Koehler K41091 Скачать руководство пользователя страница 8

K41091 Micro Carbon Residue and Ash Tester 

Operation and Instruction Manual 

 

K41091-Manual

    

 

-

6-

 

1.  Gas Inlet Connections.

 For connection of Air 

and  Nitrogen  Gas  to  the  instrument  from  an 
external source.  

 

2.  Thermocouple  Port.

  For  connection  of 

Furnace Thermocouple.  

 

3.  Power  Outlet.

  For  connection  of  line  cord 

plug.  

4.  Fuse Port.

 Location for Fuse replacement.  

 

5.  Watchdog  Shutdown  Button.

  Turns  off 

microprocessor 

to 

perform 

maintenance 

procedures.  

 

6.  Parallel  Port.

  25  Pin  Type  Parallel  Port  for 

connection to a Printer.  

 

7.  Serial Line 1.

 For connection to external PC.  

 

8.  Serial Line 2.

 Not used in instrument.  

 

5  Operation 

 

5.1  Instrument Start-up 

 

WARNING:

 

An  apparatus  showing  traces  of  an 

impact  or  any  damage  following  shipping  or 
unpacking should not be operated.  
 

WARNING:

  The  apparatus  must  be  held  at  room 

temperature  for  several  hours  before  turning  on 
the  power  in  order  to  avoid  risks  caused  by 
condensation.  
 

NOTE:

  Give  detailed  attention  to  the  lid  and  the 

top  opening  of  the  furnace  for  condensation.  The 
lid ensures that the furnace is sealed.  
 

1. 

Depending on the desired use (carbon residue 
or ash), the apparatus must be connected to a 
source  of  nitrogen  providing  a  maximum 
pressure of 2.5 Bar (250 kPa) and possibly to 
a  source  of  air  at a  maximum  pressure  of  2.5 
Bar  (250  kPa).  In  order  to  keep  a  stable  flow 
during  testing,  the  gas  supply  will  have  to  be 
regulated  with  a  pressure  reducer  to  stabilize 
the pressure upstream.  

 

NOTE:

 During the first test of using the instrument, 

which  should  be  done  without  sample,  it  is 
essential  to  check  the  value  of  the  gas  flows  and 
to adjust them according to the pressure upstream 
of the gas.  
 

WARNING:

 

Do  not  connect  any  additional 

extension  to  either  the  chimney  or  the  supplied 

Chimney  Extension  Pipe  in  an  attempt  to  further 
evacuate  the  exhaust  fumes.

 

The  chimney  must 

remain  free  to  ensure  optimal  exhaust  of  the 
system.  Any  connection  on  the  chimney  or  its 
extension pipe would be likely to cause: 

-  Condensates in the piping of the apparatus 
-  A  backpressure  which  would  disturb  the  test 

by modifying the flows and cause leaks on the 
hot lid of the furnace.  

 

2. 

Connect  the  line  cord  to  properly  fused  and 
grounded  receptacles  with  the  correct  voltage 
as  indicated  in  section  1.3  and  to  the 
receptacle on the back of the unit.  

 

WARNING:

 

For each type  of test or method used 

the  apparatus  must  be  placed  under  a  hood  to 
properly  and  safely  evacuate  the  exhaust  fumes 
generated by the instrument.  
 

3. 

Number  designations  for  the  following  set  of 
directions refer to Figure 4 below: 
a.  If  necessary,  unbolt  the  Emergency  Stop 

Button 

(1) 

b.  Switch  on  the  apparatus,  by  using  the 

circuit breaker under Lift Door beneath the 
Numeric Keypad.  

c.  If  necessary,  switch  on  the  differential 

(2)

 

then switch on the circuit breaker 

(3) 

d.  Press  the  Power  Button  to  turn  on  the 

instrument 

(4) 

 

4. 

The  apparatus  will  begin  to  boot  and  the 
standby  display  screen  will  appear  after 
approximately 20 seconds.  

 

5. 

The  furnace  will  then  begin  heating  to  a 
standard  temperature  of  50°C.  The  furnace 
will  also  revert  back  to  this  temperature  in 
between  tests.  50°C  is  a  factory  preset  value 
and  can  be  adjusted  by  accessing  the 
Setpoint  Function  from  the  instruments  menu 
screen. See section 6.2.   

 

WARNING:

  If  the  apparatus  is  powered  off  for  a 

period  of  more  than  3  weeks,  the  accumulator  of 
the  microprocessor  board  is  discharged.  The 
instrument  will  completely  reset  including  its 
internal  date  and  time. In the  event  that  this  does 
occur,  it  is  necessary  to  reset  the  date  and  time 
using 

the 

maintenance 

function 

from 

the 

instrument  menu.  All  other  parameters  will  be 
saved in the “flashEprom” memory. In the event of 
the  microprocessor  discharge,  all  operation 
parameters will be saved.  
 

Содержание K41091

Страница 1: ... Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis Instrumentation Custom Design Manufacturing K41091 Micro Conradson Carbon Residue and Ash Tester ...

Страница 2: ......

Страница 3: ...scriptions Back 5 5 Operation 6 5 1 Instrument Start up 6 5 2 Starting a Test 7 5 3 Control Panel Operation 8 5 3 1 Creation of New Programs 8 5 3 2 Software Configuration Functions 9 5 3 3 Hardware Configuration Functions 10 6 Maintenance 11 6 1 Maintenance Checks 11 6 2 Routine Maintenance 11 6 2 1 Cleaning of Furnace Opening and Hot Lid 11 6 2 2 De Carbonizing the Furnace 11 6 2 3 Temperature C...

Страница 4: ...ehler for a full range of accurate and reliable instrumentation as well as support for your laboratory testing programs Please do not hesitate to contact us at any time with your inquiries about equipment tests or technical support Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 Email info koehlerinstrument com http www koehlerinstrument com 1 2 Recommended Resources and Pub...

Страница 5: ...ions The use of this equipment may involve hazardous materials and operations This manual does not purport to address all of the safety problems associated with the use of this equipment It is the responsibility of any user of this equipment to investigate research and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use Equipment...

Страница 6: ...artz sample vial re usable Ash Content Test K41000 5 16 ml Quartz sample vial re usable Ash Content Test K41000 8 4 ml Borosilicate glass sample tube MRC test 3 2 Unpacking Carefully unpack and place the instrument and accessories in a secure location Ensure that all items listed on the packing list are present Inspect the unit and all accessories for damage If any damage is found keep all packing...

Страница 7: ...rns off the power to the entire unit 4 Numeric Keypad For entering sample data and parameter values for testing 5 Key Function Buttons For navigation through the instruments sub menus Note The function of these buttons and subsequent display icons will change depending on the menu the user is in 6 Display For user friendly control of the instrument 7 Insulating Cover For enhanced temperature stabi...

Страница 8: ... an attempt to further evacuate the exhaust fumes The chimney must remain free to ensure optimal exhaust of the system Any connection on the chimney or its extension pipe would be likely to cause Condensates in the piping of the apparatus A backpressure which would disturb the test by modifying the flows and cause leaks on the hot lid of the furnace 2 Connect the line cord to properly fused and gr...

Страница 9: ...cting an External PC to Serial Line 1 and using the Data Acquisition Software provided with the accessories of the instrument NOTE The calculation of residue percentage can also be determined by the apparatus Inputting the initial and final weight of the samples into the software will then calculate the residue percentage automatically 5 2 Starting a Test WARNING For either program selected the In...

Страница 10: ...ntage ratio of residue remaining at the end of the test 13 Choose the desired program Micro Carbon Residue or Ash 14 Confirm the launching of the test by pressing Go once again on the display panel 15 The instrument will then sound a series of beeps The display will now indicate the temperature of the furnace the duration of the test the current segment of the test program running and the limiting...

Страница 11: ...e two 2 in the single digit place resulting in the desired value 7 Set Point Function This function allows the user to input the idle set point temperature of the furnace between tests This value is limited to the range from 20 to 80 C 8 Standby Function This function allows the user to shut down the apparatus via the control panel without having to switch off the circuit breaker or push the emerg...

Страница 12: ...rature of the furnace Either in degrees Celsius or Fahrenheit 3 Calibration Function This function allows the user to calibrate the furnace temperature probe 3 1 Physical Calibration This calibration is done by entering three 3 temperature points via the keyboard Enter these points by first replacing the furnace thermocouple with a temperature simulator To do this open remove the furnace thermocou...

Страница 13: ...e each test it is recommended to check the furnace exhaust The exhaust must be free from calamine If the apparatus has calamine deposits in the furnace exhaust it is recommended to remove the deposits using the cleaning cable provided 6 2 Routine Maintenance Depending on the frequency of use and the type of samples being tested it is recommended to perform routine maintenance procedures For exampl...

Страница 14: ...its Check the state of the chimney and chimney extension pipe for calamine deposits and clean in the same manner 6 2 3 Temperature Check of the Furnace To check the temperature of the furnace it is necessary for a control thermocouple to be in place In order to make this possible the hot lid has a small thermocouple port located along the outside If the actual temperature of the furnace does not c...

Страница 15: ...tension Pipe Gripping Hook Complete Furnace Furnace Thermocouple Safety Thermocouple Thermal Printer Paper for Thermal Printer Insulating Lid Small Vial Borosilicate Large Vial Borosilicate Long Vial Borosilicate Borosilicate Vial 12mm dia 72mm height Support for Porcelain Crucible Control Thermocouple w cable Furnace Thermocouple Calibration Cord Upstream Pressure Gauge Condensate Tank Joint for ...

Страница 16: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 14 7 Diagrams 7 1 Flow Meter Calibration Chart ...

Страница 17: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 15 7 2 Function Flow Chart ...

Страница 18: ...the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product is the repair or replacement of the product In no event shall the cost of the purchaser s remedy exceed the purchase price nor shall Koehler Instrument Company be liable for any special indirect incidental conse...

Страница 19: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 17 Notes ...

Страница 20: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 18 Notes ...

Отзывы: