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Seres OL SOL-96.110.071, Руководство оператора

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SOL-96.110.071 / 180122

TOPAZ Aluminum

Startup

24

 

4.3. Priming the Reagent Tubes

Note: 

• Before priming the reagent tubes, make sure that the sample 

inlet tap is open.

• To avoid chemical reactions in the photometer, fill the reagent 

tubes one after the other, not simultaneously.

Enter the

Electrical test

menu

1

Turn the power switch to the ON position.

The peristaltic pumps are automatically readjusted and the 

panel PC starts.

2

Stop the measuring cycle by pressing the   button and entering 

the password “0712”.

3

Open the <TOOLS> tab and press the <Electrical test> button.

Check

transparent

reagent tubes

To check the flow through the transparent reagent tubes, perform the 

following steps:

4

Open the <ACTUATOR> tab and set “SV Filling” to <ON>.

MEASURE

DIAGNOSTIC

+

TOOLS

Maintenance

Electrical test

Maintenance

Maintenance

Electrical test

ON

ON

ON

ON

OFF

OFF

OFF

OFF

Stirrer

SV Emptying

Heating

SV Filling

ACTUATOR

4-20mA OUTPUT

PUMPS

RELAYS

INPUTS

Vessel temperature :

27.48 °C

Содержание SOL-96.110.071

Страница 1: ...TOPAZ Aluminum Operator s Manual TOPAZ Aluminum SOL 96 110 071 180122...

Страница 2: ...ed staff of technical specialists around the world For any technical question contact your nearest Seres OL representa tive or the manufacturer Seres OL SAS ZA de la Sipi re 219 Avenue de Provence FR...

Страница 3: ...s on I O Board 14 3 4 2 Cable thicknesses 18 3 4 3 AC power 19 3 4 4 Jbus via RS485 20 3 4 5 Jbus via TCP IP Option 21 4 Startup 22 4 1 Installing the Reagent Bottles 22 4 2 Starting Sample Flow 23 4...

Страница 4: ...inum 2 6 6 3 Standard Calibration 41 6 7 Longer Stop of Operation 42 7 Configuration of the Analyzer 43 8 Troubleshooting 47 8 1 What To Do If 47 8 2 List of Errors and Alarms 51 8 3 Saving Diagnostic...

Страница 5: ...ty instructions are given throughout this manual at the respective locations where observation is most important Strictly follow all safety instructions in this publication Target audience Operator Qu...

Страница 6: ...the prevention instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the equi...

Страница 7: ...071 180122 TOPAZ Aluminum Safety Instructions 5 Warning signs The warning signs in this manual have the following meaning Electrical shock hazard Corrosive Harmful to health Flammable Hot surface Gene...

Страница 8: ...ordance with the local regula tions of the respective country WARNING Electrical shock hazard If proper operation is no longer possible the instrument must be disconnected from all power lines and mea...

Страница 9: ...er and check it for visible damage If the analyzer shows any visible damage do not connect it to power and contact customer service immediately 1 4 International Symbols Used The symbols found on the...

Страница 10: ...channels common measuring range Signal outputs Two signal outputs per measuring channel Current loop 4 20 mA Relays Five potential free contacts per measuring channel with the following functions two...

Страница 11: ...nces and dust Process connections Sample inlet Sample outlet Sample outlet waste 1 4 BSP F soft tubing D INT 9 single channel soft tubing D INT 19 multi channel soft tubing D INT 12 Sample requirement...

Страница 12: ...180122 TOPAZ Aluminum Product Description 10 Wall cabinet Material Screws Weight Protection degree Stainless steel SS316L 4x M6 6x M6 with reagent shelf 35 kg IP55 Reagent shelf made of SS316L availab...

Страница 13: ...scription 11 2 2 Instrument Overview A B C D E F G H I J K Power switch Touchscreen Cable glands Peristaltic pumps Photometer Air cleaning inlet Pressure reducing device Calibration vessel Sample inle...

Страница 14: ...ca tions p 9 3 2 Mounting the Wall Cabinet Mounting requirements Mount the instrument in vertical position The display should be at eye level to simplify operation and maintenance For dimensions see d...

Страница 15: ...the instrument from a power outlet which has a protec tive earth connection Overview of electrical connections 1 In multi channel instruments there is an I O board for each measuring channel The I O b...

Страница 16: ...d to control internal components of the analyzer Do not connect anything else to these contacts Analog signal output OUT_ANA2 is reserved for customized versions of the analyzer that provide a second...

Страница 17: ...pins 1 and 4 unconnected Analog signal outputs 4 20 mA Name Available on Description IN_DIG1 all measuring channels Activates or deactivates the measuring channel Open contact Measuring channel will b...

Страница 18: ...e Analyzer p 43 Name Available on Description OUT_DIG2 all measuring channels Sample flow alarm OUT_DIG3 all measuring channels Threshold 1 OUT_DIG4 all measuring channels Threshold 2 OUT_DIG5 all mea...

Страница 19: ...onfigured as normally open or normally closed by setting the corresponding jumpers on the I O board The default setting is normally open jumper in the right position A Location of jumpers on I O board...

Страница 20: ...luminum Installation 18 3 4 2 Cable thicknesses In order to comply with IP55 use the following cable thicknesses Note Seal cable glands that are not in use A B Outer diameter of cable 7 5 13 mm Outer...

Страница 21: ...0122 TOPAZ Aluminum Installation 19 3 4 3 AC power Ferrite Wrap the mains cable two times around the supplied ferrite A B C Protective earth PE terminal 3 Neutral conductor terminal 2 Phase conductor...

Страница 22: ...SOL 96 110 071 180122 TOPAZ Aluminum Installation 20 3 4 4 Jbus via RS485 Terminals Terminal 1 data B terminal 2 data A A RS485 interface A...

Страница 23: ...lyzer The connection is made via the Ethernet port located on the right side of the analyzer exterior Mount the supplied connector onto the Ethernet cable and connect it to the port Addressing modes T...

Страница 24: ...f all reagent tubes are cut at an angle This will prevent the tube ends from lying flat on the bottom of the bot tles 2 Check that there are two holes in the lid of each reagent bottle one hole to fee...

Страница 25: ...122 TOPAZ Aluminum Startup 23 4 2 Starting Sample Flow Open the sample tap C so that a part of the sample overflows into the pressure reduction device A A B C Pressure reduction device Inner tube Samp...

Страница 26: ...ically readjusted and the panel PC starts 2 Stop the measuring cycle by pressing the button and entering the password 0712 3 Open the TOOLS tab and press the Electrical test button Check transparent r...

Страница 27: ...6 6 2 8 Let the pump run until the fluid has reached the photometer and there is no more air in the tube This takes approximately 2 5 minutes The pump stops automatically 9 Repeat steps 7 8 with pumps...

Страница 28: ...R tab 11 Set SV Emptying to ON and SV Filling to OFF and wait until the instrument is empty 12 Then set SV Emptying and Stirrer to OFF as well ON ON ON ON OFF OFF OFF OFF Stirrer SV Emptying Heating S...

Страница 29: ...ter and wait until the reagent arrives in the photometer This takes approximately 2 5 minutes The pump stops automatically 17 Go back to the ACTUATOR tab 18 Set Stirrer to ON 19 Check that the stirrer...

Страница 30: ...ecessary 2 Calibrate the analyzer if required For detailed descriptions see Manual Measurement and Calibration p 39 4 6 Programming Program the following parameters if applicable Concentration values...

Страница 31: ...d access levels User access Allows viewing data in the main window Access with extended permissions Allows stopping the measurement changing settings and performing maintenance tasks The password for...

Страница 32: ...last manual measurement C Measured value D Trend E Measuring cycle information Stream that is being measured Number and description of step in measurement cycle Total number of steps to be completed...

Страница 33: ...esult is satisfactory no calibration is needed If necessary calibrate the instrument Every 3 months Replace all peristaltic pump tubes After replacement of peristaltic pump tubes perform a manual meas...

Страница 34: ...ubes one after the other not simultaneously Proceed as follows 1 Remove all reagent tubes from their bottles and place them in a beaker filled with deionized water 2 Open the PUMPS tab 3 Press the ON...

Страница 35: ...ACTUATOR tab and set SV Filling to ON 7 Wait until the photometer has been filled with fresh water Then set SV Filling to OFF ON ON ON ON OFF OFF OFF OFF Stirrer SV Emptying Heating SV Filling ACTUATO...

Страница 36: ...ntamination or dilution errors Reagent consumption At the standard measurement interval the following amounts of reagents are consumed Replacing reagents 1 Prepare the reagents according to the separa...

Страница 37: ...Hexamethylenetetramine PTFE 1 6 3 2 21 Phenantrolin PTFE 1 6 3 2 22 Phenantrolin PTFE 1 6 3 2 31 Pyrocatechol violet PTFE 1 6 3 2 black 32 Pyrocatechol violet PTFE 1 6 3 2 black 91 HCl 2N Al 400 g l...

Страница 38: ...SVB NC Silicone 5 8 Calibration vessel B SVB NO Silicone 5 8 SVB C Sample inlet right of photometer D Silicone 5 8 Water fault sensor U1 Silicone 2 5 Photometer sample outlet left SVA NC Tygon 5 8 SV...

Страница 39: ...ear appropriate protective equipment gloves glasses protective clothing 1 Flush the reagent tubes with deionized water as described in Stop of Operation for Maintenance p 32 2 Turn the power switch to...

Страница 40: ...the tube around the rotor while turning it 6 Connect the other tube end to the left side fitting 7 Install the front cover on the pump 8 Insert the reagent tubes all the way to the bottom of the corre...

Страница 41: ...ntact customer service for details Entering the maintenance menu 1 To stop the current measuring cycle press the button on the main screen and enter the password 0712 In the next dialog confirm with O...

Страница 42: ...l A with the standard 3 Wait until the calibration vessel is empty and the message Add standard appears again 4 Repeat steps 2 and 3 until the measurement starts automatically 5 When the measurement i...

Страница 43: ...stream 1 Procedure The procedure is similar to the manual measurement procedure described in Manual Measurement p 40 Begin calibration by entering the reference value of the standard used Pay attentio...

Страница 44: ...as follows 1 Prime the reagent system with deionized water as described in Stop of Operation for Maintenance p 32 2 Clean the photometer thoroughly with diluted hydrochloric acid Note Do not use a bot...

Страница 45: ...by Seres OL customer service pressure setting Setpoint of the water fault sensor Adjust this value only if instructed to do so by Seres OL customer service Gain setpoint Setpoint of the electronic ga...

Страница 46: ...n mea surement cycles Note Since the analyzer is designed for continuous operation a maximum duration of 15 minutes is recommended for pauses 1 Press the Add button and select one of the following opt...

Страница 47: ...3 and OUT_DIG4 are high or low thresholds The combinations high high low high and low low are possible The threshold values can be set in the parameter menu see 46 DATE TIME tab Set time and date A B...

Страница 48: ...ld value is made in the THRESHOLD tab of the OPTIONS menu Threshold 2 Threshold value for relay OUT_DIG4 The definition as high or low threshold value is made in the THRESHOLD tab of the OPTIONS menu...

Страница 49: ...r message Water default although there is sample flow Possible cause Corrective action No power on the socket Check mains power supply Power supply defective Check output voltage of the internal 24 vo...

Страница 50: ...ptying solenoid valve SVA does not switch Check that the solenoid valve is plugged in correctly If necessary change the membrane Possible cause Corrective action Pump does not work properly Check that...

Страница 51: ...passed or if the reagents have been stored incorrectly If necessary replace the reagents Check that the reagents are of Analysis Use quality ask supplier Tubes connected to the wrong reagent containe...

Страница 52: ...s working correctly if present If no filter system is installed it might be necessary to install one Water does not drain Check that the drain is pressure free and not blocked Check condition of empty...

Страница 53: ...If the error persists contact customer support 5 Error reading cycle zero configuration Reset analyzer configuration to factory defaults by pressing the Recover button in the tab 6 Error writing cycle...

Страница 54: ...ve optical measure value in the DIAGNOSTIC tab With a functioning measuring card the value changes continuously If the value does not change restart the analyzer and check again If the error persists...

Страница 55: ...e INPUT tab and test the digital inputs If the error persists contact customer support 20 Error reading on IO card Check if all I O boards work properly Navigate to TOOLS Electrical test Open the RELA...

Страница 56: ...utton in the tab 25 Error reading on JBUS slave card Check request compliance with JBUS protocol 26 Error treatment on JBUS slave card Check request compliance with JBUS protocol 27 Error reading meas...

Страница 57: ...replace the membrane Check sample tubes 33 Optical setting Default Info setting not received Observe the Live optical measure value in the DIAGNOSTIC tab With a functioning measuring card the value c...

Страница 58: ...ncentration after linearization 0 or Calibra tion Coeff 0 Check if the calibration coefficient is equal to zero In this case make a new calibration Check if the final absorbance is equal to zero If th...

Страница 59: ...ue out of range Check that the analyzer is well calibrated check standard solution concentration by a manual measure cycle 45 Division by zero Absorbance 999998 0 Check that the optical fibers are wel...

Страница 60: ...255 analyzer cannot adjust the optical gain Check that the optical fibers are well connected to their holder on the door Check that the photometer is not dirty Check that the analyzer is supplied wit...

Страница 61: ...USB stick into the USB port A on the back of the panel PC 3 Open the TOOLS tab and press the Log files copy button Enter the password 0712 if necessary 4 On the next screen press OK to start data tra...

Страница 62: ...TOPAZ Aluminum Notes SOL 96 110 071 180122 60 9 Notes...

Страница 63: ...SOL 96 110 071 180122 TOPAZ Aluminum Notes 61...

Страница 64: ...i l G a s Seres OL SAS FR 13730 Saint Victoret www seres ol com info seres ol com Seres OL Products Analytical Instruments for Seres OL is represented worldwide by subsidiary companies and distributor...

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