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7

HI 4007

Remove protective cover from sensor tip.

Prepare HI 5315 reference electrode by filling electro-
lyte reservoir with HI 7072 fill solution.

Place sensor and reference electrodes into electrode
holder and connect cable connectors to meter.

HI 4107

Remove the protective plastic wrap that covers the
ceramic junction before assembling sensor for the first
time.

HI 7072 reference fill solution should be added daily
to electrolyte reservior before electrode use.

During measurement always operate electrode with
the fill hole open.

During normal use, fill solution will slowly drain out
of the tapered cone junction at the lower portion of the
electrode. Excessive loss (>4 cm drop within 24 hours)
is not normal. If this occurs verify cap is tightened and
the interface between the internal cone and outer
body is free of debris.

Add fill solution daily to maintain a good head pres-
sure. For optimum response, this level should be main-
tained and not be allowed to drop more than 2-3 cm
(1-inch) below fill hole. It must cover the ceramic
found on the inner stem.

If an erratic measurement occurs, check to see if for-
eign matter is seen trapped near the internal cone.
Drain and refill with fresh fill solution.

Avoid large changes in temperature (thermal shock)
as it may damage the sensor.

Содержание HI 4107

Страница 1: ...HI 4007 HI 4007 HI 4007 HI 4007 HI 4007 HI 4107 HI 4107 HI 4107 HI 4107 HI 4107 Chloride Ion Selective Electrode Instruction Manual CHLORIDE HI 4007 HI 410 COMBINATION 7 CHLORIDE Half cell Combinatio...

Страница 2: ...utions The HI 4007 is a solid state half cell sensor that requires a separate reference The HI 4107 is a combination ion selective electrode II II II II II Specifications Specifications Specifications...

Страница 3: ...asareferenceelectrode incorporated in its design The silver chloride pellet is prac tically insoluble in the test solutions being measured and producesapotentialchangeduetochangesinthesample s ion act...

Страница 4: ...4107 Design elements of the HI 4007 and HI 4107 Design elements of the HI 4007 and HI 4107 electrodes electrodes electrodes electrodes electrodes CHLORIDE HI 4007 Cap Sensing Membrane Sensor Handle U...

Страница 5: ...lutions Required Solutions Required for Chloride Measurements for Chloride Measurements for Chloride Measurements for Chloride Measurements for Chloride Measurements Select appropriate Hanna Instrumen...

Страница 6: ...libration standards and sample solutions should have the same ionic strength ISA acetate buffer or oxidizing reagent should be added to both samples and standards in the same ratio Calibration standar...

Страница 7: ...ing normal use fill solution will slowly drain out ofthetaperedconejunctionatthelowerportionofthe electrode Excessiveloss 4cmdropwithin24hours isnotnormal Ifthisoccursverifycapistightenedand the inter...

Страница 8: ...m seal found over ceramic junction on inner stem and discard This is only used for ship ping and long term storage 2 Rinseinnerstemwithdeionizedwatermakingcertain to wet the o ring found on the inner...

Страница 9: ...verify elec trodereturnstoitsoriginalposition Youmayneedto gently assist for this to occur 7 Tighten the electrode cap onto the body and fill elec trode body until fill solution volume is just below f...

Страница 10: ...action Corrective action Corrective action Corrective action Corrective action Verify protective cap has been removed HI 4007 Verify plastic film has been removed from inner stem HI4107 Verify electr...

Страница 11: ...he meter is calibrated with two or more freshly made stan dards that are in the linear measurement range of the unknowns Morecalibrationstandardsarerequiredinnon linear regions Unknowns are read direc...

Страница 12: ...ements using the oxidizing reagent must be made 10 minutes after mixing and not permitted react longer 3 Follow sectionVII GeneralGuidelinestooptimizetest set up 4 Duringcalibrationitisbesttostartwith...

Страница 13: ...mplifies the method greatly Example Chloride ion determination with known addition 1 A 50 mL sample of unknown Vsample is placed in a clean plastic beaker with a chloride sensor Add 2 mLofacetatepHbuf...

Страница 14: ...r See Section VI Titration Titration Titration Titration Titration XIV S XIV S XIV S XIV S XIV Storage and Care of the HI 4007 and torage and Care of the HI 4007 and torage and Care of the HI 4007 and...

Страница 15: ...s Conversion tables Conversion tables Conversion tables Conversion tables For Cl For Cl For Cl For Cl For Cl Multiply by Multiply by Multiply by Multiply by Multiply by Moles L M to ppm mg L 3 500x104...

Страница 16: ...6 monthsfromdateofpurchasewhenusedfortheirintended purpose and maintained according to instructions If they failtoworkwhenfirstusedcontactyourdealerimmediately Damageduetoaccidents misuse misapplicat...

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