background image

6.

Add new KCl crystals to the probe until there is approximately 0.5 cm (0.2 in.) of crystals above
the glass bulb. Refer to 

Figure 6

 on page 14.

7.

Fill the probe with new filling solution. Refer to 

Fill the probe

 on page 12.

8.5 Soak procedure for dry probes

If the glass bulb becomes dry, complete the steps that follow to hydrate the probe.

1.

Soak the probe tip in a warm pH 4 buffer solution for 2 hours.

2.

Rinse the probe with deionized water. Blot dry with a lint-free cloth.

3.

Calibrate the probe.

8.6 Storage

N O T I C E

 

Probes can become permanently damaged if kept in a storage solution that is not specified by the
manufacturer. Use only the specified storage solution (saturated KCl).

Do not store the probe in deionized water or in samples of low ionic strength. For short-term storage,
the probe can stay in the sample for a maximum of 2 hours if the sample pH is not high. Close the
filling hole and put the soaker bottle that contains the storage solution on the probe when not in use.
Refer to 

Figure 7

. Keep the probe in a vertical position with the sensor and reference junction below

the liquid level in the soaker bottle. Add storage solution to the soaker bottle if necessary.

Figure 7  Probe storage

English

   

15

Содержание PHC735

Страница 1: ...DOC022 53 80434 PHC735 05 2021 Edition 2 User Manual...

Страница 2: ......

Страница 3: ...rocedure 8 Section 6 Sample measurement 9 6 1 Sample requirements 9 6 2 Sample measurement notes 9 6 3 Sample measurement procedure 9 Section 7 Verify the calibration 10 7 1 Verification procedure 10...

Страница 4: ...Table of Contents 2...

Страница 5: ...kaline samples Figure 1 Probe overview 1 Probe soaker bottle with storage solution 5 Probe soaker bottle holder 2 Filling hole plug 6 Electrode filling and storage solution 3 Protective tape and filli...

Страница 6: ...nufacturing defects but not improper use or wear Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical probes are intended for use by individuals who measure water qu...

Страница 7: ...probe with a blocked filling hole will not operate correctly New probes are filled with electrolyte filling solution and have a soaker bottle that contains storage solution to keep the glass bulb and...

Страница 8: ...e meter starts for the first time or after battery replacement 8 Connect the probe to the meter 9 Remove the filling hole plug before use Keep the level of the electrolyte filling solution above the l...

Страница 9: ...e pH units apart For a one point calibration use a pH buffer near the expected sample pH Use the default calibration options or change the options in the probe settings menu Use the single display mod...

Страница 10: ...ffer solution Make sure that the sensor and reference junction are fully in the solution Do not put the probe on the bottom or sides of the beaker 6 Shake the probe from side to side to refresh the re...

Страница 11: ...purity or low ionic strength LIS samples absorb gases from the air that can change the sample pH For stable measurements use an LIS chamber or a flow cell 6 2 Sample measurement notes Read the notes...

Страница 12: ...res the selected pH buffer value to the measured pH value and accepts or rejects the measurement The user can change the pH buffer solution and acceptance criteria for verification in the probe specif...

Страница 13: ...ample material stays on the probe 1 Rinse the probe with deionized water Use warm 35 45 C 95 113 F deionized water to remove storage solution that dries on the probe Dry the probe body with a lint fre...

Страница 14: ...nctions Electrode cleaning solution for porous pin diaphragm reference junctions Thiourea 3 hours with stirring or until the porous plug becomes white 8 2 Fill the probe Add electrolyte filling soluti...

Страница 15: ...s less than 0 5 cm 0 2 in or when the sample temperature is more than 60 C 140 F Refer to Figure 5 and Table 2 for preparation Mix some of the filling solution with the crystals to help move the cryst...

Страница 16: ...d KCl crystals from the probe as possible Discard the solution and KCl crystals 3 Remove the remaining KCl crystals as follows a Fill the probe half full with deionized water Close the filling hole b...

Страница 17: ...N O T I C E Probes can become permanently damaged if kept in a storage solution that is not specified by the manufacturer Use only the specified storage solution saturated KCl Do not store the probe i...

Страница 18: ...ilization or inaccurate measurements The sample absorbs carbon dioxide CO2 from the air which causes the pH value to slowly decrease in low ionic strength LIS or high purity samples Use the LIS chambe...

Страница 19: ...Item no pH 4 01 buffer solution Singlet one use packets 20 mL each 20 pkg 2770020 pH 7 00 buffer solution Singlet one use packets 20 mL each 20 pkg 2770120 pH 10 01 buffer solution Singlet one use pac...

Страница 20: ...pkg SM5010 Beaker 30 mL plastic red 80 pkg SM5011 Beaker 30 mL plastic yellow 80 pkg SM5012 Beaker 30 mL plastic blue 80 pkg SM5013 Beaker 30 mL plastic green 80 pkg SM5014 Beaker dispenser and holder...

Страница 21: ......

Страница 22: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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