TAI Model 6200A SO
2
Analyzer Operator Manual, 02164, Rev. G
6.5 Permeation Tube (used with IZS option)
SO
2
is normally a gas at room temperature and pressure, but can be liquefied at moderate
pressures. The permeation tube consists of a small container of SO
2
liquid, with a small window
of PTFE which is permeable to SO
2
. The gas slowly permeates through the window at a rate in
the nanogram/min range. If the tube is kept at constant temperature, usually about 50
o
C, the
device will provide a stable source of SO
2
gas for a year or more.
The IZS permeation tube is
intended to be used as a periodic span check and is not to be used as a calibration device.
See below for permeation tube ordering information.
The permeation tube SO
2
concentration is determined by the permeation tube specific output (ppb @
1 slpm @ 50
o
C), the permeation tube temperature (
o
C) and the air flow across it (slpm). The specific
output is a fixed function of the permeation tube and is noted on shipping container.
The temperature is set at 50.0
o
C. Check SETUP-MORE-VARS and scroll to the IZS_SET variable
to verify that the temperature is properly set. It should be set to 50
o
C with over-and-under
temperature warnings set at 49
o
C and 51
o
C. There is a 50 cc/min purge flow across the permeation
tube at all times to prevent build-up of SO
2
gas in the tubing.
If desired, the output of the permeation tube can be adjusted by adjusting the oven temperature up or
down slightly. The adjust increment is 0.1
o
C to facilitate small adjustments of the setpoint
temperature.
When the IZS system is in SPAN mode, the flow across the permeation tube is the sum of the
reaction cell flow and the purge flow, which is about 700 cc/min. The gas concentration can be
calculated using following equation;
F
PxKm
C
=
where
P=permeation rate, ng/min.@ 50
o
C.
Km=(24.46)/molecular weight, where 24.46 is the molar volume in liters @ 25
o
C,
760mmHg
Km for SO
2
=0.382, H2S=0.719.
F=total flow rate (sum of sample flow and purge flow), cc/min.
C=concentration, ppm.
6-6
Содержание 6200A
Страница 1: ...MODEL 6200A TRS ANALYZER MANUAL ADDENDUM TELEDYNE ANALYTICAL INSTRUMENTS 03655 Rev A August 2000 ...
Страница 9: ...TAI Thermal Converter Operator Manual Page 5 FIGURE 2 1 BASIC CONFIGURATION ...
Страница 10: ...TAI Thermal Converter Operator Manual Page 6 FIGURE 2 2 WITH IZS OPTION ...
Страница 11: ...TAI Thermal Converter Operator Manual Page 7 FIGURE 2 3 WITH M702 CALIBRATOR OPTION ...
Страница 13: ...TAI Thermal Converter Operator Manual Page 9 FIGURE 2 4 TRS CONVERTER LAYOUT ...
Страница 15: ...TAI Thermal Converter Operator Manual Page 11 FIGURE 2 5 PNEUMATIC CONNECTIONS ...
Страница 22: ...TAI Thermal Converter Operator Manual Page 18 FIGURE 3 1 TRS WIRING DIAGRAM ...
Страница 25: ...TAI Thermal Converter Operator Manual Page 21 FIGURE 4 1 DILUTER FLOW BLOCK ASSEMBLY ...
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Страница 40: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 2 1 Removal of Shipping Screws 2 3 ...
Страница 41: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 2 2 Rear Panel 2 4 ...
Страница 42: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 2 3 Rear Panel Pneumatic Recommendations 2 5 ...
Страница 47: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 2 4 Front Panel 2 10 ...
Страница 48: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 2 5 Assembly Layout 2 11 ...
Страница 51: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G INTENTIONALLY BLANK 2 14 ...
Страница 58: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 4 1 6200A Sulfur Dioxide Analyzer 4 3 ...
Страница 65: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 5 2 Setup Menu Tree 5 2 ...
Страница 89: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 6 1 Permeation Tube Installation 6 8 ...
Страница 107: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G INTENTIONALLY BLANK 6 26 ...
Страница 110: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 7 1 Model 6200A Calibration Setup 7 3 ...
Страница 136: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 8 1 Replacing the Particulate Filter 8 3 ...
Страница 140: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 8 2 Reaction Cell 8 7 ...
Страница 141: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 8 3 Pneumatic Diagram 8 8 ...
Страница 175: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 1 CPU Board Jumper Settings 9 32 ...
Страница 184: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 3 V F Board Dip Switch Settings 9 41 ...
Страница 189: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 4 Power Supply Module Layout 9 46 ...
Страница 190: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 5 Electrical Block Diagram 9 47 ...
Страница 193: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 6 Flow Pressure Sensor 9 50 ...
Страница 194: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 7 SO2 Sensor Module 9 51 ...
Страница 195: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 8 SO2 Sensor Module 9 52 ...
Страница 198: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 9 PMT Cooler Subsystem 9 55 ...
Страница 204: ...TAI Model 6200A SO2 Analyzer Operator Manual 02164 Rev G Figure 9 11 Kicker Leak Check 9 61 ...
