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Quantum turret 6/FO, Руководство и обзор продукта

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7

 

 

5.

 

Now,

 

unscrew

 

the

 

silver

 

sleeve

 

from

 

the

 

black

 

end

 

piece

 

revealing

 

the

 

SMA

 

connector

  

(Figure

 

4).

 

6.

 

Slide

 

the

 

silver

 

sleeve

 

over

 

the

 

end

 

of

 

the

 

fiber

 

optic

 

connector

 

and

 

cable,

 

leaving

 

the

 

threaded

 

end

 

toward

 

the

 

end

 

of

 

the

 

cable.

 

7.

 

Attach

 

the

 

fiber

 

optic

 

cable

 

to

 

the

 

SMA

 

connector.

 

8.

 

Holding

 

the

 

black

 

end

 

piece,

 

screw

 

the

 

silver

 

sleeve

 

back

 

into

 

place.

 

9.

 

Insert

 

the

 

SMA

 

connector

 

and

 

silver

 

sleeve

 

into

 

the

 

hole

 

in

 

the

 

optical

 

assembly.

  

For

 

a

 

first

 

adjustment,

 

insert

 

the

 

assembly

 

until

 

the

 

alignment

 

groove

 

is

 

even

 

with

 

the

 

face

 

of

 

the

 

lens

 

assembly.

  

Later,

 

you

 

can

 

optimize

 

the

 

signal

 

intensity

 

by

 

sliding

 

the

 

SMA

 

connector

 

and

 

silver

 

sleeve

 

in

 

deeper.

 

 

D.

  

Software

 

Installation

 

NOTE:

 

IF

 

YOU

 

PURCHASED

 

THE

 

T

‐

App

 

PROGRAM,

 

DO

 

NOT

 

PLUG

 

IN

 

THE

 

USB

 

CABLE

 

UNTIL

 

THE

 

SOFTWARE

 

IS

 

LOADED!

  

IF

 

YOU

 

DO,

 

WINDOWS

 

MAY

 

AUTOMATICALLY

 

INSTALL

 

AN

 

INCORRECT

 

DRIVER

 

THAT

 

WILL

 

BE

 

DIFFICULT

 

TO

 

REMOVE.

 

 

1.

 

If

 

you

 

purchased

 

the

 

T

‐

App

 

program

 

for

 

external

 

control

 

of

 

the

 

turret 

6

,

 

insert

 

the

 

CD

 

into

 

the

 

drive.

  

If

 

the

 

installation

 

does

 

not

 

start

 

automatically,

 

locate

 

the

 

SETUP.exe

 

file

 

in

 

the

 

root

 

directory

 

and

 

run

 

it.

  

The

 

installation

 

process

 

starts

 

with

 

a

 

small

 

black

 

window

 

that

 

is

 

shown

 

during

 

installation

 

of

 

the

 

drivers

 

needed

 

to

 

control

 

the

 

turret 

6

 

through

 

a

 

USB

 

connection.

  

This

 

window

 

will

 

then

 

be

 

replaced

 

by

 

the

 

software

 

installation

 

window.

  

Follow

 

the

 

onscreen

 

prompts

 

to

 

complete

 

the

 

installation.

 

 

2.

 

Connect

 

the

 

turret 

6

 

to

 

your

 

computer

 

using

 

the

 

USB

 

cable

 

provided.

  

The

 

New

 

Hardware

 

installation

 

process

 

will

 

begin

 

automatically

 

and

 

take

 

a

 

few

 

moments

 

to

 

finish.

 

E.

  

System

 

Operation

 

1.

 

Use

 

liquid

 

samples

 

in

 

standard

 

1

 

x

 

1

‐

cm

 

square

 

cuvettes

 

and

 

place

 

the

 

cuvettes

 

in

 

the

 

turret 

6

.

 

2.

 

Place

 

a

 

magnetic

 

stir

 

bar

 

in

 

each

 

cuvette.

 

3.

 

If

 

you

 

wish

 

to

 

monitor

 

the

 

temperature

 

inside

 

a

 

cuvette,

 

plug

 

a

 

standard

 

Series

 

400

 

or

 

Series

 

500

 

thermistor

 

probe

 

(not

 

provided)

 

into

 

the

 

¼

 ‐ 

inch

 

phone

 

jack

 

labeled

 

“probe”

 

in

 

the

 

back

 

panel

 

of

 

the

 

TC

 

1

.

  

Place

 

the

 

end

 

of

 

the

 

probe

 

in

 

a

 

region

 

of

 

the

 

solution,

 

where

 

it

 

will

 

not

 

occlude

 

the

 

spectrometer

 

light

 

beam.

 

4.

 

Turn

 

on

 

the

 

TC

 

1

 

controller

 

using

 

the

 

switch

 

on

 

the

 

back

 

panel.

 

 

 

Содержание turret 6/FO

Страница 1: ...99019 8606 Tel 509 624 9290 Fax 509 624 9488 E mail quantum qnw com Web www qnw com turret 6 FO 6 Position Temperature Controlled Cuvette Turret for Fiber Optic Spectroscopy Manual Product Overview t...

Страница 2: ...the turret 6 10 A General Description 10 B Cuvettes 11 C Cuvette z Height 11 D Cooling Water for the Peltier 11 E Dry Gas Purging 12 F External Temperature Probe 12 G External Computer Control 12 H De...

Страница 3: ...le 5 USB cable 6 turret 6 accessory kit slits wrench blanks and 6 magnetic stir bars 7 vinyl tubing to connect water and gas Depending on Your Order Your Shipment May Contain Lens Systems 1 two t6 QCL...

Страница 4: ...ure that water is flowing back into the bucket Check for leaks 4 If you plan to work at low temperatures connect a source of dry gas typically nitrogen to release on the cuvette windows Attach a lengt...

Страница 5: ...osition 2 The collimating optics produce a 5 mm diameter beam that passes through the cuvette centered at 8 5 mm above the outside bottom surface Attach fiber optics as describe below Typically light...

Страница 6: ...3 to reflect the excitation source back on itself Figure 3 Components of a lens assembly 1 Use the 5 64 inch hex screwdriver from the turret 6 accessory kit to loosen the set screw Figure 3 2 Remove t...

Страница 7: ...urret 6 insert the CD into the drive If the installation does not start automatically locate the SETUP exe file in the root directory and run it The installation process starts with a small black wind...

Страница 8: ...Start page is being displayed press SET to turn off temperature control 7 After measurements are completed turn off power on the back of the TC 1 controller and turn off the water source F Using the M...

Страница 9: ...and press SET With ramping set turning on temperature control will generate a linear ramp to the target temperature When the sample holder reaches the target temperature the ramp rate will be set back...

Страница 10: ...tte to drive rotating magnet Dry gas enters a 1 16 inch hose barb on the front of the instrument and is carried through a manifold in the floor of the turret to small holes on the bottom of the 18 cuv...

Страница 11: ...ng it is particularly important to transfer this heat away from the Peltier This is accomplished with flowing water through the heat exchanger A source of water or other cooling fluid must be connecte...

Страница 12: ...pt the plug on a standard Series 400 or Series 500 thermistor probe When a probe is plugged into the jack the probe temperature is presented on the display of the TC 1 Place the probe in a sample to m...

Страница 13: ...he source fiber into the middle of the cuvette with a magnification of 2 7 The emission lens t6 QIL em focuses a small region of the illuminated volume in the center of the cuvette onto the end of the...

Страница 14: ...out of range warnings loose cable check cable The temperature controller is not receiving reasonable responses from either the cell tower or heat exchanger sensors Since it is very unlikely for both...

Страница 15: ...ature range 20 to 110 C temperature precision 0 02 C cuvette size outside dimensions 12 5 x 12 5 mm minimum cuvette height 30 mm cuvette z height 15 mm optical port dimensions 12 mm high x 10 mm wide...

Страница 16: ...rom the set temperature of temperature readings returned from the temperature controlled turret 6 for set temperatures between 15 C and 110 C Thus it is a measure of the ability of the cuvette holder...

Страница 17: ...reproducibility is a measure of the ability of the temperature to return to an original value See Figure 1 It accounts for differences depending on the direction of temperature change and differences...

Страница 18: ...hown the time required to get within 1 C the time to get within the lock on temperature of 0 05 C from the target and the final time indicating that the TC 1 indicates the temperature is stable Temper...

Страница 19: ...e controller In this case the controller includes electronics which convert the USB connection to a serial communications port However for the port to be available to programs on the computer it will...

Страница 20: ...and set it to the most recent non zero stirrer speed setting F1 SS Turn stirrer off F1 SS What is the current stirrer speed setting F1 SS 1000 Stirrer speed setting is 1000 rpm 4 Temperature Control...

Страница 21: ...22 84 The current temperature is 22 84 C F1 CT 3 Periodically report current temperature every 3 seconds F1 CT Stop periodic current temperature reports 8 Error Reporting F1 ER Report the current erro...

Страница 22: ...re is 30 5 degrees F1 PA Stop automatic reporting of probe temperature every temperature increment F1 PX Change probe temperature returned to a precision of 0 01 degree 10 Temperature Ramping F1 RR S...

Страница 23: ...anger Temperature F1 HL What is the high temperature limit for the heat exchanger F1 HT 60 The heat exchanger high temperature limit is 60 C F1 HT What is the current temperature of the heat exchanger...

Страница 24: ...een made The commands in this section are intended to allow the program to prevent the TC 1 from sending those automatic reports F1 XX R Stop R or start R reporting all manual changes including those...

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