Quantum turret 6/FO Скачать руководство пользователя страница 9

9

 

 

 

Set

 

Position:

 

To

 

rotate

 

the

 

turret

 

6,

 

use

 

the

 

up

 

and

 

down

 

arrows

 

to

 

choose

 

the

 

new

 

position

 

and

 

press

 

SET

.

  

The

 

controller

 

will

 

return

 

to

 

the

 

Display

 

page.

 

 

 

Set

 

Temperature:

 

To

 

set

 

the

 

Target

 

temperature,

 

use

 

the

 

up

 

and

 

down

 

arrows.

  

Press

 

SET

 

to

 

retain

 

this

 

new

 

Target

 

and

 

initiate

 

temperature

 

control.

 

 

 

Set

 

Stirring:

 

To

 

turn

 

on

 

magnetic

 

stirring,

 

use

 

the

 

up

 

and

 

down

 

arrows

 

to

 

choose

 

an

 

approximate

 

stirring

 

speed

 

between

 

1

 

and

 

2500

 

rpm.

  

Press

 

SET

 

to

 

turn

 

on

 

stirring

 

at

 

this

 

speed.

 

 

 

Set

 

Ramping

:

 

To

 

perform

 

a

 

ramp,

 

set

 

the

 

Ramping

 

rate

 

using

 

the

 

up

 

and

 

down

 

arrows,

 

and

 

press

 

SET

.

  

With

 

ramping

 

set,

 

turning

 

on

 

temperature

 

control

 

will

 

generate

 

a

 

linear

 

ramp

 

to

 

the

 

target

 

temperature.

  

When

 

the

 

sample

 

holder

 

reaches

 

the

 

target

 

temperature,

 

the

 

ramp

 

rate

 

will

 

be

 

set

 

back

 

to

 

0°/minute.

 

The

 

fastest

 

possible

 

ramp

 

is

 

determined

 

by

 

how

 

fast

 

the

 

cuvette

 

holder

 

could

 

reach

 

the

 

target

 

temperature

 

without

 

ramping.

  

If

 

you

 

attempt

 

to

 

ramp

 

too

 

quickly,

 

especially

 

at

 

high

 

and

 

low

 

temperature

 

extremes,

 

you

 

will

 

obtain

 

a

 

nonlinear

 

ramp.

  

The

 

slowest

 

ramp

 

that

 

may

 

be

 

set

 

on

 

this

 

page

 

is

 

0.01

 

°C/minute.

  

(If

 

needed,

 

much

 

slower

 

ramps

 

may

 

be

 

set

 

through

 

software

 

commands.)

 

Set Ramping 
 
Ramp = 0.55 °/min 
Current = 0 °/min 

Set Stirring 
  
Stir Speed = 1200rpm 
Current = 0rpm 

Set Temperature 
  
Target =  37.0 °C 
Current=  20.0 °C 

Set Position 
  
Position = 5 
Current Position = 1 

Содержание turret 6/FO

Страница 1: ...99019 8606 Tel 509 624 9290 Fax 509 624 9488 E mail quantum qnw com Web www qnw com turret 6 FO 6 Position Temperature Controlled Cuvette Turret for Fiber Optic Spectroscopy Manual Product Overview t...

Страница 2: ...the turret 6 10 A General Description 10 B Cuvettes 11 C Cuvette z Height 11 D Cooling Water for the Peltier 11 E Dry Gas Purging 12 F External Temperature Probe 12 G External Computer Control 12 H De...

Страница 3: ...le 5 USB cable 6 turret 6 accessory kit slits wrench blanks and 6 magnetic stir bars 7 vinyl tubing to connect water and gas Depending on Your Order Your Shipment May Contain Lens Systems 1 two t6 QCL...

Страница 4: ...ure that water is flowing back into the bucket Check for leaks 4 If you plan to work at low temperatures connect a source of dry gas typically nitrogen to release on the cuvette windows Attach a lengt...

Страница 5: ...osition 2 The collimating optics produce a 5 mm diameter beam that passes through the cuvette centered at 8 5 mm above the outside bottom surface Attach fiber optics as describe below Typically light...

Страница 6: ...3 to reflect the excitation source back on itself Figure 3 Components of a lens assembly 1 Use the 5 64 inch hex screwdriver from the turret 6 accessory kit to loosen the set screw Figure 3 2 Remove t...

Страница 7: ...urret 6 insert the CD into the drive If the installation does not start automatically locate the SETUP exe file in the root directory and run it The installation process starts with a small black wind...

Страница 8: ...Start page is being displayed press SET to turn off temperature control 7 After measurements are completed turn off power on the back of the TC 1 controller and turn off the water source F Using the M...

Страница 9: ...and press SET With ramping set turning on temperature control will generate a linear ramp to the target temperature When the sample holder reaches the target temperature the ramp rate will be set back...

Страница 10: ...tte to drive rotating magnet Dry gas enters a 1 16 inch hose barb on the front of the instrument and is carried through a manifold in the floor of the turret to small holes on the bottom of the 18 cuv...

Страница 11: ...ng it is particularly important to transfer this heat away from the Peltier This is accomplished with flowing water through the heat exchanger A source of water or other cooling fluid must be connecte...

Страница 12: ...pt the plug on a standard Series 400 or Series 500 thermistor probe When a probe is plugged into the jack the probe temperature is presented on the display of the TC 1 Place the probe in a sample to m...

Страница 13: ...he source fiber into the middle of the cuvette with a magnification of 2 7 The emission lens t6 QIL em focuses a small region of the illuminated volume in the center of the cuvette onto the end of the...

Страница 14: ...out of range warnings loose cable check cable The temperature controller is not receiving reasonable responses from either the cell tower or heat exchanger sensors Since it is very unlikely for both...

Страница 15: ...ature range 20 to 110 C temperature precision 0 02 C cuvette size outside dimensions 12 5 x 12 5 mm minimum cuvette height 30 mm cuvette z height 15 mm optical port dimensions 12 mm high x 10 mm wide...

Страница 16: ...rom the set temperature of temperature readings returned from the temperature controlled turret 6 for set temperatures between 15 C and 110 C Thus it is a measure of the ability of the cuvette holder...

Страница 17: ...reproducibility is a measure of the ability of the temperature to return to an original value See Figure 1 It accounts for differences depending on the direction of temperature change and differences...

Страница 18: ...hown the time required to get within 1 C the time to get within the lock on temperature of 0 05 C from the target and the final time indicating that the TC 1 indicates the temperature is stable Temper...

Страница 19: ...e controller In this case the controller includes electronics which convert the USB connection to a serial communications port However for the port to be available to programs on the computer it will...

Страница 20: ...and set it to the most recent non zero stirrer speed setting F1 SS Turn stirrer off F1 SS What is the current stirrer speed setting F1 SS 1000 Stirrer speed setting is 1000 rpm 4 Temperature Control...

Страница 21: ...22 84 The current temperature is 22 84 C F1 CT 3 Periodically report current temperature every 3 seconds F1 CT Stop periodic current temperature reports 8 Error Reporting F1 ER Report the current erro...

Страница 22: ...re is 30 5 degrees F1 PA Stop automatic reporting of probe temperature every temperature increment F1 PX Change probe temperature returned to a precision of 0 01 degree 10 Temperature Ramping F1 RR S...

Страница 23: ...anger Temperature F1 HL What is the high temperature limit for the heat exchanger F1 HT 60 The heat exchanger high temperature limit is 60 C F1 HT What is the current temperature of the heat exchanger...

Страница 24: ...een made The commands in this section are intended to allow the program to prevent the TC 1 from sending those automatic reports F1 XX R Stop R or start R reporting all manual changes including those...

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