Shodex R I-502, Руководство по эксплуатации

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Appendix Appendix Appendix Appendix 1 1 1 1
P
P P
Prrrroper
oper oper
opertttty
y y
y Data
Data Data
Data of Solvents
of Solvents of Solvents
of Solvents
Polarity
E
2
(Al
2
O
3
)
Viscosity
(cP20℃)
Refractive
Index
UV Flash
Fire Point
Vapor
Density
Boiling
Gravity
Cut-off Point Point
(nm) (℃) (℃) Lower Upper (℃)
Fluoroalkanes -0.25 - 1.25 0
n-Pentane 0.00 0.23 1.358 210 <-40 308.9 1.5 0 7.8 2.5 0 36.1 0.6
Hexane 0.00 1.375 210 -21.7 233.9 1.2 0 7.5 3.0 0 68.9 0.7
Isooctane 0.01 1.404 210
Petroleum ether 0.01 0.3 0 210
n-Decane 0.04 0.92 1.412 0 46.1 207.8 0.8 0 5.4 4.9 173.9 0.7
Cyclohexane 0.04 1.00 1.427 210 -20 .0 260 .0 1.3 0 8.0 2.9 0 81.7 0.8
Cyclopentane 0.05 0.47 1.406 210
Diisobutylene 0.06 1.411 210
i-Pentene 0.08 1.371 -17.8 272.8 1.5 0 8.7 2.4 0 30 .0 0.7
Carbon disulfide 0.15 0.37 1.626 380 -30 .0 100 .0 1.3 44 .0 2.6 0 46.1 1.3
Carbon tetrachloride 0.18 0.97 1.466 265
Amyl chloride 0.26 0.43 1.413 225 0 12.8 343.3 1.6 0 8.6 3.7 106.1 0.9
Butyl chloride 0.26 1.436 220 0 -9.4 460 .0 1.8 10.1 3.2 0.9
o-17.2 463.9 1.0 0 6.0 144.4
Xylene 0.26 290 m-25 527.8 1.1 0 7.0 3.7 138.9
p-25 528.9 1.1 0 7.0 138.3
i-Propyl ether 0.28 0.37 1.368 220 -27.8 443.3 1.4 21 .0 3.5 0 68.9 0.7
i-Propyl chloride 0.29 0.33 1.378 225 -32.2 593.3 2.8 10.7 2.7 0 35 .0 0.9
Toluene 0.29 0.59 1.496 285 00 4.4 536.1 1.4 0 6.7 3.1 110.6 0.9
n-Propyl chloride 0.30 0.35 1.389 225 <-17.8 2.6 11.1 2.7 0 46.1 0.9
Chlorobenzene 0.30 0.80 1.525 0 32.2 637.8 1.3 0 7.1 3.9 132.2 1.1
Benzene 0.32 0.65 1.501 280 -11.1 562.2 1.4 0 7.1 2.8 0 80 .0 0.9
Ethyl bromide 0.37 1.424 511.1 6.7 11.3 3.8 0 37.8 1.4
Ethyl ether 0.38 0.23 1.353 220 -45 .0 180 .0 1.9 48 .0 2.6 0 35 .0 0.7
Ethyl sulfide 0.38 0.45 1.442 290
Chloroform 0.40 0.57 1.443 245
Methylene chloride 0.42 0.44 1.424 245 -50 .0 518.9 3.8 15.4 2.2 0 38.5 0.9
Methyl i-butyl ketone 0.43 1.394 330
Tetrahydrofuran 0.45 1.408 220 -14.4 321.1 2.0 11.8 2.5 0 66.1 0.9
Ethylene dichloride 0.49 0.79 1.445 230 0 13.3 412.3 6.2 16 3.4 0 83.9 1.3
Methyl ethyl ketone 0.51 1.381 330 0 -6.1 515.6 1.8 10 2.5 0 80 .0 0.8
i-Nitropropane 0.53 1.400 380 0 48.9 420.6 2.6 3.1 131.1 1.0
Acetone 0.56 0.32 1.359 220 -17.8 537.8 2.6 12.8 2.0 0 56.7 0.8
Dioxane 0.56 1.54 1.422 260 0 12.2 180 .0 2.0 22 3.0 101.1 1.0
Ethyl acetate 0.58 0.45 1.370 260 00 4.4 460 .0 1.8 8 3.5 0 90 .0 0.9
Methyl acetate 0.60 0.37 1.362 210 -10 .0 501.7 3.1 16 2.6 0 60 .0 0.9
Amyl alcohol 0.61 4.1 0 1.410 0 32.8 300 .0 1.2 10.0 3.0 137.8 0.8
Dimethyl sulfoxide 0.62 2.24
Aniline 0.62 4.4 0 1.586 0 70 .0 617.2 1.3 3.2 184.4 1.0
Dimethyl amine 0.63 0.38 1.387 275 <-17.8 312.2 1.8 10.1 2.5 0 56.7 0.7
Nitromethane 0.64 0.67 1.394 380 0 35 .0 418.3 7.3 2.1 101.1 1.1
Acetonitrile 0.65 0.37 1.344 210 00 5.6 1.4 0 81.7 0.8
Pyridine 0.71 0.94 1.510 305 0 20 .0 1.8 12.4 2.7 115 . 0 1.0
Butyl cellosolve 0.74 220
i-Propanol n-Propanol 0.82 2.3 0 1.38 0 210 0 11.7 398.9 2.0 12 2.1 0 82.8 0.8
Ethanol 0.88 1.20 1.361 210 0 12.8 422.8 4.3 19 1.6 0 78.3 0.8
Methanol 0.95 0.60 1.329 210 0 11.1 463.9 7.3 36 1.1 0 63.9 0.8
Ethylene glycol 1.11 19.9 00 1.427 210 111.1 412.8 3.2 197.2 1.1
Acetic acid 大 1.26 1.372
Water 大 1.333
* L. R. Snyder. Dekker. ｢Principles of Adsorption Chromatography｣
Those in should not be employed