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FreeZone

Benchto

Freeze Dryers

User's Manual

Please read the User’s Manual before operating the equipment.

LABCONCO CORPORATION

8811 Prospect Avenue
Kansas City, MO 64132
(800) 821-5525, (816) 333-8811
(816) 363-0130 fax
labconco@

labconco.com

Models

70020**** 2.5L -50°C Series

71020**** 2.5L -84°C Series

70040**** 4.5L -50°C Series

71040**** 4.5L -84°C Series

72040**** 4.5L -105°C Series

70080**** 8L -50°C Series

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Содержание FreeZone 70020 Series

Страница 1: ...enue Kansas City MO 64132 800 821 5525 816 333 8811 816 363 0130 fax labconco labconco com Models 70020 2 5L 50 C Series 71020 2 5L 84 C Series 70040 4 5L 50 C Series 71040 4 5L 84 C Series 72040 4 5L...

Страница 2: ...the hours of 7 30 a m and 5 30 p m Central Standard Time Part 7343000 Rev A ECO K623 Warranty Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and...

Страница 3: ...7 CHAPTER 3 GETTING STARTED 8 Unpacking Your Freeze Dryer 8 Freeze Dryer Components 9 Setting Up Your Freeze Dryer 9 Component Identification 10 Vacuum Pump Connection 11 Electrical Connection 12 Baf...

Страница 4: ...Detection screen 33 Help screen 34 Diagnostics 34 User s Manual 35 About 35 CHAPTER 5 USING YOUR FREEZE DRYER 36 Operation Checklist 36 Vacuum Pump Ballast Setting 37 Operating the Freeze Dryer 37 Aut...

Страница 5: ...ts Collector Chamber Isolation 50 Refrigeration Module Operation 52 APPENDIX A FREEZE DRYER COMPONENTS 53 APPENDIX B FREEZE DRYER DIMENSIONS 60 APPENDIX C FREEZE DRYER SPECIFICATIONS 63 Electrical Spe...

Страница 6: ...nsitive Other than food processing e g coffee whole dinners freeze drying has been extensively used in the development of pharmaceuticals e g antibiotics and preservation of biologicals e g proteins p...

Страница 7: ...s is based on the fact that the heat of sublimation is usually absorbed on one side of the frozen sample and must travel through the frozen layer to vaporize water at the other surface In addition as...

Страница 8: ...reeze dry system With any given instrument the capacity is based on the surface area of the sample the eutectic temperature and concentration of the sample and the rate and amount of heat transferred...

Страница 9: ...ntenance and making minor modifications to your Freeze Dryer are also included Chapter 1 Introduction provides a brief overview of the Freeze Dryer explains the organization of the manual and defines...

Страница 10: ...apter and section titles are shown in italic type e g Chapter 3 Getting Started Steps required to perform a task are presented in a numbered format Comments located in the margins provide suggestions...

Страница 11: ...fully read this chapter to learn Electrical supply requirements Vacuum pump requirements Refer to Appendix C Freeze Dryer Specifications for complete Freeze Dryer electrical and environmental conditio...

Страница 12: ...yer The space for benchtop models must be large enough to accommodate the vacuum pump which will be used with the Freeze Dryer Vacuum Pump Requirements A vacuum pump must be provided by the user A vac...

Страница 13: ...Dryers weigh between 82 142 lbs 37 64 kg depending on the model If you must lift the Freeze Dryer manually use at least two 2 persons and follow safe lifting guidelines Unpacking Your Freeze Dryer Car...

Страница 14: ...ollector Chamber Lid Assembly o Acrylic Lid Assembly for 50C models o Stainless Steel Lid Assembly for 84C 105C models 2 5L 4 5L 8L Part Description Comments 1 1 1 1089005 User s Manual USB Flash Driv...

Страница 15: ...Identification USB Port Quick Connect drain fitting Power Inlet Vacuum Pump Outlet Quick Connect drain coupling Circuit Breaker Reset Vacuum Connection Port Drying Accessory End Point Detection Ethern...

Страница 16: ...ective caps from inlet and outlet ports 3 Some vacuum pumps have inlet fittings that clamp to the pump Place the centering ring with filter screen on the inlet fitting 4 Place the hose barb fitting on...

Страница 17: ...RETURN KIT CAN ALSO BE USED IN CONJUNCTION WITH THE EXHAUST FILTER TO RETURN TRAPPED OIL BACK TO THE VACUUM PUMP Electrical Connection Make sure that the outlet that you intend to use meets the volta...

Страница 18: ...ng manifold purchased separately may be positioned directly above the 3 inch hole in the collector chamber lid 12 or 16 Port Drying Chamber Installation on Acrylic Stainless Steel Lids GASKET STAINLES...

Страница 19: ...eeze Dryer Components The FreeZone Freeze Dry System is designed to be chemically resistant to most compounds that are commonly used in freeze drying processes However by necessity the freeze dryer is...

Страница 20: ...lowed to enter the vacuum pump will degrade the oil and cause damage to the vacuum pump Sugars and proteins typically will have minimal negative effect on any of the materials of construction When usi...

Страница 21: ...cautions Solvents used in the Freeze Dryer may be flammable or hazardous to your health Use extreme caution and keep sources of ignition away from the solvents When using flammable or hazardous solven...

Страница 22: ...in Chapter 3 Getting Started read this chapter to learn how to Operate the controls Understand the display Do not use the Freeze Dryer in a manner not specified by the manufacturer refer to Appendix...

Страница 23: ...ressing this button will illuminate the display Note the display can also be brought out of low power mode by touching any location on the screen 3 On Standby LED Indicator Blue LED indicator light to...

Страница 24: ...ing 4 Settings 5 Sensors 6 Drying Accessory 7 End Point Detection 8 Help Moving between Menu Screens You can move between menu screens by either touching the menu icons or swiping across the screen fr...

Страница 25: ...l read High if the vacuum level is 5 mbar If the vacuum level is 5 mbar a numerical value will be displayed The value displayed will be RED if the vacuum is 1 500 mbar The value displayed will be GREE...

Страница 26: ...ump ON OFF or change the vacuum set point value Programs Screen There are two accessories Tray Dryer Heated Product Shelves that will run programs when connected to a Benchtop Freeze Dryer The Program...

Страница 27: ...EZE DRYER THE START BUTTON WILL BE INACTIVE Edit View Use this button to Edit or View the parameters of a saved program Copy Use this button to Copy a selected program The default name will be Copy of...

Страница 28: ...ton is pressed Pressing the Back button will return to the Programs screen without saving changes Shelf Temp May be set anywhere from 40 C to 40 C in 1 C increments There is also a Max Cold MC setting...

Страница 29: ...a data log file is currently running The new data log file name will be defaulted to a three digit sequential number starting with Batch 001 that will be incremented as new data log files are added t...

Страница 30: ...ation integer value between 12 12 NTP server Enter the web address URL of the NTP server of your choice that will provide clock synchronization data to the Freeze Dryer via the Ethernet connection Day...

Страница 31: ...ail Alerts Calibration Network Users will be required to enter the security code to gain access to each individual screen that has been selected box checked 5 Alerts If a valid network connection has...

Страница 32: ...ld Configure Email Settings Pressing this button will bring up the following screen where the appropriate email settings can be entered If you do not know the proper information to enter into each of...

Страница 33: ...lert Scroll list up or down by swiping screen up or down Alerts for the Freeze Dryer will be at the top of the list Alerts for attached accessories Tray Dryer or Heated Product Shelves will appear at...

Страница 34: ...certainty An external reference sensor must be placed at the same measurement point as close as physically possible as the sensor being calibrated The Collector temperature sensor has its own referenc...

Страница 35: ...adjusted reading uncorrected Offset is the value that will be presented on all screens outside of the Sensor Calibration screen Pressing the Offset field of the desired sensor will bring up a dialog b...

Страница 36: ...ode sleep when no screen touches have been detected for the allotted set time Screen Timeout Pressing the Screen Timeout Function button will toggle between ON OFF Screen Timeout This value can be set...

Страница 37: ...single page The Sensors screen is for viewing only there are no selectable fields on this screen Drying Accessory Screen If an electrically controlled Drying Accessory is NOT connected to the Freeze...

Страница 38: ...e program name Step and Time Remaining TR in the current Step will be displayed in this location The right side of the status box will indicate if Data Logging is currently ON or OFF PROGRAM Pressing...

Страница 39: ...int Detection alert is achieved for any given flask Offset from Ref Vacuum This allows the user to determine the level of dryness at which the system will declare that the primary drying end point has...

Страница 40: ...Frequency and allow the user to run Manual or Auto Diagnostics on the unit User s Manual Allows the user to view the table of contents and browse individual sections of the manual While in the user s...

Страница 41: ...n coupling located on the left hand side of the Freeze Dryer Note Freeze Dryer Collector or Vacuum will not start if moisture is detected in the drain line 4 After completely draining the system disco...

Страница 42: ...the pump to fail Operating the Freeze Dryer Auto start up 1 Go to Home screen 2 Press AUTO then press START COLLECTOR will start immediately VACUUM will start when collector temperature reaches 40 C...

Страница 43: ...Solidification Eutectic Temperature Pre Freeze Temperatures Vacuum Set Point Bacteria Virus 40 C 50 C 0 04 mbar Milk 5 to 13 15 to 23 1 65 to 0 77 Fungi 40 50 0 04 Vegetable Tissue 25 to 50 35 to 60 0...

Страница 44: ...on of valves and sample sizes may be utilized at one time provided that the system vacuum and collector temperature remain sufficiently low to prevent melting of the frozen sample 3 When all the frost...

Страница 45: ...ensate accumulates on the collector coil to obstruct the flow of vapor to the collector chamber the Freeze Dryer should be defrosted Go to Home screen press VACUUM then STOP to turn the vacuum pump OF...

Страница 46: ...message box and audible alarm can be dismissed by pressing the Back button on the alert message box The following conditions will initiate an alert Power Fail If a power failure occurs during a Freez...

Страница 47: ...eze Dryer has accumulated a total of 1000 operating hours an alert will be activated It may be necessary to service the vacuum pump more frequently than every 1000 hours depending on the operation of...

Страница 48: ...roduct Shelves accessory is connected to the Freeze Dryer this alert will be activated when the last step of a running program has been completed Copy export a Data Log File Data Log Files can be copi...

Страница 49: ...llowing webpage will appear with a list of all the Data Log files that are stored on the Freeze Dryer 7 Single click on a file name from the list to download the file 8 Single click on the downloaded...

Страница 50: ...place before resuming normal operation of the equipment Routine Maintenance Schedule Under normal operation the Freeze Dryer requires little maintenance The following maintenance schedule is recommen...

Страница 51: ...nds upon both their usage and the surrounding environment Check all rubber hoses and gaskets and replace any that show signs of hardening permanent set or deterioration 2 Using a soft cloth sponge or...

Страница 52: ...n of the vacuum pump to the Freeze Dryer If the vacuum pump has a power switch make sure that it is turned on Note If the vacuum pump is plugged directly into a wall outlet for troubleshooting purpose...

Страница 53: ...mind too much vacuum grease can actually cause leaks 3 Check the drain line and ensure that the quick connect drain fitting is disconnected from the quick connect drain coupling on the left side of th...

Страница 54: ...talls on a chamber and a manifold Thrust Washer Valve Body Knob Stem Assembly Valve Body Trim Ring Manifold Assembly Knob Stem Assembly Bulkhead Nut Gasket No grease required Bulkhead Fitting Valve Bo...

Страница 55: ...ld 1 Remove the drying chamber or manifold 2 Leave the gasket on and turn a large freeze dry flask upside down to cover the connection port 3 Start the Freeze Dryer and observe the vacuum indication I...

Страница 56: ...in the collector chamber If it is bad the problem is in the plumbing connections from the collector chamber to the vacuum pump 3 If the leak is in the plumbing connections check all rubber parts fitt...

Страница 57: ...nd apply vacuum grease to the O rings then reassemble and test Refrigeration Module Operation Under a no load condition the FreeZone Freeze Dry Systems can achieve a collector temperature of 50 C 84 C...

Страница 58: ...8 53 Original instructions APPENDIX A FREEZE DRYER COMPONENTS The following pages list components that are available for your Freeze Dryer The parts shown are the most common replacement parts If othe...

Страница 59: ...7337000 Lanyard Drain Fitting 14 X X 1889406 Machine Screw 8 32 x 3 8 long 15 X X 7429700 Moisture Sensor 16 X X 7373450 Vacuum Hose 17 X X 7403800 Filter Female Luer Lok 18 X X 7403700 Luer 10 32 Mal...

Страница 60: ...Appendix A Freeze Dryer Components Product Service 816 333 8811 or 1 800 522 7658 55 Original instructions 2 5L 50C Models 70020xxxx 2 5L 84C Models 71020xxxx 2 5L 50C Model Shown...

Страница 61: ...g Body 11 X X X 7335300 Drain Fitting Coupling Insert 3 8 Barb 12 X X X 7337100 Retaining Ring Drain Fitting 13 X X X 7337000 Lanyard Drain Fitting 14 X X X 1889406 Machine Screw 8 32 x 3 8 long 15 X...

Страница 62: ...endix A Freeze Dryer Components Product Service 816 333 8811 or 1 800 522 7658 57 Original instructions 4 5L 50C Models 70040xxxx 4 5L 84C Models 71040xxxx 4 5L 105C Models 72040xxxx 4 5L 84C Model Sh...

Страница 63: ...Retaining Ring Drain Fitting 13 X 7337000 Lanyard Drain Fitting 14 X 1889406 Machine Screw 8 32 x 3 8 long 15 X 7429700 Moisture Sensor 16 X 7373450 Vacuum Hose 17 X 7403800 Filter Female Luer Lok 18...

Страница 64: ...Appendix A Freeze Dryer Components Product Service 816 333 8811 or 1 800 522 7658 59 Original instructions 8L 50C Models 70080xxxx...

Страница 65: ...Product Service 1 800 522 7658 60 Original instructions APPENDIX B FREEZE DRYER DIMENSIONS 2 5L 50C Models 70020...

Страница 66: ...Appendix B Freeze Dryer Dimensions Product Service 816 333 8811 or 1 800 522 7658 61 Original instructions 2 5L 84C Models 71020 4 5L 50C Models 70040 Dimensions in inches centimeters...

Страница 67: ...pendix B Freeze Dryer Dimensions Product Service 816 333 8811 or 1 800 522 7658 62 Original instructions 4 5L 84C Models 71040 4 5L 105C Models 72040 8L 50C Models 70080 Dimensions in inches centimete...

Страница 68: ...ption Nominal Operating Range Hz Max with Vacuum Pump 70020xxxx 2 5L 50C 115V 103 127 60 14 230V 187 253 60 7 230V 198 253 50 7 71020xxxx 2 5L 84C 115V 103 127 60 16 230V 187 253 60 10 230V 198 253 50...

Страница 69: ...voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes on the AC input...

Страница 70: ...65 Original instructions APPENDIX D FREEZE DRYER ACCESSORIES Labconco offers a full line of accessories to enhance your Freeze Dryer s operation and usability For a complete list of these accessories...

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