background image

EXTRACTION FLOW ADJUSTMENT

 

 
The System 96-II Pressure Processor has a two-level gas delivery system used to 
pressurize the SPE columns. 
 
One part of the system is controlled by the rotameter located on the left side of 
the instrument panel.  By switching the “SPE FLOW RATE” selector to the left, 
“ADJUST FLOW” setting, the gas is delivered to the SPE Column Manifold 
through the adjustable flow regulator and then thru the rotameter controlled by 
the needle valve located at its base.  The rotameter route provides a very precise 
and slow flow through the SPE columns by limiting the gas flow to the manifold 
from 0 to 2.5 SCFH.  
 
NOTE: 
The rotometer needle valve is for adjustment only and is NEVER to be used as an 
on off valve. Use the selector valve to turn off the nitrogen flow. 

 
The second part of the gas delivery system provides for rapid gas flow to the 
manifold.  This flow is controlled by adjusting the regulator located below the 
pressure gauge labeled “MAX FLOW.”  The pressure range is 0-80 psig and is 
used to maximize flow through the SPE columns for processing viscous or high 
particulate samples or to dry the columns in situ.  By switching the “SPE FLOW 
RATE” selector to “MAX FLOW”, gas is introduced to the manifold at the 
pressure set on the “MAX FLOW” regulator as indicated by the gauge located 
directly above it. 
 
By turning the “SPE FLOW RATE” selector to off, no gas will flow to the manifold.  
It should be in the off position during the compression and decompression 
cycles and when not in use.  
 
Note that the regulator is of the “locking” type.  The regulator can be adjusted by 
pulling out on the regulator knob and turning it to the desired pressure.  Once the 
desired pressure is set, it can be “locked in” by pushing in on the knob. 
 

MAINTENANCE

 

 

The System 96-II Pressure Processor is a rugged unit constructed of anodized 
aluminum, stainless steel and plastics.  However, the following items should be 
observed during operation: 
 
1. Solvent spillage or overflow should be cleaned immediately in order to prevent  
    instrument damage. 
 
2. The column seal is silicone rubber and can be cleaned with methanol. 

 

 

7

Содержание CEREX SYSTEM 96-II

Страница 1: ...OPERATING INSTRUCTIONS CEREX System 96 II MULTI CHANNEL SPE CEREX 96 II manual rev B ...

Страница 2: ...2 ...

Страница 3: ... atmosphere operation If this is not a consideration the unit can operate using high purity filtered instrument air This instrument is supplied with an installation kit which includes 6 feet of 1 8 i d 1 4 o d polyethylene tubing and connectors to 1 8 NPT or 1 4 NPT Using the tubing and fittings provided connect the unit to a regulated oil free gas source Optimum Source Pressure is 80 psig Min Pre...

Страница 4: ...he re usable CEREX Holder interfaces to several collection plates which are also in the 96 position format Depending upon the volume of the effluent the appropriate collection tray can be selected from the ancillary products available The CEREX Holder is keyed to the collection plates so that sample position is preserved throughout the SPE sequence Both the CEREX Holder and collection plates are k...

Страница 5: ...the exact same time to open or close the compression mechanism Activate the column compression mechanism by depressing the push buttons until the manifold has stopped moving 2 to 3 seconds If you let go too soon the manifold mechanism will automatically open This is a safety feature designed to keep your hands clear of moving parts during the compression and decompression cycle Decompression of th...

Страница 6: ...p ressu re b u ild s en o u g h to o v erco m e th e flu id flo w resistan ce an d th e flu id b eg in s to p ass th ro u g h th e so rb en t b ed In p u t P re s s u re P 3 0 p s i 2 4 p s i 2 4 p s i 2 4 p s i 3 0 p s i 3 0 p s i 3 0 p s i F ig C D ep en d in g o n flo w ch aracteristics o f co lu m n so rb en t b ed p ressu re in co lu m n reserv o ir stab ilizes In h ib itin g th e flo w w ith...

Страница 7: ...labeled MAX FLOW The pressure range is 0 80 psig and is used to maximize flow through the SPE columns for processing viscous or high particulate samples or to dry the columns in situ By switching the SPE FLOW RATE selector to MAX FLOW gas is introduced to the manifold at the pressure set on the MAX FLOW regulator as indicated by the gauge located directly above it By turning the SPE FLOW RATE sele...

Страница 8: ...al is silicone rubber and may be cleaned regularly with methanol WARRANTY The System 96 II Pressure Processor is warranted for 90 days Warranty repairs will be made given that the product has not been abused It is constructed primarily of stainless steel and anodized aluminum Other materials include silicone rubber polyethylene and polypropylene The controls and gauges are not solvent resistant So...

Страница 9: ... assists in removing residual moisture The temperature is preset on the Temperature Control Unit and requires minimal heat up time This in turn not only yields higher analyte recovery it also allows the sorbent bed to be eluted with a more selective solvent like hexane or ethyl acetate The result is an extract that is highly purified and free of interferences 9 ...

Страница 10: ...10 ...

Страница 11: ...11 ...

Отзывы: