Radleys GreenHouse Скачать руководство пользователя страница 14

GreenHouse Blowdown Parallel Evaporation System

Preventing Over-pressurisation

After Evaporation

Should over-pressure venting occur:

1. Immediately turn off gas supply

2. Either disconnect gas inlet or lift Blowdown Head Safety Pressure Relief Valve

to remove excess pressure.

3. Immediately turn off any heating.

Important Note

Allow dry ice/acetone mixture to reach ambient temperature before

disposing of it into a suitable waste solvent container. 

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important,

Important, Important, 

Warning

The Blowdown Head Safety Pressure Relief Valve and Gas Inlet

Safety Pressure Relief Valve are designed to vent at nominally 

4 to 6psi. Therefore under normal and correct operation 

procedures neither valve should be venting.

!

When evaporation is complete:

a. Turn off heat and allow gas to flow until the base unit is cool

b. Turn off inert gas supply

c. Disconnect gas inlet and outlets to Blowdown Head

d. Remove the two sealing knobs and remove the Blowdown Head

e. Carefully remove the circular glass and lift out the rack

f. Remove flask from bottom of cold trap and allow solvent to warm to ambient

temperature

Warning

Dry ice causes burns!

Ensure that suitable protective clothing 

(eye protection, insulated gloves and apron) is used during filling 

or emptying. 

!

Page 13

Содержание GreenHouse

Страница 1: ...down Parallel Evaporation System Your Local Distributor February 2023 Issue 5 Radleys Shire Hill Saffron Walden Essex CB11 3AZ United Kingdom Tel 44 0 1799 513320 Fax 44 0 1799 513283 Email sales radl...

Страница 2: ...6 Set up Operation Page 7 Set up Operation continued Page 8 Set up Operation continued Page 9 Set up Operation continued Page 10 Temperature Control Page 11 Example Evaporation Times Examples of Blow...

Страница 3: ...rays GreenHouse Blowdown Evaporator System is ideal for the evaporation of HPLC fractions in vials or micro titer plates Digitally controlled heating from a standard Carousel or IKA stirring hotplate...

Страница 4: ...ing blowdown ALWAYS ENSURE that inert gas flow rate is within recommended limits Page 3 Warning Applies when there is a possibility of personal injury Important Note Alerts the user to important facts...

Страница 5: ...9684 Blowdown Condenser RR99688 Blowdown 150ml Reservoir RR99658 System 17 GreenHouse Blowdown Complete Upgrade Comprising of the following RR99670 GreenHouse Blowdown Head RR99672 Long Blowdown Pin P...

Страница 6: ...wdown Condenser RR99688 Blowdown 150ml Reservoir RR99691 AT01 Vial Rack 4 x 2 For 27 8mm OD Vials RR99692 AT02 Vial Rack 6 x 4 For 13mm OD Vials RR99693 AT03 Vial Rack 6 x 4 For 13 8mm OD Vials RR9969...

Страница 7: ...ing giving them superior chemical resistance to most solvents and acids when compared with unplated aluminium or stainless steel They also contain Hastelloy springs and use a Kalrez fluoropolymer seal...

Страница 8: ...can damage the threads Important Important Important Important Important Important Important Important Important Important Important Important Important Important Important Note Allow the Reaction Blo...

Страница 9: ...tightening may damage the thread Do not use a spanner or wrench to tighten sealing knobs Important Important Important Important Important Important Important Important Important Important Important...

Страница 10: ...reduced for thermally less stable compounds See page 13 for important information on pressure control Important Note If the tubes are more than half full use a slower flow rate increasing the flow rat...

Страница 11: ...re to the desired level by following the instructions of RR98073 Fuzzy Logic Digital Temperature Controller The set temperature can be maintained to 0 5 C The maximum recommended operating temperature...

Страница 12: ...ad Standard GreenHouse Base and GreenHouse Reaction Block GreenHouse with Blowdown Head Standard GreenHouse Base Base Adapter and 24 Position Vial Rack GreenHouse with Blowdown Head Standard GreenHous...

Страница 13: ...Important Important Important Important Important Important Important Important Important Important Important Important Important AT01 AT05 AT06 AT03 AT02 Base Adapter with 8 position vial rack Base...

Страница 14: ...portant Warning The Blowdown Head Safety Pressure Relief Valve and Gas Inlet Safety Pressure Relief Valve are designed to vent at nominally 4 to 6psi Therefore under normal and correct operation proce...

Страница 15: ...with Silicone Rubber It is also more resistant to aromatic hydrocarbons Viton exhibits relatively good resistance to trifluoroacetic acid TFA and is the preferred gasket in this case Thermal Resistan...

Страница 16: ......

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