PerkinElmer DSC 4000, Инструкция по установке и эксплуатации оборудования

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Contents
Introduction ............................................................................................... 5
Pyris Installation ............................................................................................... 6
Safety and Regulatory Information ........................................................... 7
Symbols Used in Online Help ............................................................................. 8
Symbols Used on the Instruments ...................................................................... 8
Electrical Warnings ...........................................................................................12
Electromagnetic Compatibility (EMC) .................................................................14
Electrical Safety ...............................................................................................15
WEEE Instructions for PerkinElmer Products ......................................................16
Prepare the Laboratory ............................................................................ 18
Prepare the Laboratory .....................................................................................19
Electrical Requirements ..............................................................................19
Environmental Requirements ......................................................................19
Purge Gas and Pneumatic Supply ...............................................................20
Space Requirements ..................................................................................20
Install Multiple Analyzers ........................................................................ 23
Install Multiple Analyzers ..................................................................................24
Install a DSC 4000 ................................................................................... 27
Safety Precautions for the DSC 4000 .................................................................28
DSC 4000 Warning Labels .................................................................................32
Warning Labels on the Upper Ring Around the Furnace................................32
Warning Labels on the Back of the DSC 4000 ..............................................34
Install a DSC 4000 ...........................................................................................36
Unpacking the DSC 4000 ..................................................................................37
Set Up the DSC 4000 System Components .........................................................39
Select the Correct Voltage for the DSC 4000 ...............................................39
Connect the Purge Gas Supply to the DSC 4000 ..........................................41
Connect the Purge Gas and System Purge Gas Lines to the DSC 4000 ..........41
Connect the Cooling Device to the DSC 4000...............................................42
Connect the DSC 4000 System Components ......................................................47
Configure the DSC 4000 ...................................................................................48
Starting the Pyris Manager .........................................................................49
Calibrate the DSC 4000.....................................................................................50
DSC 4000 Hardware ................................................................................. 53
DSC 4000 ........................................................................................................54
Furnace and Sensor Design ........................................................................54
Cooling .....................................................................................................55
Calibration of the DSC 4000 ..............................................................................56
Temperature Calibration ............................................................................56
Perform Indium and Zinc Runs ...................................................................57
Perform a Peak Area with Onset Calculation ................................................57
Performing a Temperature Calibration.........................................................58
Heat Flow Calibration .................................................................................58
Operating Variables and Sample Handling ..........................................................60
Temperature Range ...................................................................................60
Scanning Rate ...........................................................................................60
Subambient Operation of the DSC 4000 .............................................................61
DSC 4000 Maintenance .....................................................................................62
DSC 4000 Part Numbers ...................................................................................63
Miscellaneous Part Numbers .......................................................................64