Radleys GreenHouse Скачать руководство пользователя страница 8

GreenHouse Blowdown Parallel Evaporation System

Using Blowdown Head with an Existing GreenHouse Synthesiser

Existing GreenHouse users need only purchase the RR99657 System 11 -

GreenHouse Blowdown Basic Upgrade kit. This allows users to do blowdown

evaporation in a standard GreenHouse reaction block with reaction tubes. 

Should users wish to use the GreenHouse Blowdown Evaporator for other vials or

micro titer plates, users need to purchase the RR99658 System 12 - GreenHouse

Blowdown Complete Upgrade kit.

Set-Up & Operation

- continued

Fitting the Blowdown Pin Plate to the Blowdown Head

Select the appropriate

Blowdown Pin Plate. 

Fix the Blowdown Pin

Plate to the Blowdown

Head by locating it

over the two pins on 

the underside of the 

head and securing 

it with the securing 

screws (orange handles).

Warning

The GreenHouse Blowdown Head should only be operated 

in a fume cupboard.

!

Important Note

Take care not to over tighten these fixing screws as this can 

damage the threads.

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important, 

Important Note

Allow the Reaction Block to cool to ambient temperature before

attempting to transfer or evaporate the solvent. 

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important, 

Place GreenHouse Reaction Block with reaction tubes containing solvent to be

evaporated into the GreenHouse base, taking note of the appropriate rack

position (A1-D6) for each sample. 

Alternatively if a reaction has just been performed in the GreenHouse, simply

remove the Reflux or Additions Head and replace with the GreenHouse

Blowdown Head.

Ensure that the circular gasket is properly located in its groove, then carefully

place glass chamber on to silicone (or optional Viton) gasket. 

1

2

RR99673

6 x 4 Blowdown 

Pin Plate for 24

position Vial

Racks 

or MTPs 

RR99672

6 x 4 Blowdown 

Long Pin Plate

for GreenHouse

Reaction Block and

Reaction Tubes

RR99674

4 x 2 Blowdown 

Pin Plate for 8 

position Vial Racks 

or MTPs 

Page 7

Содержание GreenHouse

Страница 1: ...down Parallel Evaporation System Your Local Distributor February 2023 Issue 5 Radleys Shire Hill Saffron Walden Essex CB11 3AZ United Kingdom Tel 44 0 1799 513320 Fax 44 0 1799 513283 Email sales radl...

Страница 2: ...6 Set up Operation Page 7 Set up Operation continued Page 8 Set up Operation continued Page 9 Set up Operation continued Page 10 Temperature Control Page 11 Example Evaporation Times Examples of Blow...

Страница 3: ...rays GreenHouse Blowdown Evaporator System is ideal for the evaporation of HPLC fractions in vials or micro titer plates Digitally controlled heating from a standard Carousel or IKA stirring hotplate...

Страница 4: ...ing blowdown ALWAYS ENSURE that inert gas flow rate is within recommended limits Page 3 Warning Applies when there is a possibility of personal injury Important Note Alerts the user to important facts...

Страница 5: ...9684 Blowdown Condenser RR99688 Blowdown 150ml Reservoir RR99658 System 17 GreenHouse Blowdown Complete Upgrade Comprising of the following RR99670 GreenHouse Blowdown Head RR99672 Long Blowdown Pin P...

Страница 6: ...wdown Condenser RR99688 Blowdown 150ml Reservoir RR99691 AT01 Vial Rack 4 x 2 For 27 8mm OD Vials RR99692 AT02 Vial Rack 6 x 4 For 13mm OD Vials RR99693 AT03 Vial Rack 6 x 4 For 13 8mm OD Vials RR9969...

Страница 7: ...ing giving them superior chemical resistance to most solvents and acids when compared with unplated aluminium or stainless steel They also contain Hastelloy springs and use a Kalrez fluoropolymer seal...

Страница 8: ...can damage the threads Important Important Important Important Important Important Important Important Important Important Important Important Important Important Important Note Allow the Reaction Blo...

Страница 9: ...tightening may damage the thread Do not use a spanner or wrench to tighten sealing knobs Important Important Important Important Important Important Important Important Important Important Important...

Страница 10: ...reduced for thermally less stable compounds See page 13 for important information on pressure control Important Note If the tubes are more than half full use a slower flow rate increasing the flow rat...

Страница 11: ...re to the desired level by following the instructions of RR98073 Fuzzy Logic Digital Temperature Controller The set temperature can be maintained to 0 5 C The maximum recommended operating temperature...

Страница 12: ...ad Standard GreenHouse Base and GreenHouse Reaction Block GreenHouse with Blowdown Head Standard GreenHouse Base Base Adapter and 24 Position Vial Rack GreenHouse with Blowdown Head Standard GreenHous...

Страница 13: ...Important Important Important Important Important Important Important Important Important Important Important Important Important AT01 AT05 AT06 AT03 AT02 Base Adapter with 8 position vial rack Base...

Страница 14: ...portant Warning The Blowdown Head Safety Pressure Relief Valve and Gas Inlet Safety Pressure Relief Valve are designed to vent at nominally 4 to 6psi Therefore under normal and correct operation proce...

Страница 15: ...with Silicone Rubber It is also more resistant to aromatic hydrocarbons Viton exhibits relatively good resistance to trifluoroacetic acid TFA and is the preferred gasket in this case Thermal Resistan...

Страница 16: ......

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