K430X2 Dual Twin Foaming Characteristics Test Bath
Operation and Instruction Manual
K430X2-Manual
-
13-
5 Operation
5.1 Bath
Fill each bath with the appropriate heat transfer
fluid based upon the testing temperature. Fill the
bath with the medium from the top through one of
the seven port openings using a wide neck funnel
with a 500mL griffin beaker adding about ½ L at a
time to 2" (5 cm) from the top of the bath to allow
room for fluid expansion.
NOTE:
Do not attempt moving the
instrument when filled with fluid medium. Drain all
fluid before moving or relocating the instrument.
See section 7.2 of this document. Sudden starting
and stopping could result in hot bath fluid being
forcefully ejected from the bath. It could also result
in overbalancing and tipping over the instrument.
NOTE:
Do not drain the bath until the fluid is at
ambient temperature.
Testing
Temperature
Recommended Fluid
15 - 50°C*
Distilled water will be suitable.
50 - 95°C
Koehler
supplies
highly
refined white technical oil
(part # 355-001-001) that
contains an oxidation inhibitor
to limit clouding at higher
temperatures.
CAS# 8042-47-5
Minimum Flash Point: 120°C
(248°F)
Fire Point: 202°C (395°F)
95 - 150°C
Koehler supplies a clear
silicone heat transfer fluid
(part # 355-001-002) with high
oxidation resistance and low
volatility. CAS # 63148-62-9.
Minimum Flash Point: 200°C
(392°F).
NOTE:
Do not use bath fluids that will
decompose or volatilize producing flammable
vapors below the maximum instrument operating
tempe25°C.
NOTE:
Coloration of the Mineral or Silicon Bath
Oil is an indication that the Medium must be
changed. See Draining instructions in section 7.3
of this document. When a decision is made to
discard this material, dispose of this material and
its container to a hazardous of special waste
collection point. Country, State, or local laws may
impose additional regulatory requirements
regarding disposal. Dispose in accordance to all
applicable regulations.
WARNING:
Bath oils contaminated with
light ends can pose a flammability hazard.
5.2 Power
1. Turn on the main power switches to the unit.
WARNING:
Do
NOT
turn the power on
unless the bath is filled with the proper medium;
otherwise, damage may occur to the unit and the
warranty would be void.
2. The temperature controllers will illuminate and
display the actual and set point temperatures.
3. Set each bath temperature to desired test
temperatures as per ASTM D892 using the
operating instructions in section 4.4.
5.3 Preparation of Glassware and Tubing
1. Clean the graduated cylinders as per ASTM
D892 instructions and pour the test samples
into the cylinders to the recommended level as
per the aforementioned test methods.
2. Clean and flush the air delivery tube assembly
with diffuser stone as per ASTM D892.
3. Place the four 1000 ml test cylinders into the
tops & lock in place with the four clamps
provided on each top.
4. Proceed with the test and record the test
results in accordance to ASTM D892.
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