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Due to shipping or storage the internal solution inside
the PVC modules may have developed an air pocket
near the membrane. Gently shaking the sensor down
(like the old style mercury thermometer) will place the
internal solution next to the membrane.

Presoaking the Calcium sensor in HI 4004-45
solution for at least half-hour before calibration will
help to optimize the sensor response.

 Do not leave your sensors in standard or samples

         with ISA  for long periods of time.

Calibration standards and sample solutions should
have the same ionic strength. ISA should be added to
both samples and standards.

Calibration standards and sample solutions should
be at same temperature.

Thermally insulate solution vessel from magnetic stir-
rer.

Calibration standards and sample solutions should
be stirred at the same rate using identical sized TFE
coated stir bars.

Rinse electrodes with distilled or deionized water be-
tween samples and gently dab dry with lab wipe or
other soft disposable absorbent toweling. Do not rub
the sensing surface.

Check for gas bubbles that may form near sensing
surface (due to solution temperature changes). Tap
off gently.

Avoid large changes in temperature (thermal shock)
as it may damage the sensor.

Note: The electrode membrane will develop a opaque
appearance when it becomes wetted. This is normal.

Содержание HI 4104

Страница 1: ...struction Manual SENSOR HANDLE HI 4000 50 HI 4004 HI 4004 HI 4004 HI 4004 HI 4004 HI 4104 HI 4104 HI 4104 HI 4104 HI 4104 Calcium Ion Selective Electrode Half cell Combination HI 4104 CALCIUM COMBINAT...

Страница 2: ...sensitive to calcium ions The HI 4004 is a half cell elec trode that requires a separate reference The HI 4104 is a combination ion selective electrode II II II II II Specifications Specifications Sp...

Страница 3: ...the sensor is impregnated with the organic ion exchanger Thisorganicionexchangerisconsideredacarrierionophore in that it is capable of shielding and carrying the charged calcium ion in it s polar cage...

Страница 4: ...Design elements of the HI 4004 and HI 4104 Design elements of the HI 4004 and HI 4104 electrodes electrodes electrodes electrodes electrodes Upper Cap Spring O Ring Ceramic Junction on Inner Stem Fil...

Страница 5: ...suitable mea surement vessel VI VI VI VI VI Solutions Required Solutions Required Solutions Required Solutions Required Solutions Required Standards for Calcium Measurements 0 1 M calcium standard 500...

Страница 6: ...ld be added to both samples and standards Calibration standards and sample solutions should be at same temperature Thermallyinsulatesolutionvesselfrommagneticstir rer Calibration standards and sample...

Страница 7: ...be maintained and not be allowed to drop more than 2 3 cm 1 inch below fill hole Do not use an electrode if crystallized salts are visible insidetheelectrode Drainelectrode disassembleand rinseintern...

Страница 8: ...nectors to meter 6 SoaktheCalciumelectrodesmembraneinHI4004 45 conditioning solution or a calcium standard 0 01M without ISA before calibration SENSOR HANDLE HI 4000 50 HI4104 The Hanna HI 4104 is shi...

Страница 9: ...into the outer body sliding spring down cable and screwing cap into place 6 Remove fill hole cover and o ring on fill hole spout Using the dropper pipette provided add a few drops HI 7082 fill solutio...

Страница 10: ...valent and connect BNC connector to meter IX IX IX IX IX Quick Check of Electrode Slope Quick Check of Electrode Slope Quick Check of Electrode Slope Quick Check of Electrode Slope Quick Check of Elec...

Страница 11: ...in plastic bottles If the reading is jumpy or unstable shake sensor down seesectionVII If the sensor slope just misses the suggested slope window soaking the sensor in a standard solution without ISA...

Страница 12: ...ines concentration of the unknown by a direct reading after calibrating the meter with the standards Add HI4004 00toadjustionicstrengthatadoseof2mLofper 100 mL sample or standard The meter is calibrat...

Страница 13: ...mix before taking measurements 3 FollowsectionVII GeneralGuidelinestooptimizetest set up 4 Duringcalibrationitisbesttostartwithlowerconcen trationsamplesfirst Waitforastablereadingbefore reading reco...

Страница 14: ...known addition 1 A 50 mL sample of unknown VSAMPLE is placed in a clean plastic beaker with an electrode s One mL of ISAisaddedtothesampleandpermittedtomix mV 1 is recorded 2 10mL VSTANDARD of 10 1 M...

Страница 15: ...ime periods For long term storage unscrew sensing mod ule from sensor handle and store dry in the shipping vial The model HI 4104 combination electrode can be left in HI 4004 45 for short time periods...

Страница 16: ...r 6 monthsfromdateofpurchasewhenusedfortheirintended purpose and maintained according to instructions If they failtoworkwhenfirstusedcontactyourdealerimmediately Damageduetoaccidents misuse misapplica...

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