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Method parameters of the KF-Titration ................................................................................. 231

4.7
4.7.1

Standard methods of KF ....................................................................................................... 231

4.7.2

KF Titration parameters......................................................................................................... 234

Measuring method ................................................................................................................. 239

4.8

Dosing and titration with externally connected piston burettes and titrators 244

Requirements ........................................................................................................................ 244

5.1

Dose with external piston burettes/titrators ........................................................................... 244

5.2
5.2.1

Titration with external piston burettes/titrators ...................................................................... 250

System settings ................................................................................................... 253

Calibration settings ................................................................................................................ 253

6.1

Interchangeable Unit - Reagents .......................................................................................... 255

6.2

Electrode menu ..................................................................................................................... 257

6.3

RS232 Settings ..................................................................................................................... 259

6.4

Date and Time ....................................................................................................................... 261

6.5

Password ............................................................................................................................... 262

6.6
6.6.1

Creation of the first Administrator .......................................................................................... 262

6.6.2

Creation of additional users .................................................................................................. 266

6.6.3

Predefined rights and definable rights................................................................................... 267

6.6.4

Delete of users ...................................................................................................................... 271

RESET .................................................................................................................................. 272

6.7

Printer .................................................................................................................................... 273

6.8

Device Information ................................................................................................................ 273

6.9

System Tones ....................................................................................................................... 273

6.10

Software Update .................................................................................................................... 274

6.11

Network settings .................................................................................................. 278

General .................................................................................................................................. 278

7.1

Setup a shared directory ....................................................................................................... 279

7.2

Communication via RS-232 and USB-B interface ............................................. 281

General Information............................................................................................................... 281

8.1

Chaining multiple devices -

“Daisy Chain Concept” .............................................................. 281

8.2

Instruction Set for RS-Communication .................................................................................. 281

8.3

Connection of Analytical Balances and Printers .............................................. 283

Connection of Analytical Balances ........................................................................................ 283

9.1

Balance data editor ............................................................................................................... 284

9.2

Printers .................................................................................................................................. 285

9.3

Automatic stirrer control ........................................................................................................ 286

9.4
9.4.1

General .................................................................................................................................. 286

9.4.2

Basic setting in the system menu .......................................................................................... 286

9.4.3

Set the stirring speed in the method ..................................................................................... 287

Autosampler .......................................................................................................................... 288

9.5
9.5.1

Connection of sampler changer TW alpha plus .................................................................... 288

9.5.2

Connection of sample changer TW 7400 .............................................................................. 288

Using software TitriSoft ......................................................................................................... 288

9.6
9.6.1

General .................................................................................................................................. 288

9.6.2

TitriSoft 3.15 or higher ........................................................................................................... 288

Maintenance and Care of the Titrator ................................................................ 289

Guarantee ............................................................................................................. 290

Storage and transportation ................................................................................. 290

Recycling and Disposal ...................................................................................... 290

Copyright

Xylem Analytics Germany GmbH

Reprinting - even as excerpts - is only allowed with the explicit written authorization.

Germany. Printed in Germany.

Содержание TitroLine 7800

Страница 1: ......

Страница 2: ...portantes Le mode d emploi fait partie du produit Pri re de lire et d observer attentivement le mode d emploi avant la premi re mise en marche de produit et de le conserver Pour des raisons de s curit...

Страница 3: ...olvent 169 2 9 Replacing the Glass Cylinder and the PTFE Piston 169 2 10 Combination with Accessories and Additional Devices 171 2 11 2 11 1 Connecting a printer 171 2 11 2 Connecting a USB device 171...

Страница 4: ...General 278 7 1 Setup a shared directory 279 7 2 8 Communication via RS 232 and USB B interface 281 General Information 281 8 1 Chaining multiple devices Daisy Chain Concept 281 8 2 Instruction Set f...

Страница 5: ...H Stat titrations Non aqueous potentiometric titrations such as TAN and TBN Pre dosing with a connected piston burette Connection and use of an autosampler TW alpha plus TW 7400 KF titrations with 1 c...

Страница 6: ...ne 7800 to warm up Measuring input 1 analog pH mV input with 24 bit transducer for high precision readings Electrode socket according to DIN 19 262 or additional with BNC socket insert Z 860 Reference...

Страница 7: ...Pt 1000 Connection sockets 2 x 4 mm Measurement input 2 Digital input for connector for IDS sensors pH mV LF Power supply power supply 90 240 V 50 60 Hz power input 30 VA Use the power supply TZ 1853...

Страница 8: ...Recognition of unit size and characteristics of the Titration or dosing solution Valve volume neutral cone valve made from fluorocarbon polymers PTFE TZ 3000 Cylinder borosilicate glass 3 3 DURAN Hose...

Страница 9: ...e liquid medium approx 0 8 l min Stirring speed 50 1000 U min Hoses PVC hose outer diameter 6 x 1 mm PTFE hose outer diameter 4 x 0 5 mm Connections Power supply Low voltage input 12 V on the backside...

Страница 10: ...m the place of work Examples for the assumption that a safe operation is no longer possible if the package is damaged if the device shows visible damages if the power supply shows visible damages if t...

Страница 11: ...ckaging The device may be placed on any flat surface Scope of delivery a Titrator TitroLine 7800 basic unit TitroLine 7800 Keyboard TZ 3835 Power supply TZ 1853 100V 240V incl some primary adapter Man...

Страница 12: ...S232 ports 4 channel Mini DIN RS1 for connection to the PC RS2 for connection of a weighing balance and other devices from SI Analytics 7 Measurement input 2 for intelligent digital sensors IDS 8 Ethe...

Страница 13: ...ied USB cable 2 Then screw the tube into the thread and mount the Z 305 titration clamp Installation of the Z 300 Rod Foot Plate Optional 2 4 If the TM 235 TM 235 KF magnetic stirrer is not in use it...

Страница 14: ...ears Fig 6 Fig 6 Using SYS or MODE you navigate to the system settings System settings The very first menu is to be used for setting the language Fig 7 Fig 7 Use ENTER OK to call the menu Select the l...

Страница 15: ...ted at the stand rod Please take care that the metal clamp is adjusted as shown in the attached Fig 9 Fig 9 Put all three white inner plastic adapters at the waste solvent and moisture bottle Fill the...

Страница 16: ...the TM 235 KF The waste clear bottle is connected to the left connector Fig 11 The PTFE tube from the clear waste bottle is adjusted to the ground tube 1 of the titration vessel The PTFE tube from the...

Страница 17: ...he plastic moisture tube Place it to the other NS 14 opening as shown in Fig 14 Fig 14 The electrode KF 1100 is placed into the NS 7 5 opening and connected to the A input of the TitroLine 7800 The ke...

Страница 18: ...of the Interchangeable Unit Fig 15 shows a completely assembled interchangeable unit 1 Remove the valve with the attached hoses from the pack and then push it on the valve support until it snaps in p...

Страница 19: ...1 000000 Concentration determined on Date To be used until Date Opened Produced on Date Test according to ISO 8655 Date Charge description default no charge Last modification Date Each time an interc...

Страница 20: ...e unit forward Fig 18 and Fig 17 2 7 3 Programming of the titration unit The data from the RFID transponder of the interchangeable unit will be read immediately Fig 19 Fig 19 The input menu for the re...

Страница 21: ...rant e g 5 or 2 should be entered under Concentration Thereby the drift in g min can be calculated in the right dimensions Fig 22 You will be prompted for a confirmation of the values Fig 23 Fig 23 If...

Страница 22: ...el under the titration tip Initial filling of the interchangeable unit is done using the rinsing program Fig 25 On the main menu Fig 25 press MODE to navigate to the methods system Fig 26 Fig 26 Press...

Страница 23: ...167 Initial filling requires a minimum of two rinsing cycles Fig 28 You can stop the rinsing operation Fig 29 at any time by pressing STOP and then resume rinsing with START Fig 29...

Страница 24: ...ly 1 Cut of hose end evenly 2 Slip parts of the threaded clamping joint on to the hose 3 Guide hose through shaft 4 Press the free hose end over the ring marking until it reaches the stop of the tip 5...

Страница 25: ...dditional tools In certain cases the piston extractor has to be used 1 Remove the interchangeable unit from the base unit 2 Unscrew the hose between the glass cylinder and the valve from the glass cyl...

Страница 26: ...e interchangeable unit will no longer match the cylinder size This will trigger incorrect dosage For the sake of dosing and analytical accuracy it is also recommended to replace the PTFE piston each t...

Страница 27: ...necting the electrode to the mV pH socket The bead should possibly point upward to the reference socket or in between also refer to Fig 1 The identification of the ID electrode is thereby simplified D...

Страница 28: ...onds Fig 36 Fig 36 The display then switches to the normal display showing in this case Fig 37 the conductivity in s cm and the temperature Fig 37 Are for example two measurement parameters are select...

Страница 29: ...current method new method copy and delete method ESC ESC will take you back to the previous menu level START Start and Stop of a current method FILL Filling the unit The individual functions are desc...

Страница 30: ...nge of the current method new method copy method F4 FILL Fill the interchangeable unit F5 Display and modification of the balance data With Shift F5 display and modification of the global memories F6...

Страница 31: ...enu to appear The method displayed will always be the last method that was used Fig 42 Fig 42 Pressing START will result in the immediate execution of the method shown EDIT will take you to the method...

Страница 32: ...n with ENTER OK Once the selection made you will return to the main menu with the newly selected method If no method is selected ESC will also take you back to the main menu To navigate directly to th...

Страница 33: ...displayed can now be carried out immediately with START Depending on the method settings you will be prompted for the sample identification Fig 48 and the weighed in quantity Fig 49 You can use an ex...

Страница 34: ...r of the balance data without any further confirmation being necessary The display Fig 51 will show the measured value pH mV or A and the current consumption The measured value is displayed in a sligh...

Страница 35: ...curve itself Fig 54 If a printer is connected the results will either be printed according to the settings made for the method or else they will be memorised in the form of a PDF and CSV file file on...

Страница 36: ...uccessively into 2 or 3 buffers Fig 56 Fig 56 The 1 st buffer is started with START The 2 nd and 3 rd buffers optional are to be started with ENTER OK During calibration Fig 57 Fig 59 you can view the...

Страница 37: ...he electrode Fig 60 Fig 60 The calibration values will be automatically printed or stored as a PDF file ESC will take you back to the main menu The current calibration values can be viewed at any time...

Страница 38: ...for pH measurement Fig 63 has yet to select after calling the calibration routine if a pH electrode to the measuring input A analog or a digital IDS to calibrate electrode Fig 64 Fig 63 Fig 64 The seq...

Страница 39: ...Titration the display changes Fig 66 Fig 66 You can control the metering rate with the black key of the manual controller Fig 66 a A single depression of the key will cause a step up to the first leve...

Страница 40: ...min Stage 3 12 5 ca 5 ml min Stage 2 6 8 ca 2 5 ml min Stage 1 3 4 ca 1 25 ml min Even if the titration is completed press STOP or approx for 1 sec the grey key of the manual controller The titration...

Страница 41: ...ation of the result The conditioning is run automatically after pressing START Fig 69 The final conditions are the same as the conditions of the actual sample titration Fig 69 When the final criteria...

Страница 42: ...e an external PC keyboard for entering a 20 digit alphanumeric sample ID Fig 72 Fig 73 The balance data can be entered using the front keyboard or an external keyboard The input is to be confirmed wit...

Страница 43: ...of the balance data without any further confirmation being necessary The display shows either the use in ml with the drift in g min Fig 75 or the drift with the measured value in A Fig 76 or the titra...

Страница 44: ...sults Fig 79 Fig 79 If a printer is connected the results will either be printed according to the settings made for the method or else they will be memorised in the form of a PDF and CSV file file on...

Страница 45: ...with dosing method Use START or the black key of the manual controller to start a dosage method Fig 80 and Fig 81 Fig 80 Fig 81 The dosed volume will be briefly displayed Fig 82 before the display ret...

Страница 46: ...5 2 Dosing operation without dosing method A dosing operation can also be performed without any dosing method with DOS F10 of the external keyboard Fig 84 Fig 84 The volume will be dosed with ENTER O...

Страница 47: ...rocess a solvent is dosed to a sample weight of a substance until the desired target concentration is reached Fig 87 and Fig 89 Fig 87 Fig 88 Fig 89 If the calculated volume is greater than the maximu...

Страница 48: ...mpt for the input of a method name Fig 92 This prompt will not appear in the case of the modification of an already created method Fig 92 The method name can contain up to 21 characters Special charac...

Страница 49: ...ll be taken to Change method parameters Please continue at this point with 4 6 Change Method Parameters Copy Method 4 3 Methods can be copied or stored with a new name Fig 95 If you select this functi...

Страница 50: ...he current method is actually to be deleted Fig 96 You have to reply Yes in explicit terms and also confirm this reply with ENTER OK Fig 96 Print method 4 5 The currently selected method can be printe...

Страница 51: ...99 The selection of the Method type will have an influence on the further parameterisation of the method For instance if you select the dosing mode neither a selection of a formula nor a change of the...

Страница 52: ...of dynamic titration the titration steps are adapted to the change of the measurement readings ml slope curve gradient Small slope values mean a large step sizes and large slope values indicate small...

Страница 53: ...g speed Subsequently the method will change to a linear step size of 0 02 ml until the end point of pH 4 50 is either reached or fallen short of Should this value raise again to above pH 4 50 within 5...

Страница 54: ...on the pH time Fig 103 or the ml time Fig 104 curve and the pH value ml can be displayed analog Fig 103 Fig 104 4 6 3 Result At first the calculation options dynamic and linear titration only are spec...

Страница 55: ...the calculated equivalence points of the titration curve will be used Formula Fig 105 offers the following settings Fig 107 Fig 107 The Result text may contain up to 21 alphanumeric characters includi...

Страница 56: ...formula is selected on the Formula selection submenu Fig 109 Fig 109 If two inflection points 2 EQs are selected formula 1 formula 2 and 3 can be selected Fig 110 Fig 110 The calculation formula for t...

Страница 57: ...lating the concentration of a sample taking into account a blank value in ml Back titration NCO value Epoxy number EQ1 EP1 Calculation of the consumption in the equivalence or end point EP2 T M F1 W F...

Страница 58: ...of a sample taking into account a blank value in ml Direct titration to EQ2 W F2 B EQ2 M T F1 Formula for calculating the concentration of a sample taking into account a blank value in ml Back titrat...

Страница 59: ...value the titers and factors F1 F5 can be entered or read from a global memory Fig 112 Fig 112 The values from the global memory were defined in advance by a titration or were manually entered Fig 113...

Страница 60: ...individual parameters of the selected calculation formula e g mol Fig 116 can now be input one by one Fig 116 4 6 3 2 Sample weight and volume sample quantity The Sample Quantity W item Fig 117 is us...

Страница 61: ...used for each start of the method Manual sample volume The sample volume in ml is prompted at the start of the method and manually input Fixed sample volume A fixed sample volume is input in ml This...

Страница 62: ...g l 10 mg l und ppm 10000 g 100 ml 1 1 Fd Target concentration of the solution to be prepared in g l mg l ppm g 100 ml or Fe Specific weight of the weighed in sample in g cm Ff Volume correction in m...

Страница 63: ...Statistics The mean value and relative standard deviation can be automatically calculated and documented by using the statistics Fig 123 Fig 123 The calculation of the mean value is already possible f...

Страница 64: ...126 Fig 126 The mean value is written into the global memory when the statistic is switched on You enter the submenu with ENTER OK If a global memory has not been created a memory can be created by us...

Страница 65: ...n always be accessed by pressing Shift or via system settings The name or values can be changed by using EDIT and have the methods shown that are used in the global memories Fig 129 Fig 129 4 6 4 Form...

Страница 66: ...210 Confirm the selection Result with ENTER OK Fig 131 Fig 131 Select Formula with ENTER OK Fig 132 Fig 132 The following selection appears Fig 133 Fig 133...

Страница 67: ...d confirm it with ENTER OK the currently selected formula is displayed Fig 141 Fig 135 The formula EQ1 B T M F1 W F2 can now be changed and confirmed with ENTER OK after the change If you leave the ed...

Страница 68: ...e g directly enter a numeric value Fig 139 Fig 139 The decimal point of the numeric value can be entered as a point or a comma Press ENTER OK to leave the editor The formula is automatically saved Und...

Страница 69: ...fixed manual global memory or results of other formulas T Titer of the titration burettes W Weight sample B Blanc value D Density S Slope in ml s of a pH stat application EV End or total volume of a t...

Страница 70: ...ed by the formula editor It is checked whether the number of opening brackets is equal to that of the closing ones whether the entered variables and calculation operations are allowed If an error occu...

Страница 71: ...End Point titration Dead Stop titration and pH Stat titration it is possible to enter a variety of parameters The following parameters are valid for all automatic titration modes Measured value pH mV...

Страница 72: ...asured value in terms of mV min is set by selecting normal fast or user defined Fig 148 The drift values at predefined in terms of in mV min for normal and fast drift Normal Drift 20 mV min Fast Drift...

Страница 73: ...easured value is used in most applications However there are applications in which the setting of a fixed holding time for measured value acceptance following the titration step is recommendable Examp...

Страница 74: ...l If dynamic control was selected one has a selection of 3 different stages steep average and flat or user defined dynamic parameters Fig 152 Fig 152 On the stages both the dynamic parameters and the...

Страница 75: ...54 Fig 154 A minimum waiting period should therefore also be observed for the various attenuation settings Attenuation setting Minimum waiting period Application None 1 second All aqueous titration ap...

Страница 76: ...an also be set for End Point titration pH mV and dead stop In this type of titration linear step width is used after the first continuous titration stage 4 6 5 5 Titration direction The titration dire...

Страница 77: ...Fig 158 4 6 5 7 Titration end The end of a titration Fig 159 is reached and the result will be calculated as soon as if the defined End value pH mV A value has been reached the criteria steep flat slo...

Страница 78: ...e respectively Nevertheless it is possible to calculate the EQ subsequently on the basis of the recorded measurement data If EQ detection is activated you can define the slope value for the EQ Fig 162...

Страница 79: ...fic Delta value Delta endpoint at a distance from the set end value is reached The dosing speed of this first stage can be set in terms of on the Dosing parameters menu Subsequently titration continue...

Страница 80: ...ge insensitive High polarisation voltage sensitive 4 6 7 Titration parameter pH Stat Titration Explanatory Notes for the pH Stat titration see also 4 6 2 4 The titration parameters for the first Level...

Страница 81: ...s Fig 170 Fig 170 With a measuring interval of 60 seconds that would be a total of 120 readings Up to 1000 measuring points can be recorded for a pH Stat titration Fig 171 Fig 171 Even if the measurin...

Страница 82: ...in ml s Fig 172 Fig 172 The evaluation window Fig 176 can be used to calculate the slope by entering the start time and duration Time period Fig 173 and Fig 174 Fig 173 Fig 174 The start time and the...

Страница 83: ...Fig 175 The start time always begins when the desired pH is reached If for example the target pH is reached after 25 seconds and the start time is 15 seconds the evaluation begins at 40 seconds Fig 1...

Страница 84: ...ax dosing speed ml min WA 05 10 WA 10 20 WA 20 40 WA 50 100 The filling speed can be set in terms of seconds from 20 to 240 The standard setting of this value is 30 seconds For diluted aqueous solutio...

Страница 85: ...performed after the next dosing step to find out whether the next dosing step can still be made without filling 4 6 9 Sample identification In the manual titration and in the preparation of solutions...

Страница 86: ...on curve Same as Standard documentation method contents Manual titration Method name date time sample description sample weight sample volume results and calculation formula N A Same as Short document...

Страница 87: ...to load one of the standard methods These methods have default parameters and can generally be used immediately without changes From the main menu press EDIT to access the methods menu Fig 184 Fig 184...

Страница 88: ...on of the titration agent Suitable for 1 component reagents Standard is pure water Sample 1 Component Method for sample titrations with 1 component reagents Sample 2 Component Method for sample titrat...

Страница 89: ...n Formula KF Titration The appropriate calculation formula is selected on the Formula selection submenu Fig 186 Fig 186 The following calculation formulae are available for automatic titration mode Fo...

Страница 90: ...re already introduced in 4 7 Fig 187 Fig 188 Generally applicable titration parameters Depending on the titration mode KF or dead stop titration it is possible to enter a variety of parameters The fol...

Страница 91: ...supplied The initial waiting extraction time can be specified between 0 and 999 seconds Fig 189 Fig 189 4 7 2 2 Conditioning only KF Conditioning is activated for every KF method It can be shut off vi...

Страница 92: ...the addition of the pretitration volume another defined span of time is observed as the waiting time before the next titration step is added The pretitration volume is automatically added to the titr...

Страница 93: ...Fig 196 Maximum titration time Can be set between 0 9999 seconds The default setting is 600 seconds The maximum titration time is generally used for KF titration which can create a high continuous dri...

Страница 94: ...sufficient The default drift value setting is 100 or 150 g min for sample titration 50 g min is the default setting for titer methods Endpoint A The range of the A input can be selected between 0 0 a...

Страница 95: ...usly Fig 199 Fig 198 Fig 199 Since the TitroLine 7800 features two measurement inputs two parameters can be measured simultaneously and recorded The measured value is then displayed value during a con...

Страница 96: ...y 2 nd reading the conductivity s cm Fig 201 Fig 201 you can adjust the corresponding parameters of the conductivity measurement Fig 202 and Fig 203 as the nonlinear nLF or linear temperature compensa...

Страница 97: ...5 C standard and 20 C Fig 204 Fig 204 In the linear temperature compensation you can adjust the temperature coefficient of 2 0000 1 K for the natural waters to other solutions Fig 205 Fig 205 The meas...

Страница 98: ...splay is shown with two measurement parameters from Fig 208 With continuous measurement the length of the measurement and the measurement frequency number of measuring points can be additionally speci...

Страница 99: ...be followed in a graph Fig 210 The values are stored in connected USB flash drive into a CSV file Fig 210 Examples of the measured values for a measurement with one Fig 211 and two Fig 212 measuremen...

Страница 100: ...sses are set in advance and the device is switched off and on once It is important that different addresses are set for more than one connected device In one method pre dosing can be performed with on...

Страница 101: ...tion parameter Fig 215 Fig 215 Confirm with ENTER OK Fig 216 Fig 216 Unless otherwise selected the Titration address will be int This is the short form for the use of the internal i e the own burette...

Страница 102: ...ave the setting in this example as it is and continue in the menu up to Pre dosing 1 Fig 218 Fig 218 Confirm the selection with ENTER OK Activate the pre dosing it ENTER OK Fig 219 und Fig 220 Fig 219...

Страница 103: ...d when starting the method There you can then select a variable volume But we set a fixed volume of 20 ml Fig 222 Fig 222 Confirm with ENTER OK You can set the following parameters in the pre dosing m...

Страница 104: ...5 When starting the method the internal and externally connected burettes are automatically filled This is followed by querying the sample name and weight if so parameterized and then the TITRONIC 300...

Страница 105: ...n the set waiting time is displayed Fig 227 Fig 227 The titration is then carried out as usual with the Titrator TitroLine 7800 Fig 228 Fig 228 The pre dosing with a second external burette runs accor...

Страница 106: ...ormed with an external burette As an example we perform a pH titration on EQ with an external TITRONIC 500 From the main menu Select EDIT followed by New method and confirm with ENTER OK Enter as meth...

Страница 107: ...automatically filled at the beginning Then the usual queries for sample designation and sample weight take place Then the titration begins The volume is displayed on the external device during titrat...

Страница 108: ...re dosed with the titrator Fig 235 It can be used with the titrator and e g the T 300 can be pre dosed Thereafter titration is carried out externally with the T 500 Fig 235 After each step a waiting t...

Страница 109: ...d in 2 5 Calibration settings 6 1 The Calibration settings item is used to select the buffers for the calibration of the pH electrode as well as to set the temperature of the buffer solution Fig 238 T...

Страница 110: ...0 0 to 100 0 C in increments of 0 1 Fig 239 Fig 239 The type of calibration items is used to define whether a 2 3 5 or 7 point calibration has to be performed Fig 240 Fig 240 The pH buffers can be det...

Страница 111: ...Fig 243 Interchangeable Unit Reagents 6 2 Each interchangeable unit is equipped with an RFID transponder This transponder can be used to store the following information Fig 244 Fig 246 Unit size the...

Страница 112: ...g 244 Fig 245 Fig 246 When you leave the Reagenzien WA menu using ESC you can adopt the values by Yes Fig 247 The updated values will be written into the RFID transponder of the interchangeable unit F...

Страница 113: ...here are information about the analog pH electrode slope zero and time of calibration and the digital display electrode Fig 248 Fig 250 It may also be the respective calibration routine to be started...

Страница 114: ...selected However also a temperature sensor with NTC 30 kOhm can be connected Fig 251 In a digital electrode of type batch number the software version the calibration of the electrode and the date of...

Страница 115: ...the device address of the TitroLine 7800 and set the parameters of the two RS 232 interfaces independent from each other Fig 253 Fig 253 The device address can be set from 0 15 Address 1 is the defaul...

Страница 116: ...set to 1200 19200 Fig 256 Fig 256 The parity can be selected amongst No Even and Odd No is the default setting Fig 257 Fig 257 You may select between 7 and 8 data bits 8 bits is the default setting Fi...

Страница 117: ...ase the titrator via the USB PC connection to the PC is connected Fig 259 Fig 260 For the USB connection a driver must be installed on the PC side The driver can be downloaded from the manufacturer we...

Страница 118: ...have access to the device anymore In this case please contact the service see backside of this document The administrator can create new users with different access levels to the instrument software...

Страница 119: ...n or more simple like ad Fig 265 Fig 265 Confirm with ENTER OK You have to enter now your full user name full name and then your password Fig 266 Fig 266 The password must have at least 5 characters A...

Страница 120: ...not have access to the device anymore In this case please contact the service see backside of this document We need only the serial number of the device Then we can create a master password for the d...

Страница 121: ...he example Fig 10 it is ad Fig 271 Fig 271 As administrator you have the rights to create new users with different levels If you start the titrator now you have to activate the user with crtl L Withou...

Страница 122: ...new users Fig 272 Fig 272 Confirm with ENTER OK Enter the user name of the new user The minimum characters are here two In the example Fig 273 it is Michael Fig 273 You have to enter the full user nam...

Страница 123: ...ve to enter the password Fig 276 and Fig 277 Confirm with ENTER OK Fig 276 Fig 277 6 6 3 Predefined rights and definable rights There are three predefined rights and the option of fully definable righ...

Страница 124: ...m the first Administrator The table below shows the access rights for the three predefined users Menu access functions User Extended user Administrator System settings No Yes Yes User management No No...

Страница 125: ...ights Fig 280 Fig 280 Confirm the selection with ENTER OK The default settings are always from a user if you do not have selected the extended user before X means no access W means access You can chan...

Страница 126: ...270 Fig 283 Fig 284 Fig 285 Fig 286...

Страница 127: ...on the external keyboard You select the user with the up and down keys and then press on DEL Fig 287 Fig 287 After DEL the user is immediately deleted without any additional request Fig 288 Fig 288 Yo...

Страница 128: ...t if you want easily The first administrator is still there Only a RESET will delete the first administrator RESET 6 7 RESET will reset all settings to the factory setting All methods will also be del...

Страница 129: ...94 System Tones 6 10 This is the point to set the volume of the system sounds and the front keyboard of the device Fig 295 The system sounds become audible e g at the end of the titration or in case o...

Страница 130: ...emory It is also possible to transfer the settings from one titrator to another one The backup will be started with Settings backup Fig 296 Fig 296 Backup settings is displayed during the backup in bl...

Страница 131: ...lder on the USB memory Stick starts with the backup date Fig 299 Fig 299 Confirm the selection with ENTER OK Settings are being restored is displayed during the restoring process of the backup in blue...

Страница 132: ...files that are needed have to be located in the root directory of the USB device Fig 302 Fig 302 Plug the USB device into a free USB A port wait for some seconds and then select the Software Update fu...

Страница 133: ...to the following display Fig 305 Fig 305 Upon completion of the update approx 4 5 minutes the device will shut down the software completely and proceed to a new start In the course of an update the m...

Страница 134: ...also set the output on a network printer Connect the titrator to your network with a suitable network cable Under System settings select the Network settings Fig 307 and Fig 307 conform the selection...

Страница 135: ...nter the share path Fig 311 Please ask your IT specialist what exactly this path is Fig 311 Complete the entry with ENTER OK Now enter your Username and Password for your corporate network Fig 312 Fig...

Страница 136: ...exiting the menu Now go back one step with ESC to the system settings Go to Printer selection Fig 313 Fig 313 And select Network share Fig 314 Fig 314 PDF and CSV files are now automatically saved on...

Страница 137: ...ers e g address 1 of the two ASCII characters 0 and 1 The addresses can be set from 00 to 15 i e 16 possibilities It must be ensured that the devices in a chain have different addresses If a device is...

Страница 138: ...function aay aagdm dosing speed in ml min 0 01 100 ml min aaY aaGF filling time in sec adjustable 20 999 seconds aaY aaGS output serial no Of device aaGS08154711 aaLC output of the CAL parameters aaL...

Страница 139: ...the balance must correspond to each other Additionally it is necessary to carry out some more standard settings on the side of the balances The balance is to send the balance data via RS 232 C only b...

Страница 140: ...t with the existing balance data will appear Fig 315 Fig 315 The balance data can be edited one by one Following a change a star will appear opposite the weighed in quantity Fig 316 Fig 316 Weights ma...

Страница 141: ...F and CSV format To connect the printers to the burette please use the USB socket When printing please check whether the correct printer is connected It is not possible to print HP printer layouts on...

Страница 142: ...ng in the system menu Connect the magnetic stirrer with the USB cable to one of the two USB A sockets Under System Settings select Stirrer Control Fig 320 Fig 320 Confirm the selection with ENTER OK T...

Страница 143: ...ring speed in the titration parameters can be set for each method Fig 323 and Fig 324 Fig 323 Fig 324 The stirring speed can also be set individually for the individual pre dosing steps the pre titrat...

Страница 144: ...the titrator by cable TZ 3987 The settings of the RS232 2 interface do not have to be changed They can remain at 4800 No 8 1 Using software TitriSoft 9 6 9 6 1 General The titrator is connected to the...

Страница 145: ...over time which includes e g crystalisation Considering that as of the state of the art there are no plastic hoses available for the use in titration equipment which would be perfectly free of diffus...

Страница 146: ...cal damage Defective parts have to be repaired or replaced by new parts 9 Please refer to the application Burette inspection according to ISO 8655 Part 6 11 Guarantee We provide guarantee for the devi...

Страница 147: ......

Страница 148: ...es pour le produit sont respect es Certificado del fabricante Certificamos que el aparato arriba mencionado ha sido controlado de acuerdo con la norma DIN EN ISO 9001 secci n 8 2 4 Seguimiento y medi...

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