8390 49 0 51 0...

Page 106: ...106 3200D 3 18...

Page 107: ...3 3200D 107 19...

Page 108: ...01 3 02 4 03 5 6 7 20 1999 9 1999 9 mV 8 21 pH pX 3 000 21 000 pH 9 22 0 2000 mS cm 10 23 0 100 Mohm cm 11 24 6 0 120 0 C 12 25 0 4000 nA 13 26 pH 80 120 14 27 pH 15 28 pH 16 29 17 30 pH 5 18 31 pH 1...

Page 109: ...109 Agilent Technologies Agilent 3200D 4 110 111...

Page 110: ...110 3200D 4 1 2 3 4 5 6 60 1 1 25...

Page 111: ...4 3200D 111...

Page 112: ...112 3200D 4...

Page 113: ...113 Agilent Technologies Agilent 3200D 5 3200D 3200D...

Page 114: ...3200D 5 Agilent http www agilent com chem G4388A 3200SA G4389A 3200EA G4390A 5185 8389 100 240 VAC 1 A 50 60 Hz G4388 27000 5190 3997 D6111 3 0 20 mg L 0 45 C 5185 8390 ATC 5190 0547 3 30 mL 5190 054...

Page 115: ......

Page 116: ...Agilent Technologies Inc 2012 Printed in China 03 12 First edition March 2012 5973 1780 5973 1779 www agilent com Agilent Technologies...

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